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Nano friction behaviour between magnetic materials and copper considering the inter-diffusion effect

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Friction 2024年第7期12卷 1532-1547页

作者： Zilin LI Lisha DOU Shiyu YANG Huajiang OUYANG Qichen ZHU Xiaoyang CHEN Xin JIA Shuaiwei DOU Xiaolong CUI Yudong ZHANG Jingjiang QIU Guochen QI Bangbang NIE Pan LIU Ronghan WEI School of Mechanics and Safety engineering Zhengzhou UniversityZhengzhou 450001China engineering technology research center of henan province for mems manufacturing and application Zhengzhou UniversityZhengzhou 450001China Institute of Intelligent Sensing Zhengzhou UniversityZhengzhou 450001China School of engineering University of LiverpoolLiverpool L693GHUK School of Cyber Science and engineering&Hanwei Institute of Internet of Things Zhengzhou UniversityZhengzhou 450001China

Copper,permalloy,cobalt,and silicon are the materials that have been widely utilised in magnetic *** the size of interest is down to the nanoscale,the inter-diffusion between certain materials becomes *** paper studies the nanoscale friction characteristics between frictional pairs with and without inter-diffusion properties through the atomic force *** distinct evolution features of nanoscale friction force when inter-diffusion is involved are discovered experimentally,which is also confirmed through theoretical ***,through the thin film deposition method,four pairs of contact materials(Cu–Ni_(81)Fe_(19),Si–Ni_(81)Fe_(19),Cu–Co,Cu–Si)are designed for friction tests,in which diffusion occurs at the interface of Cu–Ni_(81)Fe_(19)***,the effects of sliding velocity and loading force on the nano friction of each pair are *** is found that regardless of the diffusion phenomenon:(1)the adhesion force values exhibit a notable correlation to the values of the friction force;(2)the friction force in all four material pairs consistently increases with the growth of the normal loading force,although the growth rate may *** terms of the sliding velocity effect,the friction forces of immiscible materials(Si–Ni_(81)Fe_(19),Cu–Co,and Cu–Si)are found to increase with the increasing sliding ***,the friction force of Cu–Ni_(81)Fe_(19),decreases with the increasing sliding ***,a compositive friction model considering both the velocity and the normal force effect was proposed,which shows good agreement with the experimental results and explains the nano friction behaviour of both miscible and immiscible metals.

关键词： atomic force microscope friction force normal load sliding velocity

High Colloidal Stable Carbon Dots Armored Liquid Metal Nano-Droplets for Versatile 3D/4D Printing Through Digital Light Processing(DLP)

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Energy & Environmental Materials 2024年第03期7卷 436-442页

作者： Linan Wang Junle Zhang Xi Zhang Ge Shi Yanjie He Zhe Cui Xiaomeng Zhang Peng Fu Minying Liu Xiaoguang Qiao Xinchang Pang henan Joint International research Laboratory of Living Polymerizations and Functional Nanomaterials Henan Key Laboratory of Advanced Nylon Materials and ApplicationSchool of Materials Science and EngineeringZhengzhou University College of Materials engineering Henan International Joint Laboratory of Rare Earth Composite MaterialsHenan Engineering Technology Research Center for Fiber Preparation and ModificationHenan University of Engineering

Liquid metal (LM) and liquid metal alloys (LMs) possess unique physicochemical features,which have become emerging and functionalized materials that are attractive applicants in various ***,uniform LM nanodroplets armored by carbon dots (LMD@CDs) were prepared and exhibited high colloidal stability in various solvents,as well as *** optimization,LMD@CDs can be applied as functional additives for the 3D/4D printing of hydrogel and cross-linked resin through digital light processing (DLP).The light absorption of LMD@CDs not only improved the printing accuracy,but also led to the cross-linking density differential during the post-curing *** on the cross-linking density differential of soft hydrogel and photothermal performance of the LM,the 3D printed objects can exhibit stimulus responses to both water and laser ***,the CDs shell and LM core of LMD@CDs provide the printed objects interesting photoluminescence and electric conductivity capabilities,*** deduce this versatile 3D/4D printing system would provide a new platform for the preparation of multi-functional and stimuli-responsive advance materials.

