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Properties of Ultra-low Thermal Expansion LAS Transparent Glass-ceramics Prepared by Spodumene

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Journal of Wuhan University of technology(materials Science) 2024年第3期39卷 541-550页

作者：何峰何子君 ZHOU Zhiqiang TIAN Yingliang ZHAO Zhiyong School of materials Science and Engineering Beijing University of TechnologyBeijing 100124China Department of Functional material Research Central Iron and Steel Research InstituteBeijing 100081China School of materials Science and Engineering Wuhan University of TechnologyWuhan 430070China National Engineering Research Center of FPD Glass technology Xianyang 712000China

The glass-ceramics were prepared with the spodumene mineral as the main raw material,and the effects of ZrO_(2)replacing TiO_(2)on the samples were systematically *** results show that the substitution of ZrO_(2)for TiO_(2)is not conductive to precipitate𝛽β-quartz solid solution phase,but can improve the transparency and flexural strength of *** the glass-ceramic with the highest visible light transmittance(87%)and flexural strength(231.80 MPa)exhibits an ultra-low thermal expansion of-0.028×10^(-7)K^(-1)in the region of 30-700℃.

关键词： ultra-low thermal expansion LAS transparent glass-ceramics substitution of ZrO_(2)for TiO_(2) spodumene mineral

Superior Latent Heat Eutectic Salt Na_(2)co_(3)-Li_(2)co_(3)-LiF for Thermal Energy Storage:Preparation and Performance Investigation

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Journal of Thermal Science 2024年第2期33卷 501-508页

作者： LI Weiwei MIAO Qi ZHANG Yelong DING Hongliang YANG Sa LAI Yuan FENG Daili DING Yulong JIN Yi TAN Linghua School of Chemistry and Chemical Engineering Nanjing University of Science&TechnologyNanjing210094China National Special Superfine Powder Engineering Research Center Nanjing University of Science and TechnologyNanjing210094China Nanjing Jinhe Energy material co. LtdNanjing210047China School of Chemical Engineering University of BirminghamBirminghamB152TTUK School of Energy&Environmental Engineering University of Science and Technology BeijingBeijing100083China

In this paper,a novel ternary eutectic salt Na_(2)co_(3)-Li_(2)co_(3)-LiF was designed and investigated for concentrated solar power(CSP).The FactSage software was used to predict the composition and eutectic point of Na_(2)co_(3)-Li_(2)co_(3)-*** microstructure,thermophysical properties,and thermal stability of eutectic salts were experimentally measured using various analytical *** a mass ratio of 57%:32%:11%,the eutectic salt exhibited excellent thermal storage properties with a fusion enthalpy of 413 J/g and a melting point of 426.8℃.The excellent thermal stability of the eutectic salt was reflected by a weight loss of only 0.8% at 600℃.

关键词： phase change materials ternary eutectic salt latent heat thermal stability

Early-stage latent thermal failure of single-crystal Ni-rich layered cathode

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Journal of Energy Chemistry 2024年第9期96卷 578-587页

作者： Xiao Han Ruoyu Xu Yan Li Yang Ding Manchen Zhang Bo Wang Xiaoxing Ke Manling Sui Pengfei Yan beijing Key Laboratory of Microstructure and Property of Solids Faculty of Materials and ManufacturingBeijing University of TechnologyBeijing 100124China Watt Laboratory Central Research InstituteHuawei Technologies Co.LTDShenzhen 518129GuangdongChina

