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Anchoring eccentricity features and rectifying devices for resin grouted bolt/cable bolt

International Journal of Mining Science and Technology 2022年第5期32卷 1059-1073页

作者： Shaowei Liu Deyin He Housheng Jia Mengxiong Fu Biao Hou School of Energy Science and Engineering Henan Polytechnic UniversityJiaozuo 454000China State collaborative innovation center of coal work safety and clean-efficiency utilization Jiaozuo 454000China

The anchoring eccentricity of the bolt and cable bolt is a common problem in geotechnical support engineering and affects the ability of the bolt and cable bolt to control the rock mass to a certain extent.This paper reports on numerical simulation and laboratory experiments conducted to clarify the effect of eccentricity on the anchoring quality of the bolt and cable bolt,and to establish an effective solution strategy.The results reveal that the anchoring eccentricity causes unbalanced stress distribution and the uncoordinated deformation of the resin layer,which results in higher stress and greater deformation of the resin layer at the near side of the rod body.Additionally,as the degree of anchoring eccentricity increases,the effect becomes more significant,and the resin layer of the anchoring system becomes more likely to undergo preferential failure locally,which weakens the load-bearing performance of the anchoring system.This paper develops an innovative bolt anchoring rectifying device(B-ARD)and cable bolt anchoring rectifying device(C-ARD)on the basis of the structural characteristics of the bolt and cable bolt to better ensure the anchoring effect of them.The working effects of these two devices were verified in detailed experiments and analysis.The experimental results show that the anchoring rectifying devices(ARD)improve and ensure the anchoring concentricity of the bolt and cable bolt,which will help improve the supporting performance of them.The paper provides a convenient and effective method for improving the anchoring concentricity of the bolt and cable bolt,and provides a concept and reference for technical research on improving the effect of roof bolting.

关键词： Anchoring eccentricity features Rectifying device Roof bolting Anchoring system performance

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Construction of hierarchical In_(2)O_(3)/In_(2)S_(3) microsphere heterostructures for TEA detection

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Journal of Materiomics 2022年第6期8卷 1113-1121页

作者： Yongjie Zhang Cong Qin Run Zhang Yan Zhang Yan Wang Zhanying Zhang Jianliang Cao College of Chemistry and Chemical Engineering Henan Polytechnic UniversityJiaozuo454000China State collaborative innovation center of coal work safety and clean-efficiency utilization Henan Polytechnic UniversityJiaozuo454000China

Construction of heterojunction has been considered as an efficient strategy to enhance the gas-sensing performances of metal oxide semiconductors.On this basis,hierarchical In_(2)O_(3)/In_(2)S_(3) microsphere heterostructures were synthesized by partial oxidation of In_(2)S_(3) precursors which were obtained via a facile hydrothermal method.Besides,gas sensors based on the acquired materials were fabricated to investigate their sensing performances toward triethylamine(TEA).The results reveal that the gas sensor based on In_(2)O_(3)/In_(2)S_(3) exhibits a high response of 37 at 300℃ toward 0.45 mg/L TEA,which is 3.7 times higher than that of bare In_(2)O_(3).Meanwhile,it also possesses fast response/recovery time(19 s/154 s),good repeatability,selectivity and long-term stability.The excellent sensing performances toward TEA are mainly attributed to the massive oxygen vacancy defects and heterojunction formed between In_(2)O_(3) and In_(2)S_(3).This work provides a facile temperature-dependent route to controllably synthesize hierarchical In_(2)O_(3)/In_(2)S_(3) microsphere heterostructures,and the In_(2)O_(3)/In_(2)S_(3) sensor shows great application prospects in TEA detection.

