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Effects of acid-rock reaction on physical properties during CO_(2)-rich industrial waste gas(CO_(2)-rich IWG)injection in shale reservoirs

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Petroleum Science 2024年第1期21卷 272-285页

作者： Yi-Fan Wang Jing Wang Hui-Qing Liu Xiao-Cong Lv Ze-Min Ji National Key Laboratory of Petroleum Resources and Engineering China University of PetroleumBeijing102249China MOE Key Laboratory of Petroleum Engineering China University of PetroleumBeijing102249China Research Institute of exploration and development PetroChinaBeijing100083China

"Carbon peaking and carbon neutrality"is an essential national strategy,and the geological storage and utilization of CO_(2)is a hot issue ***,due to the scarcity of pure CO_(2)gas sources in China and the high cost of CO_(2)capture,CO_(2)-rich industrial waste gas(CO_(2)-rich IWG)is gradually emerging into the public's ***_(2)has good adsorption properties on shale surfaces,but acidic gases can react with shale,so the mechanism of the CO_(2)-rich IWG-water-shale reaction and the change in reservoir properties will determine the stability of geological ***,based on the mineral composition of the Longmaxi Formation shale,this study constructs a thermodynamic equilibrium model of water-rock reactions and simulates the regularity of reactions between CO_(2)-rich IWG and shale *** results indicate that CO_(2)consumed 12%after reaction,and impurity gases in the CO_(2)-rich IWG can be dissolved entirely,thus demonstrating the feasibility of treating IWG through water-rock *** IWG inhibits the dissolution of CO_(2),the optimal composition of CO_(2)-rich IWG is 95%CO_(2)and 5%IWG when CO_(2)geological storage is the main *** contrast,when the main goal is the geological storage of total CO_(2)-rich IWG or impurity gas,the optimal CO_(2)-rich IWG composition is 50%CO_(2)and 50%*** the CO_(2)-rich IWG-water-shale reaction,temperature has less influence on the water-rock reaction,while pressure is the most important ***2 has the greatest impact on water-rock reaction in *** minerals,clay minerals such as illite and montmorillonite had a significant effect on water-rock *** overall reaction is dominated by precipitation and the volume of the rock skeleton has increased by 0.74 cm3,resulting in a decrease in shale porosity,which enhances the stability of CO_(2)geological storage to some *** the reaction between CO_(2)-rich IWG-water-shale at simulated temperatures and pressures,precipitation

关键词： CO_(2)-rich industrial waste gas Geological storage Acid-rock reaction Shale Geochemical modelling

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Jet Characteristics and Optimization of a Cavitation Nozzle for Hydraulic Fracturing Applications

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Fluid Dynamics & Materials Processing 2024年第1期20卷 179-192页

作者： Yu Gao Zhenqiang Xu Kaixiang Shen Shenzhen South China Sea Oil Economic development Co. Ltd.Shenzhen518000China Guangzhou Marine Geological Survey China Geological SurveyGuangzhou511458China National Engineering Research Center of Gas Hydrate exploration and development Guangzhou511458China

Hydraulic jetting is a form of fracturing that involves using a high-pressure jet of water to create fractures in the reservoir rock with a nozzle serving as the central component of the hydraulic sandblasting perforation *** this study,the flow behavior of the nozzle is simulated numerically in the framework of a SST k-ωturbulence *** results show that the nozzle structure can significantly influence the jet performance and related cavitation *** orthogonal experiments,the nozzle geometric parameters are optimized,and the following configuration is found accordingly:contraction angle 20°,contraction segment length 6 mm,cylindrical segment diameter 6 mm,cylindrical segment length 12 mm,spread segment length 10 mm,and spread angle 55°.