关键词： 4D printing carbon dots liquid metal nanodroplets

A universal calibration method for eliminating topographydependent current in conductive AFM and its application in nanoscale imaging

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Nano research 2024年第7期17卷 6509-6517页

作者： Chunlin Hao Hao Xu Shiquan Lin Yaju Zhang Jinmiao He Bei Liu Yuanzheng Zhang Banghao Wu Guozhen Shen Haiwu Zheng henan province engineering research center of Smart Micro-nano Sensing technology and application School of Physics and ElectronicsHenan UniversityKaifeng 475004China School of Integrated Circuits and Electronics Beijing Institute of TechnologyBeijing 100081China Beijing Institute of Nanoenergy and Nanosystems Chinese Academy of SciencesBeijing 100083China

The topography and electrical properties are two crucial characteristics that determine the roles and functionalities of *** atomic force microscopy(CAFM)is widely recognized for its ability to independently measure the topography and *** increasing trend towards miniaturization in electrical devices and sensors has encouraged an urgent demand for enhancing the accuracy of CAFM ***,when performing CAFM tests on Bi_(0.5)Na_(0.5)TiO_(3)bulk ceramic,it is interesting to observe significant currents related to the *** do insulators exhibit“conductivity”in CAFM testing?Herein,we thoroughly investigated the topography-dependent current during CAFM testing for the first *** on the linear dependence between the current and the first derivative of topography,the calibration method has been proposed to eliminate the topographic *** method is evaluated on Bi_(0.5)Na_(0.5)TiO_(3)bulk ceramic,one-dimensional(1D)ZnO nanowire,twodimensional(2D)NbOI_(2)flake,and biological lotus *** corresponding results of negligible topography-interference current affirm the feasibility and universality of this calibration *** work effectively addresses the challenge of topographic crosstalk in CAFM characterization,thereby preventing the erroneous estimation of the conductivity of any unknown sample.

关键词： conductive atomic force microscopy topographic crosstalk current error calibration method

Method for the fruit tree recognition and navigation in complex environment of an agricultural robot

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International Journal of Agricultural and Biological engineering 2024年第2期17卷 221-229页

作者： Xiaolin Xie Yuchao Li Lijun Zhao Xin Jin Shengsheng Wang Xiaobing Han College of Agricultural Equipment engineering Henan University of Science and TechnologyLuoyang 471003HenanChina Collaborative Innovation center of Machinery Equipment Advanced manufacturing of henan province Luoyang 471003HenanChina Longmen Laboratory Luoyang 471003HenanChina College of Intelligent and manufacturing engineering Chongqing University of Arts and SciencesChongqing 402160China

To realize the visual navigation of agricultural robots in the complex environment of orchards,this study proposed a method for fruit tree recognition and navigation based on *** YOLOv5s model was selected and trained to identify the trunks of the left and right rows of fruit trees;the quadratic curve was fitted to the bottom center of the fruit tree recognition box,and the identified fruit trees were divided into left and right columns by using the extreme value point of the quadratic curve to obtain the left and right rows of fruit trees;the straight-line equation of the left and right fruit tree rows was further solved,the median line of the two straight lines was taken as the expected navigation path of the robot,and the path tracing navigation experiment was carried out by using the improved LQR control *** experimental results show that under the guidance of the machine vision system and guided by the improved LQR control algorithm,the lateral error and heading error can converge quickly to the desired navigation path in the four initial states of[0 m,−0.34 rad],[0.10 m,0.34 rad],[0.15 m,0 rad]and[0.20 m,−0.34 rad].When the initial speed was 0.5 m/s,the average lateral error was 0.059 m and the average heading error was 0.2787 rad for the navigation trials in the four different initial *** average driving was 5.3 m into the steady state,the average value of steady state lateral error was 0.0102 m,the average value of steady state heading error was 0.0253 rad,and the average relative error of the robot driving along the desired navigation path was 4.6%.The results indicate that the navigation algorithm proposed in this study has good robustness,meets the operational requirements of robot autonomous navigation in orchard environment,and improves the reliability of robot driving in orchard.

