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Nano Research 2024年第5期17卷 4478-4488页

作者： Ting Yang Chengwei Wan Xiaoyu Zhang Tong Liu Li Niu Jian Fang Yuqing Liu college of textile and clothing Engineering Soochow UniversitySuzhou 215123China

Portable power is an effective solution to realize self-powered sensors for wearable devices,promoting future sustainable development.Membrane-based triboelectric nanogenerators(M-TENGs)have emerged as a promising technology for harvesting biomechanical energy from human motion owing to their advantages,such as simple structure,lightweight design,and efficient energy conversion.However,the poor durability,low adaptability,and un-washability of two-dimensional membrane materials have largely hindered their application in wearable electronics.In this study,we propose a sheath-core polyvinylidene fluoride(PVDF)/graphene(G)-carbon fiber(CF)yarn fabricated via conjugate electrospinning,comprising a commercial CF core and an electrospun graphene-doped PVDF sheath,which improves the fatigue resistance of electrospun nanofiber films under prolonged friction and keeps a high degree of freedom.The resulting electronic textile,woven with the large-scale electrospun PVDF/G-CF yarn,demonstrates a remarkable power density of 25.5 mW·m^(-2).The tight distribution of PVDF/G nanofibers on the textile surface ensures excellent softness,washability,and durability.Furthermore,the electrospun PVDF/G-CF textile exhibits significant potential in pressure sensing,self-powered operation,and motion detection,making it highly suitable for wearable electronics applications.

关键词： yarn-based triboelectric nanogenerator(TENG) graphene polyvinylidene fluoride(PVDF) conjugated-electrospinning multifunctional

Recent Progress of Bionic Hierarchical Structure in the Field of Thermal Insulation Protection

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Journal of Bionic Engineering 2024年第1期21卷 1-18页

作者： Yina Zhuge Fujuan Liu National Engineering Laboratory for Modern Silk College of Textile and Clothing EngineeringSoochow UniversitySuzhou 215123China

Some living organisms with hierarchical structures in nature have received extensive attention in various fields.The hierarchical structure with multiple pores,a large number of solid-gas interfaces and tortuous conduction paths provide a new direction for the development of thermal insulation materials,making the living creatures under these extreme conditions become the bionic objects of scientific researchers.In this review,the research progress of bionic hierarchical structure in the field of heat insulation is highlighted.Polar bears,cocoons,penguin feathers and wool are typical examples of heat preservation hierarchy in nature to introduce their morphological characteristics.At the same time,the thermal insulation mechanism,fractal model and several preparation methods of bionic hierarchical structures are emphatically discussed.The application of hierarchical structures in various fields,especially in thermal insulation and infrared thermal stealth,is summarised.Finally,the hierarchical structure is prospected.

关键词： Hierarchical structure Bionic Heat insulation Fractal model Cocoons

Optimization on magnetic properties of Nd-doped Fe_(3)O_(4) nanoparticles for magnetic shielding fabrics

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Journal of Rare Earths 2024年第4期42卷 683-689页

作者： Xiaolei Song Congzhu Xu Yuyan Wang Huizhen Ke Yonggui Li Qufu Wei Xinqun Feng Faculty of clothing and Design Minjiang UniversityFuzhou350108China Fujian Key Laboratory of Novel Functional textile Fibers and Materials Minjiang UniversityFuzhou350108China college of textile and clothing Jiangnan UniversityWuxi214122China college of Fashion and Design Donghua UniversityShanghai201620China

