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New Design of textile Vascular Prostheses for the Reconstruction of Small Diameter Vascular Blood Vessels

Journal of Donghua University(English Edition) 2013年第5期30卷 401-405页

作者： CHRZANOWSKA Olga STRUSZCZYK Marcin Henryk KRUCINSKA Izabella department of material and commodity sciences and textile metrology Center of Advanced Technologies of Human Friendly Textiles PRO HUMANO TEXFaculty of Material Technologies and Textile DesignUniversity of Technology

The general object of research is to design new idea of the semi-biodegradable,multilayered vascular prosthesis used for the reconstruction of significantly small diameter vascular vessels( microreconstruction). The paper studies the selection of appropriate sterilization technique for resorbable tubular structures made of poly( L-lactide-co-glicolide)( PLAGA) and nonbiodegradable tubular structures made of polypropylene( PP). The designed grafts are characterized by the physical properties as well as mechanical properties according to ISO 7198 ∶ 1998 ***,the process of the grafts fabrication will be explained considering the stages affected the critical properties of the elaborated textile implants. The increase of PLAGA melt-electrospun tubular structures mechanical properties was observed due to the thermal stabilization use. The ethylene oxide( EO) and steam sterilization had a destructive effect on the designed PLAGA meltelectrospun tubular, fibrous structures, whereas the irradiation yielded in the changes in mechanical and physical properties on the acceptable level,taking into account the future clinical applications.

关键词： vascular prostheses melt-electrospinning melt-blown sterilization

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Sound Absorbing Composites from Nonwoven and Cellulose Submicrofibres

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Journal of Chemistry and Chemical Engineering 2013年第10期7卷 942-948页

作者： Eulalia Gllscinska Marina Michalak Izabella Krucinska Janusz Kazimierczak Arkadiusz Bloda Danuta Ciechanska department of material and commodity sciences and textile metrology Lodz University of Technology Lodz 90-924 Poland Institute of Biopolymers and Chemical Fibres Lodz 90-570 Poland

This paper describes possibility of utilization of waste natural fibres in production of sound absorbing composites. Waste flax fibres were modified by enzymatic treatment, after which they became more short and fine. This form of fibres can create good sound absorption. Preliminary studies concerned an application of cellulose fibres after enzymatic treatment as the filling of thermoplastic sound absorbing composites. The conditions of composite manufacturing process from multilayer structure （matrix nonwoven/submicrofibres layer） were developed. The influence of submicroflbres content in the composite on the scale of the improvement of its sound absorption property was investigated. Results showed that for the same conditions of the composite manufacturing process and similar composite thickness, gradual increase in content of that filling leads to adequately increase in sound absorption coefficient of the composites. The composites could be applied among others to accommodations and transport facilities.

关键词： Sound absorption thermoplastic composite nonwoven cellulose submicrofibres

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Poriferan chitin as a template for hydrothermal zirconia deposition

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Frontiers of materials Science 2013年第3期7卷 248-260页

作者： Marcin WYSOKOWSKI Mykhaylo MOTYLENKO Vasilii V. BAZHENOV Dawid STAWSKI lroslav PETRENKO Andre EHRLICH Thomas BEHM Zoran KLJAJIC Allison L. STELLING Teofil JESIONOWSKI Hermann EHRLICH Institute of Chemical Technology and Engineering Poznan University of Technology 60965 Poznan Poland Institute of materials Science TU Bergakademie Freiberg D-09599 Freiberg Germany Institute of Experimental Physics TU Bergakademie Freiberg 09599 Freiberg Germany department of commodity and material sciences and textile metrology Technical University of Lodz 90924 Lodz Poland Institut fur Eisenund Stahltechnologie TU Bergakademie Freiberg 09599 Freiberg Germany Institute of Mineralogy TU Bergakademie Freiberg 09599 Freiberg Germany Institute of Marine Biology University of Montenegro 85330 Kotor Montenegro department of Mechanical Engineering and materials Science Duke University 27708 Durham NC USA

