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Ag-Co3O4：Synthesis,characterization and evaluation of its photo-catalytic activity towards degradation of rhodamine B dye in aqueous medium

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Chinese Journal of Chemical Engineering 2018年第6期26卷 1264-1269页

作者： Muhammad Saeed Majid Muneer Nida Mumtaz Mohsin Siddique Nadia Akram Muhammad Hamayun department of chemisny Government College University Faisalabad Pakistan department of Chemistry Bacha Khan University Charsadda Pakistan department of Chemistry University of Gujrat Hafiz Hayat Campus Gujrat Pakistan

Synthesis,characterization of Co_3O_4 and Ag-Co_3O_4 composites and evaluation of their photo-catalytic activities towards photo-degradation of aqueous solution of rhodamine B dye under irradiation of visible light have been described in this ***_3O_4 was prepared by solid phase mechano chemical process using Co(NO_3)_2·6H_2O and NH_4 HCO_3 as precursor *** was deposited on Co_3O_4 from AgNO_3 using Calotropis gigantea extract as reducing ***,SEM and FTIR were used for characterization of prepared ***-catalytic efficiencies of as-prepared Co_3O_4 and Ag-Co_3O_4 were evaluated for aqueous phase photo-degradation of rhodamine *** was found that deposition of Ag on Co_3O_4 highly enhanced the photo-catalytic activity of Co_3O_***-catalytic degradation followed the Eley–Rideal *** 100% and 91% photo-degradation of 40 ml dye solution achieved at 313 K in 90 and 120 min over 0.05 g of Ag-Co_3O_4 as photo-catalyst using 100 and 200 mg·L^(-1) as initial concentration of dye respectively.

关键词： Co3O4 Ag-Co3O4 Photo-catalysis Photo-degradation Calotropis gigantea Rhodamine B Elay–Rideal mechanism

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SEMI-QUANTITATIVE CHARACTERIZATION OF SEGMENT DISTRIBUTION IN LLDPE BASED ON THERMAL SEGREGATION

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Chinese Journal of Polymer Science 2002年第4期20卷 347-352页

作者： Stephen Z.D.Cheng Maurice Morton Institute and department of Polymer Science University of Akron Akron Lhio 44325-3909 USA

Based on successive multiple-step isothermal crystallization and self-nucleation annealing methods, a novel semi-quantitative method for the characterization of segment distribution in linear low density polyethylene (LLDPE) was established by treating the thermal analysis data using the Gibbs-Thomson equation. The method was used to describe the segment distribution of Ziegler-Natta catalyzed LLDPE (Z-N LLDPE), metallocene catalyzed LLDPE (m-LLDPE) and two commercial LLDPEs with wide molecular weight distribution. The differences of the results obtained from the two thermally treated samples were compared. The results of segment distribution of the polymers were discussed according to their microstructure data and were compared with their characteristics. It can be deduced from the results that this characterization method is effective to characterize the sequence structure of the branched ethylene copolymers.

关键词： characterization segment distribution linear low density polyethylene thermal segregation

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