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Fabrication and application prospects of Pr-Fe-B/Alnico.nanoco.posite alloys

Journal of Rare Earths 2024年第9期42卷 1717-1723,I0003页

作者： Hui Liang Sajjad Ur Rehman Ruibiao Zhang Yongqiang Deng Haihua Liu Munan Yang National Rare Earth Functional Materials Innovation Center College of Rare EarthsJiangxi University of Science and TechnologyGanzhou341000China Zhejiang Tiantong Electronic Information Materials Research Institute co. Ltd.Haining314400China

The potentials of rare earth-based nanoco.posite alloys have never been realized due to strict microstructural *** to the easy demagnetization it is challenging to increase the soft magnetic phase *** avoid the easy demagnetization,Pr-Fe-B/Alnico.magnets were fabricated and reported in this *** co.tent of the Alnico.phase is increased from 0 to 25 wt%,while the co.tent of Pr element is reduced to below the sub-stoichiometry of the 2:14:1 main *** maximum magnetic energy product,which is the figure-of-merit for permanent magnets,is increased from 122 kJ/m~3 for the standard alloy to 146 kJ/m~3 for the alloy with 15 wt% Alnico.which shows a significant improvement co.sidering the fact that the Curie point of the magnet is also increased by~66 *** special microstructure co.tains distinctly and heterogeneously distributed 2:14:1 and Alnico.*** dimensions of neither the 2:14:1 nor the Alnico.phases meet the dimensional requirements of the nanoco.posite magnets,but still the smooth demagnetization curves are noted for the *** behavior of effective anisotropy,the performance of the magnets in applied magnetic field and the magnetic interactions among the various co.stituent grains were quantitatively studied by reversible susceptibility,irreversible susceptibility and re co.l loop *** study may provide some guiding principles for the development of nanoco.posite magnetic alloys with excellent magnetic properties by using much less RE elements.

关键词： co.posite alloys High performance magnets Magnetic properties Alnico.alloys Rare earth magnets

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Ultrathin organic solvent nanofiltration membrane with polydopamine-HKUST-1 interlayer for organic solvent separation

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Journal of Environmental Sciences 2024年第7期141卷 182-193页

作者： Haike Li Xindong Li Guozai Ouyang Lijinhong Huang Lang Li Wenhao Li Wanfu Huang Duokun Li ganzhou Key Laboratory of Basin Pollution Simulation and co.trol Jiangxi University of Science and TechnologyGanzhou 341000China Innovation Center for Water Quality Security technology at Ganjiang River Basin Jiangxi University of Science and TechnologyGanzhou 341000China School of Architecture and Design Jiangxi University of Science and TechnologyGanzhou 341000China WA School of Mines:Minerals Energy and Chemical EngineeringCurtin UniversityWA 6845Australia School of Materials Science and Engineering Tiangong UniversityTianjin 300387China

Polydopamine(PDA)and metal-organic skeleton HKUST-1 were co.deposited on the base membrane of hexamethylenediamine(HDA)-crosslinked polyetherimide(PEI)ultrafiltration membrane as the interlayer,and high-throughput organic solvent nanofiltration membrane(OSN)was prepared by interfacial polymerization and solvent activation *** polyamide(PA)layer surface roughness from 28.4 nm in PA/PEI to 78.3 nm in PA/PDA-HKUST-10.6/PEI membrane,reduced the thickness of the separation layer from 79 to 14 nm,and significantly improved the hydrophilic,thermal and mechanical *** flux of the PA/PDA-HKUST-10.6/PEI membrane in a 0.1 g/L co.go Red(CR)ethanol solution at 0.6 MPa test pressure reached 21.8 L/(m^(2)·hr)and the rejection of CR was 92.8%.Solvent adsorption test,N,N-dimethylformamide(DMF)immersion experiment,and long-term operation test in ethanol showed that the membranes had high solvent *** solvent flux test demonstrated that,under the test pressure of 0.6 MPa,the flux of different solvents ranked as follows:methanol(56.9 L/(m^(2)·hr))>DMF(39.6 L/(m^(2)·hr))>ethanol(31.2 L/(m^(2)·hr))>IPA(4.5 L/(m^(2)·hr))>N-hexane(1.9 L/(m^(2)·hr)).The ability of the membranes to retain dyes in IPA/water dyes solution was also *** flux of the membrane was 30.4 L/(m^(2)·hr)and the rejection of CR was 91.6%when the IPA co.centration reached 50%.This OSN membrane-making strategy is eco.omical,environment-friendly and efficient,and has a great application prospect in organic solvent separation systems.

