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Evolution of inclusions in vacuum induction melting of superalloys containing 70%return material

Journal of Iron and Steel Research International 2024年第3期31卷 719-728页

作者： Jin-guo Gao Shu-lei Yang Shu-feng Yang Jing-she Li Wei Liu Meng-jing Zhao An-ren Wang School of metallurgical and Ecological engineering University of Science and Technology BeijingBeijing 100083China State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China metallurgical and Building Materials Business department China International Engineering Consulting CorporationBeijing 100048China

The variation law of inclusions type and size in the vacuum induction melting process and ingot of Ni-based superalloy containing 70%return material was studied by industrial test sampling,and the mechanism of inclusions formation was analyzed with thermodynamic *** results show that there are mainly two types of composite inclusions in the vacuum induction melting of Ni-based superalloys,which are nitride-and oxide-based composite inclusions,like Al_(2)O_(3)-SiO_(2)-Cr_(2)O_(3),TiN-(Mo,Nb)C,*** type and proportion of inclusions from the center to the edge of the vacuum induction ingot did not change *** number density of inclusions from the center to the edge of the ingot varied less,and the size of inclusions became smaller from the center to the *** addition,thermodynamic calculations show that oxides(M_(2)O_(3))are present in the liquid phase and mainly contain Al,Ti,Cr,Fe and O *** nitride consists mainly of Ti and N and contains small amounts of Cr,C,Nb,and Mo *** is consistent with the results of industrial *** the temperature decreases,the precipitation phases such as M_(2)O_(3),MN,γ,MC,δ,γ'andμphases are gradually precipitated,where oxides and nitrides are present in the liquid *** contents of O and N elements are the main influencing factors for the inclusions content and precipitation temperature;when the nitrogen content is reduced to below 0.0015%,it can make MN precipitate below the liquid-phase line.

关键词： Ni-based superalloy Vacuum induction melting Return material Inclusion Thermodynamic

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Effect of austenitizing condition on mechanical properties,microstructure and precipitation behavior of AISI H13 steel

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Journal of Iron and Steel Research International 2024年第1期31卷 143-156页

作者： An-gang Ning Yang Liu Rui Gao Stephen Yue Ming-bo Wang Han-jie Guo College of Materials Science and engineering Taiyuan University of TechnologyTaiyuan030024ShanxiChina department of mining and Materials engineering McGill UniversityMontrealQCH3A 0C5Canada ASSAB Tooling Technology(Chongqing)Co. Ltd.Chongqing401120China School of metallurgical and Ecological engineering University of Science and Technology BeijingBeijing100083China

The effects of austenitizing temperature(1223,1303,and 1373 K)and holding time(1-1500 s)on the microstructure,mechanical properties,and precipitation behavior of the H13 hot work die steel were *** results indicate a softening phenomenon when H13 steel is austenitized at 1303 K beyond 900 s and 1373 K beyond 600 s,*** the sample held for 1200 s,the tensile strength is found capable of reaching up to 2.2 GPa when quenched from a temperature above 1303 ***,prior-austenite grain size increases with the increase in austenitizing *** kinetic behavior of the precipitates(mainly MC-type carbides)in H13 steel could be elaborated through the principles set forth by the Arrhenius and Avrami ***,the comprehensive strengthening of the H13 steel was discussed in *** results show that the activation energy of the transformed fraction of carbides is higher than that of the diffusion process for common alloying elements(Cr,V,Mo,and Ni)found in the *** suggests that it would be difficult for precipitates to dissolve into the matrix when H13 steel is austenitized at high *** the increasing austenitizing temperature,the precipitation fraction decreases,and the dislocation density *** dislocation strengthening is regarded as the dominant strengthening contributed to yield strength in as-quenched H13 steel.

关键词： H13 steel Austenitizing Mechanical property Precipitation behavior Comprehensive strengthening

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Residual subsidence time series model in mountain area caused by underground mining based on GNSS online monitoring

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International Journal of Coal Science & Technology 2024年第2期11卷 173-186页

作者： Xugang Lian Lifan Shi Weiyu Kong Yu Han Haodi Fan School of mining engineering Taiyuan University of TechnologyTaiyuanChina