关键词： Cavitation jet angle nozzle hydraulic characteristics nozzle parameters

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Multi-Scale Pore Structure Heterogeneity in Tuff Reservoirs Investigated with Multi-Experimental Method and Fractal Dimensions in Chang 7 Formation,Southern Ordos Basin

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Journal of Earth Science 2024年第2期35卷 666-686页

作者： Hao Lu Qing Li Dali Yue Dongdong Xia Shenghe Wu Lang Wen Yu He State Key Laboratory of Petroleum Resources and Prospecting China University of PetroleumBeijing102249China College of Geosciences China University of PetroleumBeijing102249China Petroleum exploration and development Institute of SINOPEC Beijing100083China

The tight tuff reservoir is an unusual type of unconventional reservoir with strong ***,there is a lack of research on the microscopic pore structure that causes the heterogeneity of tuff *** the Chang 7 Formation in Ordos Basin,China as a case study,carbon-dioxide gas adsorption,nitrogen gas adsorption and high-pressure mercury injection are integrated to investigate the multi-scale pore structure characteristics of tuff ***,the fractal dimension is introduced to characterize the complexity of pore structure in tuff *** this multi-experimental method,the quantitative characterizations of the full-range pore size distribution of four tuff types were obtained and compared in the size ranges of micropores,mesopores and *** dimension curves derived from full-range pores are divided into six segments as D1,D2,D3,D4,D5 and D6 corresponding to fractal characteristics of micropores,smaller mesopores,larger mesopores,smaller macropores,medium macropores and larger macropores,*** macropore volume,average macropore radius and fractal dimension D5 significantly control petrophysical *** larger macropore volume,average macropore radius and D5 correspond to favorable pore structure and good reservoir quality,which provides new indexes for the tuff reservoir *** study enriches the understanding of the heterogeneity of pore structures and contributes to unconventional oil and gas exploration and development.

关键词： tuff reservoir pore structure carbon-dioxide gas adsorption nitrogen gas adsorption high-pressure mercury injection fractal dimension petroleum geology

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The Middle Miocene lobe-shaped and band-shaped submarine fans in the Lingshui Sag,Qiongdongnan Basin:source-to-sink system,genesis and implication

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Acta Oceanologica Sinica 2024年第4期43卷 61-79页

作者： Xingzong Yao Congjun Feng Hongjun Qu Min Zhang Daming Li State Key Laboratory of Continental Dynamics Northwest UniversityXi’an 710069China Department of Geology Northwest UniversityXi’an 710069China exploration and development Technology Research Center of Yanchang Oilfield Co. Ltd.Yan’an 716000China Chexplor Resource exploration Technology Co. Ltd.Huaibei 235000China

Deepwater oil and gas exploration is the key to sustainable breakthroughs in petroleum exploration *** Central Canyon gas field has confirmed the Lingshui Sag is a hydrocarbon-generating sag,and the deepwater reservoirs in the Lingshui Sag still have more fabulous oil and gas exploration *** on drilling data and three-dimensional(3D)seismic data,this paper uses seismic facies analysis,seismic attribute analysis,and coherence slice analysis to identify the types of submarine fans(lobe-shaped and band-shaped submarine fans)that developed in the Lingshui Sag during the Middle Miocene,clarify the source-to-sink system of the submarine fans and discuss the genesis mechanism of the submarine *** results show that:(1)the deepwater source-to-sink system of the Lingshui Sag in the Middle Miocene mainly consisted of a“delta(sediment supply)-submarine canyon(sediment transport channel)-submarine fan(deepwater sediment sink)”association;(2)the main factor controlling the formation of the submarine fans developed in the Lingshui Sag was on the relative sea level decline;and(3)the bottom current reworked the lobe-shaped submarine fan that developed in the northern Lingshui Sag and formed the band-shaped submarine fan with a greater sand *** paper aims to provide practical geological knowledge for subsequent petroleum exploration and development in the deepwater area of the Qiongdongnan Basin through a detailed analysis of the Middle Miocene submarine fan sedimentary system developed in the Lingshui Sag.