关键词： In_(2)O_(3)/In_(2)S_(3) Heterojunction Hierarchical structure Triethylamine Gas sensor

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Design and synthesis of two dimensional-ZnIn2S4 nanosheets with sulfur vacancies for improving photocatalytic hydrogen production performance

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Progress in Natural Science:Materials International 2023年第5期33卷 607-615页

作者： Jianguo He Guanghui Zhang Yichen Jiang Jianfa Jia Jianliang Cao College of Chemistry and Chemical Engineering Henan Polytechnic University State collaborative innovation center of coal work safety and clean-efficiency utilization Henan Polytechnic University

The remarkable properties exhibited by two-dimensional(2D) photocatalytic materials,differing from bulk materials,have captivated significant interest.In this study,a hexagonal-phase ZnIn2S4were synthesized using thiosulfate,thioacetamide,and L-cysteine as sulfur sources(denoted as ZIS-A,ZIS-B and ZIS-C),respectively.The synthesized ZnIn2S4 exhibited varying morphologies and photocatalytic properties,which were characterized through XRD,SEM,TEM,EPR,XPS and so on.The results confirmed that ZIS-B with 2D nanosheets structures exhibited superior photocatalytic properties compared with that of the flower-like spheres and block ZnIn2S4samples.The hydrogen evolution rate of the ZIS-B is 3653 μmol g-1h-1,which is 3.1 times than that of the other samples.This improvement was attributable to that the ZIS-B have 2D nanosheets structures and sulfur vacancies.Notably,the 2D nanosheets structure endowed ZnIn2S4with a larger surface area and abundant reactive sites for efficient evolution reaction.Additionally,the presence of sulfur vacancies served as active sites,facilitating carrier transport and ultimately promoting the rate of photocatalytic hydrogen evolution.These results present a novel method for optimizing 2D ZnIn2S4photocatalyst to improve the photocatalytic hydrogen evolution.

关键词： Nanosheets Photocatalytic hydrogen production Sulfur vacancies ZnIn2S4

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Synthesis and characterization of a novel collector for the desulfurization of fine high-sulfur bauxite via reverse flotation

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Particuology 2023年第8期79卷 64-77页

作者： Gan Cheng Jianqiang Zhang Huanhuan Su Zhanyun Zhang Zhengzhou Non-ferrous Metals Research Institute Co.Ltd. Aluminum Corporation of ChinaZhengzhou450041China College of Chemistry and Chemical Engineering Henan Polytechnic UniversityJiaozuo454000China Collaborative Innovation Center of Coal Work Safety and Clean High Efficiency Utilization Henan Polytechnic UniversityJiaozuo454000China

Bauxite is one of the main raw materials in the alumina industry.Fine high-sulfur bauxite flotation desulfurization is a great challenge presently.This study aims to synthesize nanoparticle collectors(NPCs)by emulsion polymerization to improve the abovesaid flotation desulfurization process.The physicochemical properties of high-sulfur bauxite were analyzed,and the experimental conditions for the synthesis of NPCs were optimized.The interaction mechanism between NPCs and pyrite was studied via fundamental analyses including SEM(Scanning Electron Microscope),FT-IR(Fourier Transform Infrared spectoscopy),Zeta-potential,XPS(X-ray Photoelectron Spectroscopy),and wettability.Under the closed-circuit flotation flowsheet of"one roughing-two cleaning-three scavenging",aluminum concen-trate with a yield of 85.91%and sulfur content of 0.56%were obtained using a common collector.However,with the addition of the novel NPC,aluminum concentrate with a yield of 85.70%and sulfur content of 0.36%could be obtained by a simpler flowsheet of"one roughing-one cleaning-two scav-enging".The improvement in flotation performance is suggested to be contributed by the addition of spherical NPC,which induced a rougher and more hydrophobic pyrite surface.