High magnetic protective fabrics with rare earth Nd doped Fe_(3)O_(4) nanoparticles were fabricated via a grafting method.The structure,crystal form,and elemental composition of nanoparticles were investigated by transmission electron microscopy,energy dispersive X-ray,X-ray powder diffraction,and X-ray photoelectron spectroscopy.The obtained NdFe_(2)O_(4) nanoparticles show spherical shape with fine dispersion and reasonable element composition.However,they demonstrate fine superparamagnetic properties with a magnetic saturation value of 29.25 A·m^(2)/g and low coercivity of 1.902 mT through the vibrating sample magnetometry technique,which can be well developed in magnetic shielding protective applications.Then,the cotton fabrics with plain weave were finished by a proofing rapier loom as a carrier.The NdFe_(2)O_(4) nanoparticles underwent some appropriate surface modification and then were grafted onto the cotton fabrics by a bridge agent of N,N’-dissuccinimidyl carbonate.The morphology,structure,dispersion effect,and electromagnetic protective properties of the fabrics were observed through scanning electron microscopy,Fourier infrared spectroscopy,thermogravimetric analysisdifferential scanning calorimetry(TG-DSC),and a vector network analyzer.The reliable fabrics with grafting reaction on the interface are expected to have potential applications in the field of electromagnetic protection and biomedicine fields.

关键词： Magnetic property Nd Fe_(3)O_(4)nanoparticles Magnetic shielding Fabrics Rare earths

Fabricating a smart clothing system based on strain-sensing yarn and novel stitching technology for health monitoring

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Science China(Technological Sciences) 2024年第2期67卷 587-596页

作者： TANG Jian WU YuTing MA ShiDong ZHANG YuMin XU RuoJie YAN Tao PAN ZhiJuan college of textile and clothing Engineering Soochow UniversitySuzhou 215123China National Engineering Laboratory for Modern Silk Suzhou 215123China

Various yarn-shaped flexible strain sensors have recently been developed.However,research is lacking on additive manufacturing for smart clothing for integrating yarn sensors with commercial garments.Herein,a strain-sensing yarn is sewn into a piece of fabric through a novel stitching technique,and the influence of the stitching method and needle pitch on the sensing performance is investigated using finite element analysis(FEA).The sensing performance could be improved when the sensing yarn is self-locked in the fabric at the needle eyes,and the needle pitch was reduced to 0.5 cm,which is attributed to the enhanced stress and strain concentration.Meanwhile,the composite sensing fabric featured outstanding performance,including a low detection limit(0.1%),rapid response(280 ms),excellent durability(10000 cycles),and high stability(negligible drift and frequency independence).In addition,the remarkable wear resistance,washability,and anti-interference to ambient humidity and perspiration were obtained.Therein,the optimal stitch trace lengths of sensing yarn for detecting elbow motion,breathing,and heartbeats are discussed.Finally,a smart clothing system composed of smart clothing,data acquisition unit,and mobile APP was developed to simultaneously detect human movement and physiological signals.This work provides a reference to produce intelligent garments based on yarn sensors for health monitoring.

关键词： strain-sensing yarn composite sensing fabric smart clothing system stitching technology health monitoring

Preliminary Biocompatibility Evaluation of Regenerated Antheraea yamamai Silk Fibroin in vitro

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Journal of Wuhan University of Technology(Materials Science) 2011年第6期26卷 1044-1048页

作者：王建南 National Engineering Laboratory for Modern Silk College of Textile and Clothing EngineeringSoochow University

The study aimed to investigate the adhesion, morphology and proliferation of Sprague Dawley （SD） albino rat bone marrow-derived mesenchymal stem cells （BMSCs） by inverted microscope, cell counting, MTT test and laser scanning confocal microscop （LSCM）. On the regenerated A yamamai SF film or blend films, the cell morphology was almost the same as that on collagen （collagen type I） film, the cell adhesion rate was higher than that on plastic cell plate and B mori SF film after 1 h （p 〈 0.01） of culture, and the cell proliferation was significantly higher than that on collagen film （p 〈 0.01） and plastic cell plate （p 〈 0.01）, and also obviously better than that on B mori SF film. On the other hand, the viability of BMSCs in the regenerated A yamamai SF porous scaffold was better than that in B mori SF porous scaffold and medical grade polyvinyl alcohol （PVA） sponge.