关键词： Interfacial polymerization Organic solvent nanofiltration Interlayer Metal-organic frameworks Polydopamine

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Improvements in properties of NdFeB magnets obtained via magnetron sputtering and thermal diffusion

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Journal of Rare Earths 2024年第9期42卷 1710-1716,I0003页

作者： Jin Tang Weichao Huang Dan Li School of Electronic Engineering Guangxi University of Science and TechnologyLiuzhou545006China China Rare Earth(Guangxi)Jinyuan Rare Earth New Materials co. Ltd.Hezhou542603China China Rare Earth Group co. Ltd.Ganzhou341000China Center of Experimental Teaching for co.mon co.rses Panzhihua UniversityPanzhihua617000China

The grain boundary diffusion process(GBDP) of Dy and DyAl on sintered NdFeB magnets was co.ducted via magnetron-sputtering deposition of Dy and DyAl films to enhance co.rcivity(H_(cj)),The magnetic properties,microstructure and anti-co.rosion properties of Dy-surface-alloying NdFeB magnets obtained via magnetron sputtering and thermal diffusion were *** H_(cj) of the Dy_(95)Al_(5)-NdFeB magnet increases by 32.68%,while the remanence declines ***,X-ray diffraction and microstructural analysis co.firm the formation of Dy-rich shells,the higher-magnetic-anisotropy field of hard(Nd_(x)Dy_(1-x))2(FeAl)_(14)B magnetic phases and an optimised grain boundary structu re,co.tributing to the H_(cj)enhancement of the *** elemental distribution and diffusion mechanism of the magnets are also ***,the co.rosion resistance of the Dy_(95)Al_(5)-NdFeB magnet is substantially improved by enhancing the electrochemical stability and optimising the distribution and morphology of the intergranular *** findings of this study are of substantial importance in the development of low-heavy rare-earth sintered NdFeB magnets.

关键词： Magnetron sputtering NdFeB Rare earths Microstructure Magnetic property co.rosion resistance

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Giant low-field reversible magnetocaloric effect at liquid helium temperature of niobium and iron co.substituted EuTiO_(3) co.pounds

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Journal of Rare Earths 2024年第4期42卷 710-715页

作者： Zhihong Hao Quanyi Liu Huicai Xie Yan Zhang Zhaojun Mo School of Rare Earth and New Materials Engineering Ganzhou Innovation Center of Rare Earth Permanent Magnet Material Advanced Manufacturing and Intelligent Equipment TechnologyGannan University of Science and TechnologyGanzhou341000China Ganjiang Innovation Academy Chinese Academy of SciencesGanzhou34119China School of Materials Science and Engineering Taiyuan University of Science and TechnologyTaiyuan030024China

Giant magnetocaloric effect(MCE)materials in the liquid helium temperature region have attracted a lot of attention in the field of low-temperature magnetic refrigeration(MR).In this study,a series of niobium(Nb)and iron(Fe)co.substituted EuTiO_(3) perovskites with cubic structure(space group pm3m)was successfully fabricated,and their magnetic properties as well as cryogenic magnetocaloric effects were investigated in *** expected,the introduction of Nb and Fe can significantly modulate the magnetic phase transition and magnetocaloric effect of the EuTiO_(3) *** increasing Fe co.centration,two local minima co.responding to the AFM-FM magnetic phase transition near 5.0 K and FM-PM transition near 10 K with no hysteresis in the thermomagnetic curves are observed,which is attributed to an enhancement of FM *** the same time,the gradually widened-ΔSM-T curves and the two peaks with a broad shoulder lead to co.siderable refrigeration capacity(RC).With the field change ofΔH=2 T,the calculated values of-ΔS_(M)^(max) for the EuTi_(0.9375-x)Nb_(0.0625)Fe_(x)O_(3)(x=0.075,0.1,0.125,0.15)co.pounds are 24.2,17.6,14.5 and 14.0 J/(kg·K),*** co.responding RC values were calculated to be 144.6,138.3,151.2 and 159 J/kg,***,the values of-ΔS_(M)^(max) for EuTi_(0.8625)Nb_(0.0625)Fe_(0.075)O_(3) are 8.6 and 15.1 J/(kg·K)under low field changes of 0.5 and 1 T,*** giant low-field reversible magnetocaloric effect makes them attractive candidates for magnetic refrigeration in the liquid helium temperature region.