关键词： Bauxite Flotation desulfurization Nanoparticle collector Pyrite

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Graphene-like h-BN supported polyhedral NiS_(2)/NiS nanocrystals with excellent photocatalytic performance for removing rhodamine B and Cr(Ⅵ)

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Frontiers of Chemical Science and Engineering 2021年第6期15卷 1537-1549页

作者： Wei Wang Linlin Song Huoli Zhang Guanghui Zhang Jianliang Cao College of Chemistry and Chemical Engineering Henan Key Laboratory of Coal Green ConversionHenan Polytechnic UniversityJiaozuo454000China State collaborative innovation center of coal work safety and clean-efficiency utilization Henan Polytechnic UniversityJiaozuo454000China

Human health is deteriorating due to the effluent containing heavy metal ions and organic dyes.Hence,photoreduction of Cr(Ⅵ)to Cr(Ⅲ)and degradation of rhodamine B(RhB)using a novel photocatalyst is particularly important.In this work,h-BN/NiS_(2)/NiS composites were prepared via a simple solvothermal method and a double Z-scheme heterojunction was constructed for efficiently removing RhB and Cr(Ⅵ).The 7 wt-%h-BN/NiS_(2)/NiS composites were characterized via a larger specific surface area(15.12 m^(2)·g^(−1)),stronger light absorption capacity,excellent chemical stability,and high yield of electrons and holes.The experimental result indicated that the photoreduction efficiency of the 7 wt-%h-BN/NiS_(2)/NiS photocatalyst achieved 98.5%for Cr(Ⅵ)after 120 min,which was about 3 times higher than that of NiS_(2)/NiS(34%).However,the removal rate of RhB by the 7 wt-%h-BN/NiS_(2)/NiS photocatalyst reached 80%.This is due to the double Z-scheme heterojunction formed between NiS_(2)/NiS and h-BN,which improved the charge separation efficiency and transmission efficiency.Besides,the influence of diverse photogenerated electron and hole scavengers upon the photoreduction of Cr(Ⅵ)was studied,the results indicated that graphene-like h-BN promoted transportation of photoinduced charges on the surface of the h-BN/NiS_(2)/NiS photocatalyst via the interfacial effects.

关键词： graphene-like h-BN h-BN/NiS_(2)/NiS composites photocatalysis Cr(Ⅵ)reduction degradation of RhB

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Lateral abutment pressure distribution and evolution in wide pillars under the first mining effect

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International Journal of Mining Science and Technology 2023年第3期33卷 309-322页

作者： Zhen Zhang Zhen Li Gang Xu Xiaojin Gao Qianjin Liu Zhengjie Li Jiachen Liu coal Mining and Designing Branch China Coal Research InstituteBeijing 100013China CCTEG coal Mining Research Institute Beijing 100013China coal Mining&Designing Department Tiandi Science&Technology Co.Ltd.Beijing 100013China School of Civil Engineering Henan Polytechnic UniversityJiaozuo 454003China Collaborative Innovation Center of Coal Work Safety and Clean High Efficiency Utilization Jiaozuo 454003China

The wide pillars are generally popular due to the high productivity and efficiency in Northwest China.The distribution of lateral abutment pressure in coal pillars is important for mining safety.To reveal the effect of the first mining on the lateral abutment pressure distribution and evolution in wide pillars,an in-situ experiment,theoretical analysis and numerical simulation were performed.First,the field monitoring of lateral abutment pressure was conducted from the perspective of time and space in the Chahasu coal Mine,Huangling No.2 coal Mine and Lingdong coal Mine during the first mining.Based on the field monitoring stress,a theoretical model was proposed to reveal the lateral abutment pressure distribution.The methodology was demonstrated through a case study.Aiming at the distribution mechanism,a numerical experiment was conducted through the finite-discrete element method(FDEM).Last,field observations of borehole fractures were performed to further study the damage distribution.In addition,two types of lateral abutment pressure evolution with mining advance were discussed.Suggestions on the stress monitoring layout were proposed as well.The results could provide foundations for strata control and disaster prevention in wide pillars in underground coal mines.

