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Facile Synthesis of Fe/Cr-Codoped ZnO Nanoparticles with Excellent Adsorption Performance for Various Pollutants

Journal of Ocean University of China 2021年第2期20卷 349-360页

作者： SUN Yongkai LUO Siqi XING Jing LI Zhenjiang MENG Alan College of Electromechanical Engineering Qingdao University of Science and TechnologyQingdao 266061China gaomi campus Qingdao University of Science and TechnologyGaomi 266000China Key Laboratory of Sensor Analysis of Tumor Marker Ministry of EducationCollege of Chemistry and Molecular EngineeringQingdao University of Science and TechnologyQingdao 266042China

Adsorption is an effective and low-cost method for removing antibiotics and dyes. However, it remains a challenge to prepare an adsorbent with excellent adsorption properties for both various antibiotics and dyes. Herein, Fe/Cr-codoped ZnO with high adsorption capacity and fast adsorption rate are prepared by an environmentally friendly solvothermal method. Fe/Cr-codope ZnO with a diameter of 10–20 nm exhibits superior adsorption capacities for the antibiotics of tetracycline hydrochloride(TC-HCl)(826.45 mg g-1) and tetracycline(TC)(331.01 mg g-1), and anionic dyes of methyl orange(MO)(1023.88 mg g-1), methyl blue(MB)(726.26 mg g-1) and direct red(DR)(642.25 mg g-1). Meanwhile, it presents fast adsorption rate, it only took 30 min to reach more than 90% of the equilibrium adsorption amount for TC-HCl, TC, MO, MB and DR. The adsorption process closely fitted the Langmuir isotherm model and pseudo second-order rate equation. More importantly, simple method has been developed for separating the pollutant from the adsorbent, which not only regenerates the materials, but also completes the recovery of antibiotics and dyes, avoiding the secondary pollution. The broad-spectrum, rapid, environment-friendly and effective adsorption properties make Fe/Crcodoped ZnO a promising adsorbent for water treatments.

关键词： antibiotics dyes codoped adsorption regeneration

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An Equivalent Substitute Strategy for Constructing 3D Ordered Porous Carbon Foams and Their Electromagnetic Attenuation Mechanism

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Nano-Micro Letters 2022年第10期14卷 15-35页

作者： Meng Zhang Hailong Ling Ting Wang Yingjing Jiang Guanying Song Wen Zhao Laibin Zhao Tingting Cheng Yuxin Xie Yuying Guo Wenxin Zhao Liying Yuan Alan Meng Zhenjiang Li College of Materials Science and Engineering College of Electromechanical EngineeringQingdao University of Science and TechnologyQingdao 266061People’s Republic of China State Key Laboratory Base of Eco-Chemical Engineering College of Chemistry and Molecular EngineeringCollege of Chemical Engineering in Gaomi CampusQingdao University of Science and TechnologyQingdao 266042People’s Republic of China

Three-dimensional(3D)ordered porous carbon is generally believed to be a promising electromagnetic wave(EMW)absorbing ***,most research works targeted performance improvement of 3D ordered porous carbon,and the specific attenuation mechanism is still ***,in this work,a novel ultra-light egg-derived porous carbon foam(EDCF)structure has been successfully constructed by a simple carbonization combined with the silica microsphere template-etching *** on an equivalent substitute strategy,the influence of pore volume and specific surface area on the electromagnetic parameters and EMW absorption properties of the EDCF products was confirmed respectively by adjusting the addition content and diameter of silica *** a primary attenuation mode,the dielectric loss originates from the comprehensive effect of conduction loss and polarization loss in S-band and C band,and the value is dominated by polarization loss in X band and Ku band,which is obviously greater than that of conduction ***,in all samples,the largest effective absorption bandwidth of EDCF-3 is 7.12 GHz under the thickness of 2.13 mm with the filling content of approximately 5 wt%,covering the whole Ku ***,the EDCF-7 sample with optimized pore volume and specific surface area achieves minimum reflection loss(RL_(min))of−58.08 dB at 16.86 GHz while the thickness is 1.27 *** outstanding research results not only provide a novel insight into enhancement of EMW absorption properties but also clarify the dominant dissipation mechanism for the porous carbon-based absorber from the perspective of objective experiments.

关键词： Porous carbon foam Electromagnetic wave absorption Adjustable pore structure Polarization loss Attenuation mechanism

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Boosted electromagnetic wave absorption performance from synergistic induced polarization of SiC_(NWs)@MnO_(2)@PPy heterostructures

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Nano Research 2023年第2期16卷 3558-3569页

作者： Meng Zhang Laibin Zhao Wenxin Zhao Ting Wang Liying Yuan Yuying Guo Yuxin Xie Tingting Cheng Alan Meng Zhenjiang Li College of Electromechanical Engineering Key Laboratory of Polymer Material Advanced Manufacturing’s Technology of Shandong provinceCollege of Materials Science and EngineeringQingdao University of Science and TechnologyQingdao 266061China Key Laboratory of Optic-electric Sensing and Analytical Chemistry for Life Science MOEShandong Key Laboratory of Biochemical AnalysisCollege of Gaomi CampusCollege of Chemistry and Molecular EngineeringQingdao University of Science and TechnologyQingdao 266042China

In the last decade,electromagnetic pollution has caused people’s considerable *** absorbing material with low cost,lightweight,simple preparation,and high electromagnetic attenuation efficiency has become a feasible means to deal with this *** this work,core–shell SiC_(NWs)@MnO_(2)@PPy(NWs:nanowires,PPy:polypyrrole)heterostructures composed of SiC nanowires core,MnO_(2)nanosheets inter-layer,and PPy coating were successfully prepared through chemical vapor deposition and two-step electrodeposition *** advantage of the interfacial polarization and dipole polarization,the obtained product displays excellent electromagnetic wave absorption performances with the minimum reflection loss(RLmin)of−50.59 dB when the matching thickness is 2.41 mm,and the optimal effective absorption bandwidth(EAB)value reaches to 6.64 GHz at a matching thickness of 2.46 mm,revealing that the SiC_(NWs)@MnO_(2)@PPy nanocomposite could be served as a promising electromagnetic wave absorbing *** the basis of systematic analysis concerning the electromagnetic parameters,the dissipation process of the incident electromagnetic wave was demonstrated reasonably,which may provide a referable preparation strategy for novel heterostructures,especially nonmagnetic lightweight absorbing material.

关键词： SiC nanowires heterostructure polarization loss electromagnetic wave absorption attenuation mechanism

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