The residual subsidence caused by underground mining in mountain area has a long subsidence duration time and great potential harm,which seriously threatens the safety of people's production and life in the mining ***,it is necessary to use appropriate monitoring methods and mathematical models to effectively monitor and predict the residual subsidence caused by underground *** with traditional level survey and InSAR(Interferometric Synthetic Aperture Radar)technology,GNSS(Global Navigation Satellite System)online monitoring technology has the advantages of long-term monitoring,high precision and more flexible monitoring *** empirical equation method of residual subsidence in mining subsidence is effectively combined with the rock creep equation,which can not only describe the residual subsidence process from the mechanism,but also predict the residual ***,based on GNSS online monitoring technology,combined with the mining subsidence model of mountain area and adding the correlation coefficient of the compaction degree of caving broken rock and the Kelvin model of rock mechanics,this paper constructs the residual subsidence time series model of arbitrary point on the ground in mountain *** the example,the predicted results of the model in the inversion parameter phase and the dynamic prediction phase are compared with the measured data *** results show that the model can carry out effective numerical calculation according to the GNSS monitoring data of any point on the ground,and the model prediction effect is good,which provides a new method for the prediction of residual subsidence in mountain mining.

关键词： Underground mining in mountain area Residual subsidence GNSS online monitoring Mathematical model Subsidence prediction

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Microstructural characterization,tribological and corrosion behavior of AA7075-TiC composites

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China Foundry 2024年第4期21卷 334-342页

作者： Surendarnath Sundaramoorthy Ramesh Gopalan Ramachandran Thulasiram department of Mechanical engineering DVR&Dr.HS MIC College of Technology(A)Vijayawada521180India department of metallurgical and Materials engineering Rajiv Gandhi University of Knowledge TechnologiesRK ValleyKadapaIndia department of Mechanical engineering Jain UniversityBangaloreIndia

Aluminum alloys are the potential materials in the automobile and aerospace sectors due to their lower density,easy forming and excellent corrosion *** demand of high strength-to-weight ratio materials in structural applications needs the engineering industries to seek aluminum alloy with new versions of hard and brittle ceramic *** microstructure,hardness,wear and corrosion behaviors of AA7075 composites with 2.5wt.%and 5wt.%TiC particles were *** analysis is evident that the transformation of the strong dendritic morphology to non-dendritic morphology on the incorporation of TiC into ***,the precipitation of the second-phase compounds such as Al_(2)CuMg,Al_(2)Cu andFe-rich Al_6(Cu,Fe)/Al_(7)Cu_(2)Fe)is promoted by TiC particles at inter-and intra-dendritic ***,the hardness of composites is improved by grain boundary strengthening and particulate strengthening *** coefficient of friction and wear rate have an inverse relation with TiC *** base alloy without TiC shows adhesive-type wear-induced deformation due to the formation of an oxide film,while composite samples exhibit a mechanically mixed layer and abrasive-type wear *** samples shows a higher corrosion rate due to the presence of numerous precipitates which promote pitting corrosion.

关键词： AA7075 alloy TiC reinforcement composite microstructure wear corrosion tribological

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Study on creep deformation and energy development of underground surrounding rock under four‐dimensional support

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Deep Underground Science and engineering 2024年第1期3卷 25-38页

作者： Zhanguo Ma Junyu Sun Peng Gong Pengfei Yan Nan Cui Ruichong Zhang School of Mechanics and Civil engineering China University of Mining and TechnologyXuzhouChina State Key Laboratory of Intelligent Construction and Healthy Operation and Maintenance of Deep Underground engineering China University of Mining and TechnologyXuzhouChina department of mining engineering Colorado School of MinesGoldenUSA

There is an urgent need to develop optimal solutions for deformation control of deep high‐stress roadways,one of the critical problems in underground *** previously proposed four‐dimensional support(hereinafter 4D support),as a new support technology,can set the roadway surrounding rock under three‐dimensional pressure in the new balanced structure,and prevent instability of surrounding rock in underground ***,the influence of roadway depth and creep deformation on the surrounding rock supported by 4D support is still *** study investigated the influence of roadway depth and creep deformation time on the instability of surrounding rock by analyzing the energy *** elastic strain energy was analyzed using the program redeveloped in *** numerical simulation results indicate that the combined support mode of 4D roof supports and conventional side supports is highly applicable to the stability control of surrounding rock with a roadway depth exceeding 520 *** the increase of roadway depth,4D support can effectively restrain the area and depth of plastic deformation in the surrounding ***,4D support limits the accumulation range and rate of elastic strain energy as the creep deformation time increases.4D support can effectively reduce the plastic deformation of roadway surrounding rock and maintain the stability for a long deformation period of 6 *** confirmed by in situ monitoring results,4D support is more effective for the long‐term stability control of surrounding rock than conventional support.