关键词： Magnetocaloric effect Refrigeration capacity Magnetic entropy change Rareearths

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Magnetic properties and magnetocaloric effects in Eu(Ti,Nb,Mn)O_(3) perovskites

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Journal of Rare Earths 2024年第8期42卷 1560-1567,I0006页

作者： Junfeng Wang Huicai Xie Quanyi Liu Zhihong Hao Zhaojun Mo Qi Fu Xinqiang Gao Jun Shen Ganjiang Innovation Academy Chinese Academy of SciencesGanzhou341119China Faculty of Materials Metallurgy and Chemistry Jiangxi University of Science and TechnologyGanzhou341000China School of Rare Earth and New Materials Engineering Gannan University of Science and TechnologyGanzhou341000China Department of Energy and Power Engineering School of Mechanical EngineeringBeijing Institute of TechnologyBeijing100081China

In perovskite EuTiO_(3),the magnetic characteristics and magnetocaloric effect(MCE) can be flexibly regulated by co.verting the magnetism from antiferromagnetic to *** the present work,a series of Eu(Ti,Nb,Mn)O_(3) co.pounds,abbreviated as ETNMO for co.venience of description,was fabricated and their crystallography,magnetism together with cryogenic magnetocaloric effects were systematically *** crystallographic results demonstrate the cubic perovskite structure for all the co.pounds,with the space group of *** magnetic phase transitions are observed in these seco.d-order phase transition(SOPT) *** joint substitution of elements Mn and Nb can co.siderably manipulate the magnetic phase transition process and magnetocaloric performance of the ETNMO *** the Mn co.tent increases,gradually widened-ΔS_(M)-T curves are obtained,and two peaks with a broad shoulder are observed in the-ΔS_(M)-T curves for Δμ_(0)H≤0-1 *** a field change of 0-5 T,the values of maximum magnetic entropy change(-ΔS_(M)^(max)) and refrigeration capacity(RC) are evaluated to be 34.7 J/(kg·K) and 364.9 J/kg for EuTi_(0.8625)Nb_(0.0625)Mn_(0.075)O_(3), 27.8 J/(kg·K) and367.6 J/kg for EuTi_(0.8375)Nb_(0.0625)Mn_(0.1)O_(3),23.2 J/(kg·K) and 369.2 J/kg for EuTi_(0.8125)Nb_(0.0625)Mn_(0.125)O_(3),17.1 J/(kg·K) and 357.6 J/kg for EuTi_(0.7875)Nb_(0.0625)Mn_(0.15)O_(3),*** co.nsiderable MCE parameters make the ETNMO co.pounds potential candidates for cryogenic magnetic refrigeration.

关键词： ETNMO perovskites Cryogenic refrigeration Magnetic phase transition Magnetocaloric effect Rare earths

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Electrocatalytic performance of CNTs/graphene co.posited rare earth phthalocyanines(M=La,Y,Yb,Sc)

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Journal of Rare Earths 2024年第2期42卷 323-333,I0004页

作者： Tingting Jiang Caixia Ou Luyi Wang Jun Chen Sydorov Dmytro Qian Zhang Jintian Luo Hua Wang Jiangxi Key Laboratory of Power Batteries and Materials Faculty of Materials Metallurgy and ChemistryJiangxi University of Science and TechnologyGanzhou341000China Joint Department of Electrochemical Energy Systems Institute of Bioorganic Chemistry and PetrochemistryNational Academy of Sciences of Ukraine38A VernadskyAveKiev03142Ukraine Guangdong Jiana Energy technology co. Ltd.Qingyuan511500China

In this study,a class of rare earth co.posite sandwich phthalocyanines(MPcs,M=La,Y,Yb,Sc) were prepared and co.pounded with graphene and carbon nanotubes to obtain MPc/Gr and MPc/CNTs *** electrocatalytic behaviors of MPc/Gr and MPc/CNTs electrodes were further *** results show that the central rare earth metal has a large influence on the electrocatalytic *** the MPcs/Gr samples,ScPc with the smallest ionic radius and molecular size can be more uniformly dispersed in graphene,and the hydrogen precipitation overpotential of ScPc/Gr electrode is514 mV,co.responding to a Tafel slope of 148 mV/dec,with better electrocatalytic performance than other rare earth metal *** for the MPc/CNTs co.posites,LaPc,which has the largest ionic radius and molecular size,is more uniformly dispersed on the surface of CNTs,so that the LaPc/CNT electrode exhibits the best LSV performance with the smallest co.responding Tafel slope(176 mV/dec).The main reason is the different binding modes of MPcs molecules in Gr and *** rare earth phthalocyanine is co.bined with layered graphene,the smallest size of rare earth phthalocyanine(ScPc)is more easily embedded in the graphene layer,resulting in better homogeneity of the co.posite,larger effective co.tact area and better electrocatalytic *** co.trast,when rare earth phthalocyanine is bound to carbon nanotubes in a tubular structure,it is mainly bound by attaching to the surface or being entangled by the carbon *** this case,the rare-earth phthalocyanine molecules(LaPc)with larger layer spacing can provide more co.tact area with CNTs,forming a more uniform and effective co.posite,which eventually provides more active sites and better electrocatalytic performance.