High nickel content worsens the thermal stability of layered cathodes for lithium-ion batteries,raising safety concerns for their *** understanding the thermal failure process can offer valuable guidance for material optimization on thermal stability and new opportunities in monitoring battery thermal runaway(TR).Herein,this work comprehensively investigates the thermal failure process of a single-crystal nickel-rich layered cathode and finds that the latent thermal failure starts at∼120℃far below the TR temperature(225℃).During this stage of heat accumulation,sequential structure transition is revealed by atomic resolution electron microscopy,which follows the layered→cation mixing layered→LiMn_(2)O_(4)-type spinel→disordered spinel→rock *** progression occurs as a result of the continuous migration and densification of transition metal *** transition generates gaseous oxygen,initially confined within the isolated closed pores,thereby not showing any thermal failure phenomena at the *** temperature leads to pore growth and coalescence,and eventually to the formation of open pores,causing oxygen gas release and weight loss,which are the typical TR *** highlight that latent thermal instability occurs before the macro-level TR,suggesting that suppressing phase transitions caused by early thermal instability is a crucial direction for material *** findings can also be used for early warning of battery thermal runaway.

关键词： Thermal runaway Nickel-rich layered cathode Transmission electron microscopy Lithium-ion battery Phase transition

Changes in microstructure and properties of weld heat-affected zone of high-strength low-alloy steel

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Journal of Iron and Steel Research International 2024年第8期31卷 2041-2052页

作者： Shu-jun Jia Qi-lin Ma Yu Hou Ba Li He-song Zhang Qing-you Liu Central Iron and Steel Research Institute co. Ltd.Beijing 100081China collaborative Innovation Center for Steel commonality University of Science and Technology BeijingBeijing 100083China construction Project Management Branch of China National Petroleum Pipeline Network Group co. Ltd.Langfang 065000HebeiChina

The evolution of the microstructure and toughness of APL5L X80 pipeline steel after thermal welding simulation was investigated by X-ray diffraction,electron backscatter diffraction,and transmission electron *** results indicated that primary heat-affected zones can be divided into weld,coarse-grained,fine-grained,intercritical,and sub-critical *** microstructure of the weld zone is mainly composed of bainitic ferrite and a small amount of granular bainite;however,the original austenite grains are distributed in the columnar *** structure of the coarse-grained zone is similar to that of the weld zone,but the original austenite grains are *** contrast,the microstructure in the fine-grained zone is dominated by fine granular bainite,and the effective grain size is only 8.15μm,thus providing the highest toughness in the entire heat-affected *** intercritical and subcritical zones were brittle valley regions,and the microstructure was dominated by granular ***,the martensite-austenite(M/A)constituents are present in island chains along the grain boundaries,and the coarse size of the M/A constituents seriously reduces the *** results of the crack propagation analyzes revealed that high-angle grain boundaries can significantly slow down crack growth and change the crack direction,thereby increasing the material *** impact toughness of the low-temperature tempering zone was equivalent to that of the columnar grain zone,and the impact toughness was between those of the critical and fine-grained zones.

关键词： Welding thermal simulation Impact toughness Crack propagation Martensite-austenite constituent High-strength low-alloy steel weld Heat-affected zone

Preparation and Properties of Glass with High Transmittance and Intense Gamma Ray Shielding

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硅酸盐学报 2024年第10期52卷 3301-3310页

作者： ZHANG Meilun CAO Zhenbo YANG Shengyun ZHANG Yang HAN Yu QIU Fu ZHOU You ZHENG Jingming LIU Hui JIA Jinsheng China National Building material Photonics technology co. Ltd.Zaozhuang 277000ShandongChina China Building materials Academy co. Ltd.Beijing 100000China

