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Microstructure and mechanical behavior of similar butt-joints of ZK60 and ZK60-1.5RE magnesium alloys produced by linear friction stir welding

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Journal of Magnesium and alloys 2021年第5期9卷 1802-1817页

作者： Erenilton Pereira da Silva Ricardo Henrique Buzolin Ulises Alfaro Guillermo Requena Haroldo Calvalcanti Pinto Institute of Engineering Science and Technology(IECT)Federal University of Vales do Jequitinhonha e Mucuri(UFVJM)JanaúbaMGBrazil Department of Materials Engineering São Carlos School of Engineering(EESC)University of São Paulo(USP)São Carlos-SP CEP 13563-120Brazil christian doppler laboratory for design of high-performance alloys by thermomechanical processing Kopernikusgasse 24Graz 8010Austria Institute of Materials Science Joining and Forming at Graz University of Technology opernikusgasse 24/IGraz 8010Austria German Aerospace Center(DLR)Institute of Materials Research Linder HöheCologne 51147Germany RWTH Aachen University Metallic Structures and Materials Systems for Aerospace EngineeringD-52062 AachenGermany.

The microstructure and mechanical properties of butt-joints produced by linear friction stir welding of similar plates of as-cast ZK60 and modified ZK60 with 1.5 wt.%RE(ZK60-1.5 RE)are *** thermomechanical affected zone is investigated in both advancing and retrieving sides,and the microstructure is compared to the base metal and the stirred *** backscattered diffraction measurements provide the average microstructural features of the transformed *** mechanical properties are assessed using hardness,tensile testing,and surface residual stress measured using X-ray *** torque and heat input are obtained for the ZK60-1.5 RE compared to the *** thermomechanical affected zone is notably larger for the ZK60 compared to the ZK60-1.5 RE.A gradient microstructure is formed in thermomechanical affected zones where deformed grains are progressively more recrystallised towards the stirred *** is no visible interface between the thermomechanical affected zone and the stirred zone.A fine and partially recrystallised microstructure is formed in the stirred *** retrieving side of the ZK60-1.5 RE has a slightly more refined microstructure compared to the other investigated *** measured with increment in the maximum intensity of the(0001)increases towards to stirred *** formed microstructure is correlated with the role of twinning,recovery,static,and dynamic recrystallisation that can occur during friction stir *** and grains with large misorientation spread are more pronounced in the thermomechanical affected zone and regions towards the base *** low angle grain boundaries are observed towards the stirred *** refined recrystallised grains decorating the grain in the thermomechanical affected zone,a mosaic-like of low and high angle grain boundaries are observed in the stirred *** joints have comparable surface residual *** friction stir welding improved th

关键词： ZK60 Mischmetal FSW Recrystallization Microstructure thermomechanical

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Effect of Ce-base mischmetal addition on the microstructure and mechanical properties of hot-rolled ZK60 alloy

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Journal of Magnesium and alloys 2021年第3期9卷 995-1006页

作者： E.P.Silva R.H.Buzolin F.Marques F.Soldera U.Alfaro H.C.Pinto Institute of Engineering Science and Technology(IECT)Federal University of Vales do Jequitinhonha e Mucuri(UFVJM)JanaúbaMGBrazil São Carlos School of Engineering(EESC) University of São Paulo(USP)Department of Materials EngineeringCEP 13563-120 São Carlos-SPBrazil christian doppler laboratory for design of high-performance alloys by thermomechanical processing Kopernikusgasse 24/I8010 GrazAustria Technische Universität Graz(TU Graz) Institute of Materials ScienceJoining and FormingKopernikusgasse 24/I8010 GrazAustria Institute of Functional Materials Department of Materials Science and EngineeringSaarland UniversitySaarbrueckenGermany German Aerospace Center(DLR)Institute of Materials Research Linder Höhe51147 CologneGermany

Mg-Zn-Zr(ZK)alloys exhibit notably high mechanical strength amongst all magnesium alloy ***,due to the formation of low melting point Mg_3Zn_7-precipitates,these alloys are susceptible to hot cracking,thus compromising their metallurgical *** addition of rare earths to ZK alloys is an alternative to form higher melting point intermetallic compounds,speed up dynamic recrystallization,refine grain size,enhance corrosion resistance and extend the service temperature due to improved creep *** work deals with the effect of Ce-base mischmetal addition on the hot rolling behaviour of as-cast ZK60 *** microstructure investigation conducted using electron microscopy and X-Ray diffraction shows that precipitation of Mg_(7)Zn_(3) intermetallics occur during hot rolling,whereas no further precipitation is observed for the ZK60-Mm *** fragmentation of the intermetallic compounds occur during hot rolling and finer particles of Mg_(7)Zn_(3) are observed for the ZK60,whereas Mg_(7)Zn_(3) and Mg Zn_(2) Ce intermetallics are formed in the alloy modified with mischmetal addition.A higher fraction of dynamically recrystallized grains is observed for the ZK60-Mm in comparison to the *** recrystallization takes place in ZK60 with the formation of sub-grains near to the intermetallics and the addition of mischmetal promotes the occurrence of discontinuous recrystallization with the nucleation of new grains close to the *** mechanical strength and,in particular,the ductility of the hot-rolled alloys are notably improved when compared to the same alloys in the as-cast *** mechanical strength is,however,higher for the ZK60 *** solid solution strengthening,softer Mg Zn_(2) Ce intermetallics and more extensive recrystallization contribute to reduce the mechanical strength of *** in both alloys are initiated at coarse intermetallics and propagate through intermetallic-rich regions.

关键词： Magnesium alloys Hot rolling Mischmetal Recrystallization Microstructure Mechanical properties

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