关键词： fruit tree recognition visual navigation YOLOv5 complex environments orchards

Yeast-Controlled Double-Shelled CacO_(3)/CaF_(2)Hollow Nanospheres with Hierarchically Porous for Sustained pH-Sensitive Drug Release

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Chinese Journal of Chemistry 2024年第15期42卷 1713-1720页

作者： Xinhe Liu Yi Chang Guanglei Ma Tingting Liu Penghui Song Heng Yu Xueqing Ren Yuming Guo Xiaoming Ma School of Chemistry and Chemical engineering Henan Normal UniversityXinxiangHenan 453007China Collaborative Innovation center of henan province for Green manufacturing of Fine Chemicals Key Laboratory of Green Chemical Media and ReactionsMinistryof EducationHenan Normal UniversityXinxiangHenan 453007China

Hierarchically porous materials(HP materials)are believed one of the most hopeful matrix materials because of their distinctive multimodal pore structures and tremendous application potentials in the field of ***,green and facile synthesis of hierarchically porous nanomaterials with beneficial water dispersibility and biocompatibility is still a great ***,a novel biomimetic strategy is proposed to prepare the cell-tailored double-shelled HPCaCO_(3)/CaF_(2) hollow nanospheres under the mediation of yeast *** biomolecules derived from the secretion of yeast cells are used as conditioning and stabilizing agents to control the biosynthesis of the HPCaCO_(3)/CaF_(2) materials,which exhibit excellent water dispersibility and favorable *** double-shelled CaCO_(3)/CaF_(2) nanospheres hold hierarchically porous structure and have abundant pore channel and large specific surface area,showing high drug-loading and a prolonged drug sustainable release profile by the pore-by-pore diffusion pattern of the hierarchical ***,the HPCaCO_(3) with pH-sensitivity could controllably release drug doxorubicin hydrochloride(DOX)at the acidic tumor *** in vitro and in vivo results demonstrate that HPCaCO_(3)/CaF_(2) has the sustainable pH-sensitive drug release property,showing an enhanced therapeutic ***,this study provides a biomimetic strategy to synthesize the hierarchically porous double-shelled hollow nanomaterials for applying in sustainable drug delivery system.

关键词： Biomimetic synthesis Hierarchically porous Sustained pH-sensitive drug release Antitumor agents Drug delivery Calcium Cancer therapy/Hollow structures

Building stabilized Cu_(0.17)Mn_(0.03)V_(2)O_(5−□)·2.16H_(2)O cathode enables an outstanding room‐/low‐temperature aqueous Zn‐ion batteries

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Carbon Energy 2024年第8期6卷 25-35页

作者： Ao Wang Dai‐Huo Liu Lin Yang Fang Xu Dan Luo Haozhen Dou Mengqin Song Chunyan Xu Beinuo Zhang Jialin Zheng Zhongwei Chen Zhengyu Bai Key Laboratory of Green Chemical Media and Reactions Ministry of EducationCollaborative Innovation Center of Henan Province for Green Manufacturing of Fine ChemicalsSchool of Chemistry and Chemical EngineeringHenan Normal UniversityXinxiangHenanChina The State Key Laboratory of Catalysis(SKLC) Power Battery and System Research CenterDalian Institute of Chemical PhysicsChinese Academy of SciencesDalianChina