Chitin is a thermostable biopolymer found in various inorganic-organic skeletal structures of numerous invertebrates including sponges （Porifera）. The occurrence of chitin within calcium- and silica-based biominerals in organisms living in extreme natural conditions has inspired development of new （extreme biomimetic） synthesis route of chitin-based hybrid materials in vitro. Here, we show for the first time that 3D-a-chitin scaffolds isolated from skeletons of the marine sponge Aplysina aerophoba can be effectively mineralized under hydrothermal conditions （150℃） using ammonium zirconium（IV） carbonate as a precursor of zirconia. Obtained chitin-ZrO2 hybrid materials were characterized by FT-IR, SEM, HRTEM, as well as light and confocal laser microscopy. We suggest that formation of chitin-ZrO2 hybrids occurs due to hydrogen bonds between chitin and ZrO2.

关键词： chitin biocomposite zirconia hydrothermal synthesis ammonium zirco-nium carbonate

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Extreme biomimetic approach for developing novel chitin-GeO2 nanocomposites with photoluminescent properties

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Nano Research 2015年第7期8卷 2288-2301页

作者： Marcin Wysokowski Mykhailo Motylenko Jan Beyer Anna Makarova Hartmut Stocker Juliane Walter Roberta Galli Sabine Kaiser Denis Vyalikh Vasilii V. Bazhenov laroslav Petrenko Allison L Stelling Serguei L. Molodtsovs Dawid Stawski Krzysztof J.Kurzydfowski Enrico Langer Mikhail V Tsurkan Teofil Jesionowski Johannes Heitmann Dirk C. Meyer Hermann Ehrlich Institute of Chemical Technology and Engineering Poznan University of Technology 60965 Poznan Poland Institute of materials Science TU Bergakademie Freiberg 09599 Freiberg Germany Institute of Applied Physics TU Bergakademie Freiberg 09599 Freiberg Germany Institute of Solid State Physics Dresden University of Technology 01069 Dresden Germany Institute of Experimental Physics TU Bergakademie Freiberg 09599 Freiberg Germany Faculty of Medicine Carl Gustav Carus Department of Anaesthesiology and Intensive Care Medicine Clinical Sensoring and Monitoring TU Dresden 01069 Dresden Germany epartment of Physics St. Petersburg State University 198504 St. Petersburg Russia department of Mechanical Engineering and materials Science Duke University 27708 Durham NC USA European X-Ray Free-Electron Laser Facility (XFEL) GmbH 22761 Hamburg Germany ITMO University 197101 St. Petersburg Russia department of commodity and material sciences and textile metrology Technical University of Lodz 90924 LSdz Poland materials Design Group Faculty of Materials Science and Engineering Warsaw University of Technology PL-02507 Warsaw Poland Institute of Semiconductors and Microsystems TU Dresden 01062 Dresden Germany Leibniz Institute of Polymer Research Max Bergmann Centre for Biomaterials 01062 Dresden Germany

This work presents an extreme biomimetics route for the creation of nano- structured biocomposites utilizing a chitinous template of poriferan origin. The specific thermal stability of the nanostructured chitinous template allowed for the formation under hydrothermal conditions of a novel germanium oxide- chitin composite with a defined nanoscale structure. Using a variety of analytical techniques （FTIR, Raman, energy dispersive X-ray （EDX）, near-edge X-ray absorption fine structure （NEXAFS）, and photoluminescence （PL） spectroscopy, EDS-mapping, selected area for the electron diffraction pattern （SAEDP）, and transmission electron microscopy （TEM））, we showed that this bioorganic scaffold induces the growth of GeO2 nanocrystals with a narrow （150-300 nm） size distri- bution and predominantly hexagonal phase, demonstrating the chitin template＇s control over the crystal morphology. The formed GeO2-chitin composite showed several specific physical properties, such as a striking enhancement in photo- luminescence exceeding values previously reported in GeOR-based biomaterials. These data demonstrate the potential of extreme biomimetics for developing new-generation nanostructured materials.

关键词： extreme biomimetics, chitin-GeO2 photoluminescence, near-edge X-ray absorption fine structure (NEXAFS) spectroscopy

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