关键词： A yamamai SF BMSC adhesion proliferation cell probe LSCM

Bioactivity of silk fibroin peptides on vascular endothelial cells

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Frontiers of Materials Science 2024年第1期18卷 85-94页

作者： Mengnan Dai Meng Li Peixuan Li Boyu Zhang Jianmei Xu Jiannan Wang National Engineering Laboratory for Modern Silk College of Textile and Clothing EngineeringSoochow UniversityNo.199 Ren-ai RoadSuzhou Industrial ParkSuzhou 215123China

To determine the contribution of non-repetitive domains to the bioactivity of the heavy chain in silk fibroin(SF)macromolecules,a gene motif f(1)encoding this fragment and its multimers(f(4)and f(8))were biosynthesized from Escherichia coli BL21.Based on the positive application potential of SF materials for the vascular tissue engineering,this study focused on examining the active response of these polypeptides to vascular endothelial cells.Biosynthetic polypeptides F(1),F(4),and F(8)were separately grafted onto the surfaces of bioinert polyethylene terephthalate(PET)films,resulting in remarkable improvements in the spread and proliferation of human umbilical vein endothelial cells(HUVECs).Using the same grafting dose,the activity of cells on polypeptide-modified PET films enhanced with the increase of the molecular weight of those grafted polypeptides from F(1)to F(8).Meanwhile,the growth of cells on the surface of the alkaline-treated PET film was improved,indicating that the hydrophilicity of the surface material had influence on the growth of HUVECs.Moreover,on surfaces with the same water contact angle,the spread and proliferation activity of cells on PET films were significantly lower than those on polypeptide-modified PET films.

关键词： silk fibroin heavy chain non-repetitive fragment cytoactive endothelial cell

Gelation behavior of Antheraea pernyi silk fibroin

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Science China Chemistry 2010年第3期53卷 535-541页

作者： YAN ShuQin,ZHAO ChunXia,WU XiuFang,ZHANG Qiang & LI MingZhong National Engineering Laboratory for Modern Silk college of textile and clothing Engineering,Soochow University,Suzhou 215123,China National Engineering Laboratory for Modern Silk college of textile and clothing Engineering Soochow University Suzhou China

The sol-gel transition behavior of Antherae pernyi silk fibroin(Ap-SF) has not been systematically investigated.In this work,the influence of environmental temperature,pH,the concentration of Ap-SF,K+ and Ca2+ on the gelation time,and the structural changes of Ap-SF in sol-gel transformation were studied.The results indicated that the gelation time of the Ap-SF aqueous solution decreased with the increase of the Ap-SF concentration and environmental temperature.The sol-gel transformation of Ap-SF was much more rapid than that of Bombyx mori silk fibroin under the same conditions.The Ap-SF was sensitive to changes in the concentration of Ca2+ and K+.Upon gelation,the random coil structure of the Ap-SF was significantly transformed into the β-sheet structure.

关键词： Antheraea pernyi silk fibroin gelation sol-gel transition

Woven fabric triboelectric nanogenerators for human-computer interaction and physical health monitoring

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Nano Research 2024年第6期17卷 5540-5548页

作者： Yu Miao Mengjuan Zhou Jia Yi Yanyan Wang Guangjin Tian Hongxia Zhang Wenlong Huang Wenhao Wang Ronghui Wu Liyun Ma college of textile and clothing Xinjiang UniversityUrumqi 830046China college of textiles Donghua UniversityShanghai 201620China college of Physics Xiamen UniversityXiamen 201620China Department of Bioengineering Imperial College LondonLondon SW72AZUK

Triboelectric nanogenerator(TENG)converts mechanical energy into valuable electrical energy,offering a solution for future energy needs.As an indispensable part of TENG,textile TENG(T-TENG)has incredible advantages in harvesting biomechanical energy and physiological signal monitoring.However,the application of T-TENG is restricted,partly because the fabric structure parameter and structure on T-TENG performance have not been fully exploited.This study comprehensively investigates the effect of weaving structure on fabric TENGs(F-TENGs)for direct-weaving yarn TENGs and post-coating fabric TENGs.For direct-weaving F-TENGs,a single-yarn TENG(Y-TENG)with a core-sheath structure is fabricated using conductive yarn as the core layer yarn and polytetrafluoroethylene(PTFE)filaments as the sheath yarn.Twelve fabrics with five different sets of parameters were designed and investigated.For post-coating F-TENGs,fabrics with weaving structures of plain,twill,satin,and reinforced twill were fabricated and coated with conductive silver paint.Overall,the twill F-TENGs have the best electrical outputs,followed by the satin F-TENGs and plain weave F-TENGs.Besides,the increase of the Y-TENG gap spacing was demonstrated to improve the electrical output performance.Moreover,T-TENGs are demonstrated for human-computer interaction and self-powered real-time monitoring.This systematic work provides guidance for the future T-TENG’s design.