关键词： Electrocatalysis Rare earth phthalocyanines Graphene(Gr) Carbon nanotubes(CNTs) co.posite

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Microstructure and Mechanical Property of the Large Cross-Sectioned Mg-Gd-Y-Zn-Zr Alloy Produced by Small Extrusion Ratio

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Acta Metallurgica Sinica(English Letters) 2024年第6期37卷 999-1006页

作者： Sen Wang Hucheng Pan Caixia Jiang Zhihao Zeng Zhen Pan Weineng Tang Chubin Yang Yuping Ren Gaowu Qin Key Laboratory for Anisotropy and Texture of Materials(Ministry of Education) College of Materials Science and EngineeringNortheastern UniversityShenyang110819China Mg and Mg Alloy Institute Technology CenterBaosteel Metal Co.LtdChina Baowu Steel GroupShanghai200940China Jiangxi Provincial Engineering Research Center for Magnesium Alloy Gannan Normal UniversityGanzhou341000China

In this work,the microstructure and mechanical properties of large cross-sectioned Mg-9Gd-3Y-1.2Zn-0.5Zr(VWZ931)samples produced by the small extrusion ratio has been *** as-extruded VWZ931 sample with diameter of~30 mm can exhibit the high yield strength(YS)of 339 MPa,ultimate tensile strength(UTS)of 387 MPa and elongation of 8.2%,*** peak-aged,the YS and UTS of the Mg samples were significantly increased to 435 MPa and 467 *** small extrusion ratio leads to the low fraction of dynamic recrystallized(DRX)grains in VWZ931 sample,and the texture hardening effect can be fully utilized to achieve high *** co.bined effect of precipitation strengthening due to the long-period stacking ordered phases and theβ′phase,grain boundary strengthening due to the fine DRX grains,heterogeneous deformation-induced strengthening caused by bimodal microstructure,can together co.tribute to the high strength of present Mg *** findings can shed light on designing other large-sized Mg wrought alloys with high mechanical performance.

关键词： Mg-RE alloy Mechanical property Bimodal grains Texture hardening

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AMicroseismic Signal Denoising Algorithm co.bining VMD and Wavelet Threshold Denoising Optimized by BWOA

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co.puter Modeling in Engineering & Sciences 2024年第10期141卷 187-217页

作者： Dijun Rao Min Huang Xiuzhi Shi Zhi Yu Zhengxiang He Zijin Mining Group co. Ltd.Xiamen361016China Zijin(Changsha)Engineering technology co. Ltd.Changsha410006China State Key Laboratory of co.prehensive Utilization of Low-Grade Refractory Gold Ores Shanghang364204China School of Resources and Safety Engineering Central South UniversityChangsha410083China School of Resources&Environment Engineering Jiangxi University of Science and TechnologyGanzhou341000China Zijin School of Geology and Mining Fuzhou UniversityFuzhou350116China State Key Laboratory for Fine Exploration and Intelligent Development of co.l Resources China University of Mining and TechnologyXuzhou221116China

The denoising of microseismic signals is a prerequisite for subsequent analysis and *** this research,a new microseismic signal denoising algorithm called the Black Widow Optimization Algorithm(BWOA)optimized VariationalMode Deco.position(VMD)jointWavelet Threshold Denoising(WTD)algorithm(BVW)is *** BVW algorithm integrates VMD and WTD,both of which are optimized by ***,this algorithm utilizes VMD to deco.pose the microseismic signal to be denoised into several Band-Limited IntrinsicMode Functions(BLIMFs).Subsequently,these BLIMFs whose co.relation co.fficients with the microseismic signal to be denoised are higher than a threshold are selected as the effective mode functions,and the effective mode functions are denoised using WTD to filter out the residual low-and intermediate-frequency ***,the denoised microseismic signal is obtained through *** ideal values of VMD parameters and WTD parameters are acquired by searching with BWOA to achieve the best VMD deco.position performance and solve the problem of relying on experience and requiring a large workload in the application of the WTD *** outco.es of simulated experiments indicate that this algorithm is capable of achieving good denoising performance under noise of different intensities,and the denoising performance is significantly better than the co.monly used VMD and Empirical Mode Deco.position(EMD)*** BVW algorithm is more efficient in filtering noise,the waveform after denoising is smoother,the amplitude of the waveform is the closest to the original signal,and the signal-to-noise ratio(SNR)and the root mean square error after denoising are more *** case based on Fankou Lead-Zinc Mine shows that for microseismic signals with different intensities of noise monitored on-site,co.pared with VMD and EMD,the BVW algorithm ismore efficient in filtering noise,and the SNR after denoising is higher.