关键词： submarine fan source-to-sink system genesis mechanism Middle Miocene Lingshui Sag

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Horizontal well spacing optimization and gas injection simulation for the ultra-low-permeability Yongjin reservoir

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Energy Geoscience 2024年第1期5卷 196-203页

作者： Yao Zhang Chengyuan Lv Zengmin Lun Shuxia Zhao Yingfu He Ran Gao SINOPEC exploration and Production Research Institute BeijingChina

Optimal spacing for vertical wells can be effectively predicted with several published methods,but methods suitable for assessing the proper horizontal well spacing are *** work proposes a method for calculating the optimal horizontal well spacing for an ultra-low permeability reservoir e the Yongjin reservoir in the Juggar Basin,northwestern *** result shows that a spacing of 640m is the most economical for the development of the *** better develop the reservoir,simulation approaches are used and a new model is built based on the calculated well *** the reservoir has an ultralow permeability,gas injection is regarded as the preferred enhanced oil recovery(EOR)*** of different gases including carbon dioxide,methane,nitrogen and mixed gas are *** results show that carbon dioxide injection is the most efficient and economical for the development of the ***,if the reservoir produces enough methane,reinjecting methane is even better than injecting carbon dioxide.

关键词： Ultra-low-permeability reservoir Well spacing optimization Numerical simulation Gas injection EOR

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Mechanical characteristics and reservoir stimulation mechanisms of the Gulong shale oil reservoirs, the northern Songliao Basin

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Petroleum Science 2024年第3期21卷 2023-2036页

作者： Si-Wei Meng Jia-Ping Tao Tian-Jiao Li Dong-Xu Li Su-Ling Wang Liu Yang Xin Liu Li-Hao Liang He Liu PetroChina Research Institute of Petroleum exploration development National Key Laboratory of Continental Shale Oil Dalian University of Technology PetroChina Daqing Oilfield Co.Ltd. Northeast Petroleum University China University of Mining and Technology (Beijing)

Shale oil of the Qingshankou Formation of the Gulong Sag, the northern Songliao Basin, represents the first attempt at large-scale development of pure-shale-type shale oil in China. By integrating the multiscale refined reservoir characterization with macro-micro-scale mechanical testing, it is clarified that the Gulong shale is characterized by high clay mineral content, high rock plasticity, highly-developed bedding, and prominent mechanical anisotropy. A three-dimensional(3D) fracture propagation model of hydraulic fracturing was built for the Gulong shale, which fully captures the hydraulic fracture distribution pattern affected by the high bedding density, in-situ stress, and fracturing treatment parameters. Our research showed that due to influences of bedding, hydraulic fracturing in the Gulong shale forms a complex fracture morphology featuring the main fracture with multiple perpendicular branches that have different lengths(like the outdoor directional TV antenna); however, the vertical propagation of fractures is inhibited, and the fracture height is commonly less than 10 m. The limited stimulated reservoir volume(SRV) is the main problem facing the fracturing stimulation of the Gulong shale *** density has vital effects on fracture morphology, so case-specific fracturing designs shall be developed for shale intervals with different bedding development degrees. For reservoirs with welldeveloped bedding, it is suggested to properly increase the perforation cluster spacing and raise the volume and proportions of viscous fluids of the pad, so as to effectively promote vertical fracture propagation and improve reservoir stimulation performance. This study integrates multi-scale fine reservoir characterization and macro-micro-scale mechanical testing, as well as the construction and numerical simulation of hydraulic fracturing models for high-density layered shale reservoirs, providing a new approach and methodological framework for the fracturing rese

关键词： Shale oil Hydraulic fracturing High bedding density Fracture propagation model

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Identifying the real fracture hidden in rock microcrack zone by acoustic emission energy

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International Journal of Mining Science and Technology 2024年第6期34卷 731-746页

作者： Yuekun Xing Bingxiang Huang Guangqing Zhang Binghong Li Hang Xu Xuejie Jiao Yang Yu Taisen Han Jinlong Chen State Key Laboratory for Fine exploration and Intelligent development of Coal Resources China University of Mining and TechnologyXuzhou 221116China State Key Laboratory of Petroleum Resources and Engineering China University of Petroleum-BeijingBeijing 102249China