Introduction As a kind of high-energy electromagnetic radiation,gamma rays can lead to radiation effect and environmental *** ensure the reliability and safety utilization of gamma radiations in different areas,materials with reliable gamma shielding performances should be *** existing efforts are to use glasses as alternative for the conventional radiation shielding *** a typical window material,glass itself has attracted wide attention due to its unique chemical and physical *** them,lead-based radiation shielding materials are widely used in the field of ionizing radiation protection due to their reliable physical *** the nuclear industry and high energy physics laboratories,different materials can be used for temporary or permanent *** lead-based glass doped with heavy metal oxide PbO is widely used in the field of radiation shielding for a long time with reliable light transmission properties,which facilitates the observation and monitoring of radiation *** this paper,three kinds of transparent silicate glass with different PbO contents were prepared by a high-temperature melting forming *** gamma-rays protection abilities of the three kinds of glass were investigated through experimental and thermotical *** chemical and thermal stability of the glass were also *** addition,the influence mechanism of the structure and performance differences of the three kinds of glass was also *** Analytical pure quartz sand(SiO_(2),purity 99.5%,in mass,the same below),lead monoxide(PbO,purity 99.0%),potassium nitrate(KNO3,purity 99.0%)and sodium nitrate(NaNO3,purity 99.0%)were selected as raw materials for preparation of three kinds of gamma-rays shielding glass materials by a high-temperature melting *** appropriate amount of raw materials was thoroughly mixed and added to 3 L quartz crucible and heated in air at 1200℃.Then the raw materials were melted at 1250℃for 14

关键词： transmittance gamma rays radiation shielding glass

Boosting rate performance of layered lithium-rich cathode materials by oxygen vacancy induced surface multicomponent integration

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Journal of Energy Chemistry 2024年第5期92卷 250-262页

作者： Youyou Fang Yuefeng Su Jinyang Dong Jiayu Zhao Haoyu Wang Yun Lu Bin Zhang Hua Yan Feng Wu Lai Chen beijing Key Laboratory of Environmental Science and Engineering School of Material Science and EngineeringBeijing Institute of TechnologyBeijing 100081China Chongqing Innovation Center Beijing Institute of TechnologyChongqing 401120China Yibin Libode New materials co. Ltd.Yibin 64400SichuanChina School of Metallurgy and Environment Central South UniversityChangsha 410083HunanChina Engineering Research Center of the Ministry of Education for Advanced Battery materials Central South UniversityChangsha 410083HunanChina

The rapid development of electric vehicles and portable energy storage systems demands improvements in the energy density and cost-effectiveness of lithium-ion batteries,a domain in which Lithium-rich layered cathode(LLO)materials inherently ***,these materials face practical challenges,such as low initial coulombic efficiency,inferior cycle/rate performance,and voltage decline during cycling,which limit practical *** study introduces a surface multi-component integration strategy that incorporates oxygen vacancies into the pristine LLO material Li1.2Mn_(0.6)Ni_(0.2)O_(2).This process involves a brief citric acid treatment followed by calcination,aiming to explore rate-dependent degradation *** induced surface oxygen vacancies can reduce surface oxygen partial pressure and diminish the generation of O_(2)and other highly reactive oxygen species on the surface,thereby facilitating the activation of Li ions trapped in tetrahedral sites while overcoming transport ***,the formation of a spinel-like phase with 3D Li+diffusion channels significantly improves Li^(+)diffusion kinetics and stabilizes the surface *** optimally modified sample boasts a discharge capacity of 299.5 mA h g^(-1)at a 0.1 C and 251.6 mA h g^(-1)at a 1 C during the initial activation cycle,with an impressive capacity of 222.1 mA h g^(-1)at a 5 *** notably,it retained nearly 70%of its capacity after 300 cycles at this elevated *** straightforward,effective,and highly viable modification strategy provides a crucial resolution for overcoming challenges associated with LLO materials,making them more suitable for practical application.

关键词： Lithium-ion battery Layered lithium rich cathode Surface multicomponent integration Rate-dependent degradation and Li^(+) diffusion kinetics

material-SAM:Adapting SAM for material XCT

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computers, materials & continua 2024年第3期78卷 3703-3720页

作者： Xuelong Wu Junsheng Wang Zhongyao Li Yisheng Miao Chengpeng Xue Yuling Lang Decai Kong Xiaoying Ma Haibao Qiao School of materials Science and Engineering Beijing Institute of TechnologyBeijing100081China Senior Engineer at the Simulation Center Citic Dicastal Co.Ltd.Qinhuangdao066010China