Vanadium oxide cathode materials with stable crystal structure and fast Zn^(2+)storage capabilities are extremely important to achieving outstanding electrochemical performance in aqueous zinc‐ion *** this work,a one‐step hydrothermal method was used to manipulate the bimetallic ion intercalation into the interlayer of vanadium *** pre‐intercalated Cu ions act as pillars to pin the vanadium oxide(V‐O)layers,establishing stabilized two‐dimensional channels for fast Zn^(2+)*** occupation of Mn ions between V‐O interlayer further expands the layer spacing and increases the concentration of oxygen defects(Od),which boosts the Zn^(2+)diffusion *** a result,as‐prepared Cu_(0.17)Mn_(0.03)V_(2)O_(5−□)·2.16H_(2)O cathode shows outstanding Zn‐storage capabilities under room‐and lowtemperature environments(e.g.,440.3 mAh g^(−1)at room temperature and 294.3 mAh g^(−1)at−60°C).Importantly,it shows a long cycling life and high capacity retention of 93.4%over 2500 cycles at 2 A g^(−1)at−60°***,the reversible intercalation chemistry mechanisms during discharging/charging processes were revealed via operando X‐ray powder diffraction and ex situ Raman *** strategy of a couple of 3d transition metal doping provides a solution for the development of superior room‐/lowtemperature vanadium‐based cathode materials.

关键词： aqueous zinc‐ion batteries Cu_(0.17)Mn_(0.03)V_(2)O_(5−□)·2.16H_(2)O oxygen defects room‐/lowtemperature performance stabilized nanostructure

Detection of the farmland plow areas using RGB-D images with an improved YOLOv5 model

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International Journal of Agricultural and Biological engineering 2024年第3期17卷 156-165页

作者： Jiangtao Ji Zhihao Han Kaixuan Zhao Qianwen Li Shucan Du College of Agricultural Equipment engineering Henan University of Science and TechnologyLuoyang 471003HenanChina Science&technology Innovation center for Completed Set Equipment Longmen LaboratoryLuoyang 471023HenanChina Collaborative Innovation center of Machinery Equipment Advanced manufacturing of henan province Luoyang 471003HenanChina School of Art and Design Henan University of Science and TechnologyLuoyang 471003HenanChina

Recognition of the boundaries of farmland plow areas has an important guiding role in the operation of intelligent agricultural *** precisely recognize these boundaries,a detection method for unmanned tractor plow areas based on RGB-Depth(RGB-D)cameras was proposed,and the feasibility of the detection method was *** method applied advanced computer vision technology to the field of agricultural *** and improving the YOLOv5-seg object segmentation algorithm,first,the Convolutional Block Attention Module(CBAM)was integrated into Concentrated-Comprehensive Convolution Block(C3)to form C3CBAM,thereby enhancing the ability of the network to extract features from plow *** GhostConv module was also utilized to reduce parameter and computational ***,using the depth image information provided by the RGB-D camera combined with the results recognized by the YOLOv5-seg model,the mask image was processed to extract contour boundaries,align the contours with the depth map,and obtain the boundary distance information of the plowed ***,based on farmland information,the calculated average boundary distance was corrected,further improving the accuracy of the distance *** experiment results showed that the YOLOv5-seg object segmentation algorithm achieved a recognition accuracy of 99%for plowed areas and that the ranging accuracy improved with decreasing detection *** ranging error at 5.5 m was approximately 0.056 m,and the average detection time per frame is 29 ms,which can meet the real-time operational *** results of this study can provide precise guarantees for the autonomous operation of unmanned plowing units.