Identifying the real fracture of rock hidden in acoustic emission(AE)source clusters(AE-depicted microcrack zone)remains challenging and *** we revealed the AE energy(representing dissipated energy)distribution rule in the rock microcrack zone and proposed an AE-energy-based method for identifying the real fracture.(1)A set of fracture experiments were performed on granite using wedgeloading,and the fracture process was detected and recorded by *** microcrack zone associated with the energy dissipation was characterized by AE sources and energy distribution,utilizing our selfdeveloped AE analysis program(RockAE).(2)The accumulated AE energy,an index representing energy dissipation,across the AE-depicted microcrack zone followed the normal distribution model(the mean and variance relate to the real fracture path and the microcrack zone width).This result implies that the nucleation and coalescence of massive cracks(i.e.,real fracture generation process)are supposed to follow a normal distribution.(3)Then,we obtained the real fracture extension path by joining the peak positions of the AE energy normal distribution curve at different cross-sections of the microcrack ***,we distinguished between the microcrack zone and the concealed real fracture within *** deviation was validated as slight as 1–3 mm.

关键词： GeoEnergy exploitation Rock fracture Fracture identification Acoustic emission AE energy analysis

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Depositional model of the Member Deng-2 marginal microbial mound-bank complex of the Dengying Formation in the southwestern Sichuan Basin, SW China: Implications for the Ediacaran microbial mound construction and hydrocarbon exploration

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Petroleum Science 2024年第2期21卷 806-822页

作者： Jin-Min Song Xin Jin Zhong Luo Shu-Gen Liu Shao-Bo Liu Xing-Zhi Ma Zhi-Wu Li Xue-Song Lu Ling-Li Zhao Ke-Ran Li Jia-Xin Ren Li-Zhou Tian Hao-Shuang Deng State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation Chengdu University of TechnologyChengdu610059SichuanChina PetroChina Research Institute of Petroleum exploration and development Beijing100083China Xihua University Chengdu610039SichuanChina

Recent advances in hydrocarbon exploration have been made in the Member Deng-2 marginal microbial mound-bank complex reservoirs of the Dengying Formation in the western Sichuan Basin, SW China,where the depositional process is regarded confusing. The microfacies, construction types, and depositional model of the Member Deng-2 marginal microbial mound-bank complex have been investigated using unmanned aerial vehicle photography, outcrop section investigation, thin section identification,and seismic reflections in the southwestern Sichuan Basin. The microbialite lithologic textures in this region include thrombolite, dendrolite, stromatolite, fenestral stromatolite, spongiostromata stone,oncolite, aggregated grainstone, and botryoidal grapestone. Based on the comprehensive analysis of“depositional fabrics-lithology-microfacies”, an association between a fore mound, mound framework,and back mound subfacies has been proposed based on water depth, current direction, energy level and lithologic assemblages. The microfacies of the mound base, mound core, mound flank, mound cap, and mound flat could be recognized among the mound framework subfacies. Two construction types of marginal microbial mound-bank complex have been determined based on deposition location, mound scale, migration direction, and sedimentary facies association. Type Jinkouhe microbial mound constructions(TJMMCs) develop along the windward margin owing to their proximity to the seaward subfacies fore mound, with a northeastwardly migrated microbial mound on top of the mud mound,exhibiting the characteristics of large-sized mounds and small-sized banks in the surrounding area. Type E'bian microbial mound constructions(TEMMCs) primarily occur on the leeward margin, resulting from the presence of onshore back mound subfacies, with the smaller southwestward migrated microbial mounds existing on a thicker microbial flat. The platform margin microbial mound depositional model can be correlated with certain late

关键词： Sichuan Basin The Member Deng-2 Marginal microbial mound-bank complex Depositional model exploration implications

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Rheological study of methane gas hydrates in the presence of micron-sized sand particle

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Chinese Journal of Chemical Engineering 2024年第6期70卷 149-161页