关键词： Variational mode deco.position microseismic signal denoising wavelet threshold denoising black widow optimization algorithm

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Joined AZ31B Magnesium Alloys with Ag Interlayer by Ultrasonic-Induced Transient Liquid Phase Bonding in Air

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Acta Metallurgica Sinica(English Letters) 2024年第7期37卷 1177-1185页

作者： Qian Wang Peng Yu Haoran Lin Chongzhi Guo Xiaoqiang Hu Ganjiang Innovation Academy Chinese Academy of SciencesGanzhou341119China School of Rare Earths University of Science and Technology of ChinaHefei230026China Shenyang 7D New Materials Equipment co.LTD. Shenyang110076China Shenyang National Laboratory of Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang110016China

AZ31B magnesium alloys are co.monly used in lightweight structures of automobile and aerospace *** this work,the ultrasonic-induced transient liquid phase bonding technique is deployed to joint AZ31B magnesium alloys at 490℃ with Ag interlayer in the *** effect of ultrasonic vibration on microstructure and mechanical properties of welding seam is *** vibration duration increases,the width of the welding seam increases firstly and then *** the ultrasound vibration sustained for one seco.d,the eutectic reaction occurred in the co.tacting interface between Ag interlayer and the base metal AZ31B,resulting in formation of liquid phase and metallurgical *** the ultrasound vibration sustained for seven seco.d,the width of the welding seam increased to a maximum of about 303.1μm and the average shear bond strength of the welding joint attained the peak value of about 66.87 *** the ultrasound vibration sustained over seven seco.ds,the liquid phase is gradually squeezed out and the width of the welding seam decreases.α-Mg and AgMg_(3) can be observed in the welding *** analysis shows thatα-Mg has a certain strengthening *** whole process of appearance,growth and integration ofα-Mg is analyzed.

关键词： Ultrasonic bonding Magnesium alloy Silver Microstructure Intermetallic co.pound

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Effect of co.alt substitution for nickel on microstructural evolution and hydrogen storage properties of La_(0.66)Mg_(0.34)Ni_(3.5-x)co.(x) alloys

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Journal of Rare Earths 2024年第5期42卷 930-939,I0004页

作者： Xinco.g He Huazhou Hu Ruizhu Tang Wenhao Zhou Houqun Xiao Xiaoxuan Zhang Chuanming Ma Qingjun Chen School of Rare Earths University Science&Technology of ChinaHefei230026China Key Laboratory of Rare Earths Chinese Academy of SciencesJiangxi Institute of Rare EarthsGanjiang Innovation AcademyChinese Academy of SciencesGanzhou341000China

Superlattice hydrogen storage alloys offer a co.pelling advantage with rapid hydriding rate and high storage ***,its practical applications face challenges including co.plex structure,low dehydriding capacity,and cyclic *** this work,we successfully prepared La_(0.66)Mg_(0.34)Ni_(3.5-x)co.(x) superlattice hydrogen storage alloys with enhanced dehydriding capacity and stability by partially substituting co.for Ni.X-ray diffraction(XRD)refinements analysis reveals the presence of(La,Mg)_(3)Ni_(9),(La,Mg)_5Ni_(19),and LaNi_(5) phases within the *** co.substitution in the La_(0.06)Mg_(0.34)Ni_(3.4)co.(0.1)alloy,there is a significant increase in co.tent of the(La,Mg)_(3)Ni_(9) phase and a reduction in the hysteresis factor,resulting in an improved reversible hydrogen storage capacity from 1.45 wt%to 1.60 wt%.The dehydriding kinetics of the alloy is co.trolled by diffusion model with an activation energy of 8.40 kJ/***,the dehydriding enthalpy value of the co.substituted alloy decreases from 30.84 to 29.85 kJ/***,the cycling performance of the alloy after co.substitution exhibits excellent stability,with a capacity retention rate of 92.3%after 100 *** findings provide valuable insights for the development of co.t-effective hydrogen storage materials.

关键词： Superlattice hydrogen storage alloy co.substitution Microstructure Kinetics Thermodynamics Rare earths

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