关键词： plow areas RGB-D camera YOLO object segmentation contour boundary average distance

Online diagnosis platform for tomato seedling diseases in greenhouse production

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International Journal of Agricultural and Biological engineering 2024年第1期17卷 80-89页

作者： Xin Jin Xiaowu Zhu Jiangtao Ji Mingyong Li Xiaolin Xie Bo Zhao College of Agricultural Equipment engineering Henan University of Science and TechnologyLuoyang 471003HenanChina Science&technology Innovation center for Completed Set Equipment Longmen LaboratoryLuoyang 471023HenanChina Institute of Mechatronics technology and application China Mechanized Agriculture Science Research Institute Group Co.LtdBeijing 100020China

The facility-based production method is an important stage in the development of modern agriculture,lifting natural light and temperature restrictions and helping to improve agricultural production *** address the problems of difficulty and low accuracy in detecting pests and diseases in the dense production environment of tomato facilities,an online diagnosis platform for tomato plant diseases based on deep learning and cluster fusion was proposed by collecting images of eight major prevalent pests and diseases during the growing period of tomatoes in a facility-based *** diagnostic platform consists of three main parts:pest and disease information detection,clustering and decision-making of detection results,and platform diagnostic ***,based on the You Only Look Once(YOLO)algorithm,the key information of the disease was extracted by adding attention module(CBAM),multi-scale feature fusion was performed using weighted bi-directional feature pyramid network(BiFPN),and the overall construction was designed to be compressed and lightweight;Secondly,the k-means clustering algorithm is used to fuse with the deep learning results to output pest identification decision values to further improve the accuracy of identification applications;Finally,a detection platform was designed and developed using Python,including the front-end,back-end,and database of the system to realize online diagnosis and interaction of tomato plant pests and *** experiment shows that the algorithm detects tomato plant diseases and insect pests with mAP(mean Average Precision)of 92.7%,weights of 12.8 Megabyte(M),inference time of 33.6 *** with the current mainstream single-stage detection series algorithms,the improved algorithm model has achieved better performance;The accuracy rate of the platform diagnosis output pests and diseases information of 91.2%for images and 95.2%for *** is a great significance to tomato pest control research and t

关键词： pest and disease detection YOLO diagnosis platform k-means clustering facility production base

Optimizing 3d spin polarization of CoOOH by in situ Mo doping for efficient oxygen evolution reaction

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Carbon Energy 2024年第1期6卷 236-244页

作者： Zhichao Jia Yang Yuan Yanxing Zhang Xiang Lyu Chenhong Liu Xiaoli Yang Zhengyu Bai Haijiang Wang Lin Yang Key Laboratory of Green Chemical Media and Reactions School of Chemistry and Chemical EngineeringCollaborative Innovation Center of Henan Province for Green Manufacturing of Fine ChemicalsMinistry of EducationHenan Normal UniversityXinxiangHenanChina School of Physics Henan Normal UniversityXinxiangHenanChina Oak Ridge National Laboratory Electrification and Energy Infrastructures DivisionOak RidgeTennesseeUSA Department of Mechanical and Energy engineering Key Laboratory of Energy Conversion and Storage TechnologiesSouthern University of Science and TechnologyShenzhenGuangdongChina

Transition-metal oxyhydroxides are attractive catalysts for oxygen evolution reactions(OERs).Further studies for developing transition-metal oxyhydroxide catalysts and understanding their catalytic mechanisms will benefit their quick transition to the next ***,Mo-doped CoOOH was designed as a high-performance model electrocatalyst with durability for 20 h at 10 mAcm−***,it had an overpotential of 260 mV(glassy carbon)or 215 mV(nickel foam),which was 78 mV lower than that of IrO_(2)(338 mV).In situ,Raman spectroscopy revealed the transformation process of *** using the density functional theory showed that during OER,doped Mo increased the spin-up density of states and shrank the spin-down bandgap of the 3d orbits in the reconstructed CoOOH under the electrochemical activation process,which simultaneously optimized the adsorption and electron conduction of oxygen-related intermediates on Co sites and lowered the OER *** research provides new insights into the methodical planning of the creation of transition-metal oxyhydroxide OER catalysts.

关键词： electrocatalyst in situ Raman Mo-doped CoOOH oxygen evolution reaction