作者： Bohui Shi Shangfei Song Yuchuan Chen Shunkang Fu Lihao Liu Xinyao Yang Haihao Wu Guangjin Chen Jing Gong National Engineering Research Center of Oil and Gas Pipeline Transportation Safety MOE Key Laboratory of Petroleum EngineeringBeijing Key Laboratory of Urban Oil and Gas Distribution TechnologyChina University of Petroleum-BeijingBeijing 102249China China's Oil and Gas exploration and development Company(CNODC) Beijing 100034China China National Petroleum corporation Mozambique LDA MaputoMozambique PipeChina West East Pipeline Company Shanghai 200122China

Natural gas hydrates,intricate crystalline structures formed by water molecules and small gas molecules,have emerged as a significant and globally impactful clean energy ***,their commercial exploitation faces challenges,particularly operational disruptions caused by sand-related *** the rheological properties of hydrate slurry,especially in the presence of micron-sized sand particles,is imperative for ensuring the flow assurance of subsea hydrate *** study extensively investigates the rheological properties of sand-containing hydrate *** findings reveal that these slurries exhibit non-Newtonian fluid characteristics,including yield stress,thixotropy,and shear-thinning ***-like elastic features are observed in sand-containing hydrate slurries before yielding,transitioning to viscous behavior after *** with a minimal amount of sand,both static yield stress and yield strain experience substantial changes,correlating with the increase in sand *** research conclusively establishes the thixotropic nature of sand-hydrate slurries,where the viscosity decay rate is directly influenced by the shear *** insights aim to contribute comprehensively to the development of effective flow assurance strategies,ensuring the safe and stable operation of subsea hydrate exploitation.

关键词： Natural gas hydrate production Sand-containing hydrate slurries Yield stress Thixotropy Shear-thinning behavior

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Paleoenvironment evolution and organic matter enrichment mechanisms in the first member of the Qingshankou Formation,Songliao Basin,China

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Frontiers of Earth Science 2024年第2期18卷 364-383页

作者： Ying LI Min WANG Yu YAN Xin WANG Jinyou ZHANG Xuefeng BAI Yuchen ZHANG Jiaheng XUE Junsheng FEI Lianbin ZHANG Guojun WANG School of Geoscience China University of Petroleum(East China)Qingdao 266580China Shandong Provincial Key Laboratory of Deep Oil and Gas Qingdao 266580China exploration and development Research Institute of Daqing Oilfield Co Ltd. Daqing 163712China exploration Division PetroChina Daqing Oilfield CompanyDaqing 163453China Department of Physics Xiamen University MalaysiaBandar Sunsuria 43900Malaysia

Organic matter is the basis for oil and gas generation,and the depositional environment controls its *** first member of the Qingshankou Formation(K_(2)qn^(1))in Songliao Basin has a thick organic-rich shale and so is an important target section for shale oil exploration and *** the Gulong Sag,shale samples from this unit were collected over the full length of the *** characterization of the environments of deposition(EOD)of K_(2)qn^(1)was improved by utilizing lithological characteristics,thin section observations,elemental compositions,and organic carbon *** with the normalization coefficients proposed in this paper,an organic matter correlation model was established to elucidate the factors that influence organic matter *** the bottom to the top of K2qn1,the lake depth gradually becomes shallower,the primary productivity first decreases and then increases,the reducing conditions become stronger and then weaker,the water salinity gradually decreases,the climate first becomes semi-humid and then warm and humid,and the input of terrigenous debris first decreases and then increases.A major marine transgression at the base of the K_(2)qn^(1)᾽s brought in nutrients to increase primary productivity,and the density-stratified reducing environment preserved and enriched organic *** primary productivity occurred during the middle of the deposition of the K_(2)qn^(1),while terrigenous input is *** matter is preserved in reduced deep lake environments,resulting in organic matter-rich black *** lake became shallower,and the salinity decreased in the upper part of K_(2)qn^(1).Benthic organisms rapidly multiplied,consuming large amounts of oxygen and destroying the previously depositional environment,resulting in a reducing environment disturbed by benthic organisms with poor preservation conditions and the lowest organic matter content.

关键词： major and trace elements paleoenvironment evolution OM enrichment mechanism lacustrine shale Songliao Basin Qingshankou Formation

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