关键词： Wide pillar Lateral abutment pressure Pillar stress First mining effect Field monitoring

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Mechanical properties and damage characteristics of solidified body-coal combination in continuous driving and gangue backfilling

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International Journal of Mining Science and Technology 2023年第10期33卷 1217-1228页

作者： Yi Tan Hao Cheng Wenbing Guo Erhu Bai Shaopu Zhang Yu Wang Zihao Li School of Energy Science and Engineering Henan Polytechnic UniversityJiaozuo 454000China State collaborative innovation center of coal work safety and clean-efficiency utilization Henan Polytechnic UniversityJiaozuo 454000China

Recovery of the coal buried under buildings,railways and water bodies and the residual coal in irregularly arranged fully mechanized mining faces is a common engineering problem facing underground coal mining.In this study,a mining technology of continuous driving and gangue backfilling(CDGB)was proposed.The technology,which can not only alleviate ground subsidence and gangue discharge,but also release the above-mentioned coals,contributes to green and efficient sustainable development of mining.The stability of the system of the solidified body-reserved coal pillar combination(S-C combination)is crucial to the CDGB technology.Therefore,it is of great significance to explore the mechanical and damage characteristics of S-C combination in the synergistic bearing process.First,four sets of differentshaped S-C combination specimens were fabricated and a S-C combination bearing structure in CDGB was constructed to explore the differences in mechanical characteristics and damage modes of different-shaped S-C combination specimens during CDGB.Subsequently,their surface strain field evolutions and acoustic emission(AE)response characteristics in the load-bearing process were obtained with the aid of the digital image correlation technique and the AE signal monitoring system.Furthermore,a damage evolution model based on AE parameters and mechanical parameters was established to clarify the damage evolution law.The following results were obtained:(1)The free area of S-C combination can serve as a quantitative index to evaluate the stability of the overburden control system;(2)The concept of critical value k of the free area was first proposed.When the free area exceeds the critical value k(free area ratio greater than 1.13),the deformation resistance and the free area changes becomes negatively correlated;(3)As the free area expands,the failure of the S-C combination specimen evolves from tensile failure to shear failure.The distribution characteristics of the axial strain field also verified such a change in the failure

关键词： Continuous driving and gangue backfilling Solidified body-coal combination Mechanical properties Damage characteristics Digital image correlation technology Acoustic emission

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A novel method for the green utilization of waste fried oil

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Particuology 2024年第1期84卷 1-11页

作者： Gan Cheng Mengni Zhang Yang Lu Yanhui Zhang Bin Lin Ee Von Lau College of Chemistry and Chemical Engineering Henan Polytechnic UniversityJiaozuo454003China Henan Key Laboratory for Green and Efficient Mining&Comprehensive utilization of Mineral Resources Henan Polytechnic UniversityJiaozuo454003China Collaborative Innovation Center of Coal Work Safety and Clean High Efficiency Utilization Henan Polytechnic UniversityJiaozuo454003China School of Engineering Monash University MalaysiaSubang JayaSelangor47500Malaysia

Waste fried oil was studied to prepare three different types of detergent such as soap,liquid soap and soap powder via saponification process.The preparation conditions of soap base were optimized by orthogonal experiment.The specific preparation processes included waste fried oil treatment,orange peel extract preparation,saponification,demoulding and drying.Results showed that the optimal con-ditions for saponification were as follows:ratio of pure waste fried oil to coconut oil=6∶4,alkali liquor(NaOH)mass fraction 30%,saponification temperature 70℃,orange peel extract concentration 15%.The mature soap was then used to make liquid soap and soap powder by surfactant(sodium dodecylbenzene sulfonate,coconut diethanol amide)addition,followed by grinding.The prepared detergent conforms to the production standard of strong decontamination ability,possesses stable performance,is gentle to skin and non-toxic.