关键词： coal mines elastic strain energy four‐dimensional support large roadway depth long‐term stability control plastic deformation surrounding rock

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Quasi-static and dynamic compressive behaviour of additively manufactured Menger fractal cube structures

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Defence Technology（防务技术） 2024年第7期37卷 39-49页

作者： Damith Mohotti Dakshitha Weerasinghe Madhusha Bogahawaththa Hongxu Wang Kasun Wijesooriya Paul JHazell School of engineering and Technology UNSWCanberraACT2600Australia School of Civil Mining and Environmental EngineeringFaculty of Engineering and Information SciencesUniversity of WollongongWollongongNSWAustralia

This paper presents the first-ever investigation of Menger fractal cubes'quasi-static compression and impact *** cubes with different void ratios were 3D printed using polylactic acid(PLA)with dimensions of 40 mm×40 mm×40 *** different orders of Menger cubes with different void ratios were considered,namely M1 with a void ratio of 0.26,M2 with a void ratio of 0.45,and M3with a void ratio of ***-static Compression tests were conducted using a universal testing machine,while the drop hammer was used to observe the behaviour under impact *** fracture mechanism,energy efficiency and force-time histories were *** the structured nature of the void formation and predictability of the failure modes,the Menger geometry showed some promise compared to other alternatives,such as foams and *** the increasing void ratio,the Menger geometries show force-displacement behaviour similar to hyper-elastic materials such as rubber and *** third-order Menger cubes showed the highest energy absorption efficiency compared to the other two geometries in this *** findings of the present work reveal the possibility of using additively manufactured Menger geometries as an energy-efficient system capable of reducing the transmitting force in applications such as crash barriers.

关键词： Additive manufacturing Fractal geometries Menger cube Energy absorption Quasi-static

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Numerical modelling of post-failure behaviors of coal specimens

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Journal of Rock Mechanics and Geotechnical engineering 2024年第2期16卷 514-531页

作者： Ajeet Yadav Bhaskara Behera Gauri Shankar Prasad Singh Sanjay Kumar Sharma department of mining engineering Indian Institute of Technology(Banaras Hindu University)VaranasiUttar Pradesh221005India

A modelling approach consisting of best-fit relations to estimate the post-yield strength parameters is presented for simulating post-peak behavior beyond the point of residual strength of coal pillars having different w/h *** model was developed based on back-analysis of the complete stress-strain behavior of specimens belonging to six different Indian coal seams with different w/h ratios of 0.5 *** was found that the simultaneous degradation of the cohesion and friction angle of the Mohr-Coulomb rock material characterizes the post-peak strength behavior of the *** resulting expressions are simplistic as they require parameters that can be easily determined using uniaxial and triaxial compression ***,the developed model was validated by simulating the triaxial tests of coal specimens with different sizes under varying confining stresses and comparing its findings with the published test *** study showed that its implementation in the numerical model could reproduce laboratory-observed mechanical response,deformation behavior,and failure mechanism very closely.

关键词： Strain softening Dilatancy Interface Shape effect Residual strength

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Investigation of Adhesive Perception Based on Friction and Brain Activation

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Journal of Bionic engineering 2024年第4期21卷 1862-1877页

作者： Xingxing Fang Wei Tang Shousheng Zhang Tengfei Zhuang School of Mechatronic engineering China University of Mining and TechnologyXuzhou221116JiangsuChina

The enhancement of adhesive perception is crucial to maintaining a stable and comfortable grip of the skin-touch *** study the tactile perception of adhesive surfaces,subjective evaluation,skin friction and vibrations,and neurophysiological response of the brain activity were investigated *** materials,which are commonly used for bionic materials and skin-touch products,were chosen for the tactile *** results showed that with the increasing of surface adhesion,the dominant friction transferred from a combination of adhesive friction and deformation friction to adhesive *** friction coefficient and vibration amplitude had strong correlations with the perceived adhesion of *** parietal lobe and occipital lobe were involved in adhesive perceptions,and the area and intensity of brain activation increased with the increasing surface *** with larger adhesion tended to excite a high P300 amplitude and short latency,indicating that the judgment was faster and that more attentional resources were involved in adhesive ***,the electroencephalograph signals of the adhesive perception were simulated by the neural mass *** demonstrated that the excitability and intensity of brain activity,and the connectivity strength between two neural masses increased with the increasing surface *** study is meaningful to understand the role of surface adhesion in tactile friction and the cognitive mechanism in adhesive perception to improve the tactile experience of adhesive materials.