关键词： single-yarn triboelectric nanogenerators woven fabric triboelectric nanogenerators fabric weaving structures and parameters human-computer interaction physical health monitoring

A scalable versatile methodology to construct micro/nano open-cell polypropylene foam with high oil adsorption capacity and speed

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Nano Research 2024年第4期17卷 2814-2823页

作者： Chenguang Yang Dechang Tao Kun Yan Zhiyao Li Qingshi Guo Wenwen Wang Dong Wang Key Laboratory of textile Fiber and Products(Wuhan textile University) Ministry of EducationWuhan Textile UniversityWuhan 430200China college of Chemistry Chemical Engineering and BiotechnologyDonghua UniversityShanghai 201620China

Oil pollution is a serious environmental and natural resource problem.Traditional adsorption materials for oil–water separation have limitations in terms of their preparation cost,reusability,and mechanical properties.Among the conventional adsorption materials,super-hydrophobic/super-lipophilic materials are easily contaminated by oil.In this study,polypropylene(PP)is used as a foam substrate to prepare an open-cell PP foam via hot pressing,supercritical CO_(2) foaming,and electron beam(EB)irradiation.The impact of EB irradiation dose on the open-cell content of PP foam can lead to cell wall rupture,resulting in an open-cell structure that enhances oil-water separation performance.At an absorbed radiation dose of 200 kGy,the PP foams exhibit optimal oil–water separation performance,cyclic compression stability,heat insulation,and preparation cost.The open-cell content of PP foam is increased to 86.5%,the adsorption capacity for diesel oil is 42.8 g/g,and the adsorption efficiency remains at 99.6%after 100 cycles of oil desorption in a complex pH environment.Meanwhile,cracks and nano-voids simultaneously promote the capillary action of oil,and the oil transport rate is 0.0713 g/(g·s).This study provides a new concept for the preparation of open-cell polymer foams that can meet the demand for high oil-absorption capacity under complex acid-base pH conditions.

关键词： open-cell polypropylene(PP)foam electron beam irradiation oil/water separation cyclic compression complex acid-base pH conditions

用于高风险环境安全监测和可调热管理的具有分层核壳结构的耐化学品纱线

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Engineering 2024年第1期32卷 217-225页

作者： Duo Xu Yingcun Liu Can Ge Chong Gao Ze Chen Ziyi Su Haoran Gong Weilin Xu Jian Fang college of textile and clothing Engineering Soochow UniversitySuzhou 215123China State Key Laboratory of New textile Materials and Advanced Processing Technologies Wuhan Textile UniversityWuhan 430200China

Chemical resistant textiles are vital for safeguarding humans against chemical hazards in various settings.such as industrialproduction,chemicalaccidents,laboratory activities,and road transportation.However,the ideal integration of chemical resistance,thermal and moisture management,and wearer condition monitoring in conventional chemically protective textiles remains challenging.Herein,the design,manufacturing,and use of stretchable hierarchical core-shell yarns(HCSYs)for integrated chemical resistance,moisture regulation,and smart sensing textiles are demonstrated.These yarns con-tain helically elastic spandex,wrapped silver-plated nylon,and surface-structuredpolytetrafluo-roethylene(PTFE)yarns and are designed and manufactured based on a scalable fabrication process.In addition to their ideal chemical resistance performance,HCSYs can function as multifunctional stretch-able electronics for real-time human motion monitoring and as the basic element of intelligent textiles.Furthermore,a desirable dynamic thermoregulation function is achieved by exploiting the fabric structure with stretching modulation.Our HCSYs may provide prospective opportunities for the future development of smart protective textiles with high durability,flexibility,and scalability.

关键词： Hierarchical core-shell structure Chemical resistant yam Wearable strain sensor Thermoregulation