关键词： Waste fried oil Detergent Saponification Decolorization

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Motion characteristics and density separation of fine coal in an inflatable-inclined liquid-solid fluidized bed

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Particuology 2021年第5期19卷 299-307页

作者： Bo Lv Bobing Dong Xiaowei Deng Chaojun Fang College of Chemistry and Chemical Engineering Henan Polytechnic UniversityJiaozuo 454000China Henan Key Laboratory for Green and Efficient Mining&Comprehensive utilization of Mineral Resources Henan Polytechnic UniversityJiaozuo 454000China Collaborative Innovation Center of Coal Work Safety and Clean High Efficiency Utilization Henan Polytechnic UniversityJiaozuo 454000China

To improve the adaptability of fluidized beds for fine coal separation,a new type of liquid-solid fluidized bed was constructed,i.e.,the inflatable-inclined liquid-solid fluidized bed(IILSFB).A combination of simulation analysis and separation experiments was used to analyze the fluidization characteristics and separation performance of the IILSFB.The results showed that there was upflow and downflow in the fluidized bed.The upflow was mainly composed of water flow,followed by light and heavy particles;on the other hand,the downflow was caused by the backflow of heavy particles that settled at the inclined section.In addition,the light particles that settled at the inclined section could return to the rising water flow under the action of secondary airflow.As the water velocity,separation time,and secondary gas velocity increased,the comprehensive separation efficiency of fine coal in the fluidized bed improved,while the value decreased as the feed quantity increased.This also indicated the order of importance for these four factors,i.e.,water velocity,separation time,feed quantity,and secondary gas velocity,on fluidisation.Furthermore,the comprehensive separation efficiency of 0.1-1 mm fine coal varied significantly with various factors,while that of∼0.1 mm and 1-3 mm fine coal was always at a low value.In the latter case,the classification process of the size fraction was significantly better than the separation process in the fluidized bed.Under optimal working conditions,an IILSFB was used to separate the fine coal(0.1-1 mm).The yield of clean coal was 37.95% with an ash content of 12.11%,and the possible error was 0.085 g/cm^(3),indicating that the IILSFB had good separation performance for 0.1-1 mm fine coal.

关键词： Inflatable-inclined liquid-solid fluidized bed Fine coal separation Fluidization Separation efficiency Secondary gas velocity Size fraction

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Tomography of the dynamic stress coefficient for stress wave prediction in sedimentary rock layer under the mining additional stress

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International Journal of Mining Science and Technology 2021年第4期31卷 653-663页

作者： Wenlong Shen Guocang Shi Yungang Wang Jianbiao Bai Ruifeng Zhang Xiangyu Wang Henan Key Laboratory for Green and Efficient Mining&Comprehensive utilization of Mineral Resources School of Energy Science and EngineeringHenan Polytechnic UniversityJiaozuo 454000China Key Laboratory of Deep coal Resource Mining Ministry of Education State Key Laboratory of Coal Resources and Safe MiningChina University of Mining and TechnologyXuzhou 221116China Collaborative Innovation Center of Coal Work Safety and Clean High Efficiency Utilization Jiaozuo 454000China

In this study,the tomography of dynamic stress coefficient(TDSC)was established based on a mechanical model of stress wave propagation in bedding planes and a mathematical model of the stress wave attenuation in rock masses.The reliability of the TDSC was verified by a linear bedding plane model and field monitoring.Generally,the TDSC in the dynamic stress propagation of bedding planes increases with the following conditions:(1)the increase of the normal stiffness of the bedding plane,(2)the increase of the incident angle of the stress wave,(3)the decrease of the incident frequency of the stress wave,or(4)the growth of three ratios(the ratios of rock densities,elastic moduli,and the Poisson’s ratios)of rocks on either side of bedding planes.The additional stress weakens TDSC linearly and slowly during the stress wave propagation in bedding planes,and the weakening effect increases with the growth of the three ratios.Besides,the TDSC decreases exponentially in the rock mass as propagation distance increases.In a field case,the TDSC decreases significantly as vertical and horizontal distances increase and its wave range increases as vertical distance increases in the sedimentary rock layers.

关键词： Tomography of the dynamic stress coefficient Stress wave attenuation Mining additional stress Sedimentary rock layer

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