关键词： Surface adhesion Tactile perception Friction Brain activation Neural mass model

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Transient synthesis of carbon-supported high-entropy alloy sulfide nanoparticles via flash Joule heating for efficient electrocatalytic hydrogen evolution

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Nano Research 2024年第4期17卷 3379-3389页

作者： Yuntian Liao Rongtao Zhu Wenjun Zhang Haiyang Zhu Yang Sun Jiale Chen Zhenhua Dong Ronghuan Lv School of Chemical engineering and Technology China University of Mining and TechnologyXuzhou 221116China

High entropy alloys(HEA)are frequently employed as catalysts in electrocatalytic hydrogen ***,the traditional high entropy alloy synthesis methods are time-consuming,energy-intensive,and environmentally polluting,which limits their application in the hydrogen evolution reaction(HER).This study leveraged the capabilities of flash Joule heating(FJH)to synthesize carbon-supported high-entropy alloy sulfide nanoparticles(CC-S-HEA)on carbon cloth(CC)with good self-standing properties within 300 *** carbon thermal shock generated by the Joule heating could pyrolyze the sulfur source into gas,resulting in numerous pore structures and defects on CC,forming an S-doped carbon substrate(CC-S).Then the S atoms were used to stably anchor the metal atoms on CC-S to form high-density uniformly dispersed HEA *** electrochemical test results demonstrated that CC-S-HEA prepared at 60 V flash voltage had HER performance comparable to Pt/*** density functional theory(DFT)calculation indicated that the S atoms on CC-S accelerated the electron transfer between the carbon substrate and HEA ***,the unique electronic structure of CC-S-HEA was beneficial to H*adsorption and promoted catalytic *** simplicity and versatility of FJH synthesis are of great significance for optimizing the synthesis of HEA and improving the quality of HEA products,which provides a broad application prospect for the synthesis of nanocatalysts with efficient HER performance.

关键词： high entropy alloy flash Joule heating carbon thermal shock hydrogen evolution reaction density functional theory

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Enhanced photothermal dehydration of methanol over W_(18)O_(49)/Au/SAPO-34 catalysts with broadened light absorption

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Rare Metals 2024年第3期43卷 1139-1152页

作者： Ya-Qin Tang Meng-Xia Yan Chang-Qian Lu Shao-Yuan Li Kui-Xian Wei Tao Qu Wen-HuiMa Yong-Nian Dai Kong-Zhai Li Da-Jun Luo Xue-Liang Zhang Yi-Ke Liu Faculty of metallurgical and Energy engineering Kunming University of Science and TechnologyKunming650093China School of Materials and Energy engineering Guizhou Institute of TechnologyGuiyang550003China

Methanol-to-olefins(MTO)process is one of the most critical pathways to produce low carbon ***,the reaction is driven by thermal catalysis,which inevitably needs to consume large amounts of fossil *** a new technique to substitute for the fuel burning is urgent for MTO process to improve the industry prospects and ***,we report a novel W_(18)O_(49)/Au/SAPO-34(W/Au/S),a multifunctional photothermal catalyst for the MTO reaction.A high methanol conversion was achieved under xenonum(Xe)lamp irradiation,yielding methyl ether(ME)and ethylene as the main *** optimized W/Au/S catalysts showed ethylene yield as high as 250μmol in 60 min,which was 2.5 times higher than that of Au/*** physiochemical characterization revealed that the SAPO-34 molecular sieves were surrounded by Au and W_(18)O_(49)nanoparticles,which exhibited a strong localized surface plasmon resonance excitation around 540 nm and light absorption beyond 500 *** multifunctional catalysts showed a strong photothermal effect,arising from the broadened light absorption of Au and W_(18)O_(49)nanoparticles,leading to a temperature as high as 250℃on the surface of the *** study showed that the superior ethylene selectivity of W/Au/S catalysts was attributed to the moderating acidic sites of W_(18)O_(49)for methanol dehydration to *** research may provide new insight for designing heterostructures to improve photo-to-chemical conversion performance and is expected to accelerate progress toward the excellent multifunctional photothermal catalysts with broad light absorption for methanol activation and C-C bond formation.

关键词： Methanol conversion Ethylene Photothermal catalysis W_(18)O_(49) BrΦnsted-acid

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