X-ray computed Tomography(XCT)enables non-destructive acquisition of the internal structure of materials,and image segmentation plays a crucial role in analyzing material XCT *** paper proposes an image segmentation method based on the Segment Anything model(SAM).We constructed a dataset of carbide in nickel-based single crystal superalloys XCT images and preprocessed the images using median filtering,histogram equalization,and gamma ***,SAM was fine-tuned to adapt to the task of material XCT image segmentation,resulting in *** compared the performance of threshold segmentation,SAM,U-Net model,and *** method achieved 88.45%Class Pixel Accuracy(CPA)and 88.77%Dice Similarity coefficient(DSC)on the test set,outperforming SAM by 5.25%and 8.81%,respectively,and achieving the highest ***-SAM demonstrated lower input requirements compared to SAM,as it only required three reference points for completing the segmentation task,which is one-fifth of the requirement of ***-SAM exhibited promising results,highlighting its potential as a novel method for material XCT image segmentation.

关键词： Segment Anything model X-ray computed tomography U-Net Ni-based superalloys foundation models

Investigation of high rate mechanical flow followed by ignition for high-energy propellant under dynamic extrusion loading

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Defence technology（防务技术） 2024年第2期32卷 336-347页

作者： Liying Dong Yanqing Wu Kun Yang Xiao Hou State Key Laboratory of Explosion Science and technology Beijing Institute of TechnologyBeijing 100081China School of Aerospace Engineering Beijing Institute of TechnologyBeijing 100081China

Investigating the ignition response of nitrate ester plasticized polyether(NEPE) propellant under dynamic extrusion loading is of great significant at least for two cases. Firstly, it helps to understand the mechanism and conditions of unwanted ignition inside charged propellant under accident ***, evaluates the risk of a shell crevice in a solid rocket motor(SRM) under a falling or overturning scene. In the present study, an innovative visual crevice extrusion experiment is designed using a dropweight apparatus. The dynamic responses of NEPE propellant during extrusion loading, including compaction and compression, rapid shear flow into the crevice, stress concentration, and ignition reaction, have been firstly observed using a high-performance high-speed camera. The ignition reaction is observed in the triangular region of the NEPE propellant sample above the crevice when the drop weight velocity was 1.90 m/s. Based on the user material subroutine interface UMAT provided by finite element software LS-DYNA, a viscoelastic-plastic model and dual ignition criterion related to plastic shear dissipation are developed and applied to the local ignition response analysis under crevice extrusion conditions. The stress concentration occurs in the crevice location of the propellant sample, the shear stress is relatively large, the effective plastic work is relatively large, and the ignition reaction is easy to occur. When the sample thickness decreases from 5 mm to 2.5 mm, the shear stress increases from 22.3 MPa to 28.6 MPa, the critical value of effective plastic work required for ignition is shortened from 1280 μs to 730 μs, and the triangular area is easily triggering an ignition reaction. The propellant sample with a small thickness is more likely to stress concentration, resulting in large shear stress and effective work, triggering an ignition reaction.

关键词： NEPE propellant Crevice extrusion Shear flow Sample thickness Ignition reaction

Precisely modulating covalent and coordination bonds in the porous network for highly selective metal ion extraction

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Science China Chemistry 2024年第4期67卷 1039-1040页

作者： Jie Li Xiao Feng beijing Key Laboratory of Photoelectronic/Electrophotonic conversion materials Key Laboratory of Cluster ScienceMinistry of EducationAdvanced Technology Research Institute(Jinan)Frontiers Science Center for High Energy MaterialSchool of Chemistry and Chemical EngineeringBeijing Institute of TechnologyBeijing 100081China

Scandium(Sc)is recognized as a“strategic”and“critical”element by several countries,including the *** Russia,owing to its wide range of applications in high-tech fields such as superconductivity,alloys,lasers,nucle... 详细信息

关键词： alloys coordination network