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Acta Metallurgica Sinica(English Letters) 2024年第3期37卷 577-585页

作者： Fanjing Meng Wenbo Du Ning Ding Jian Sun Xian Du Ke Liu Shubo Li college of materials {2. and engineering Faculty of Materials and ManufacturingBeijing University of TechnologyBeijing 100124China

The hybrid of carbon nanotube(CNT)and reduced graphene oxide(RGO)reinforced ZK61 composite was fabricated by a hot extrusion *** with the raw ZK61 alloy and single-reinforced composites,the hybrid-reinforced by RGO+CNT complex exhibited significant enhancements both in mechanical and thermal *** adjusting the proportion of RGO and CNT in ZK61 alloy,the obtained optimum ZK61/(0.06 wt%RGO+0.54 wt%CNT)composite exhibited increase of 2..4%in yield strength,2..5%in ultimate tensile strength,104%in failure strain and 30.4%in thermal conductivity,respectively,in comparison with ZK61 *** superior properties of the nano-hybrid composite are attributed to the synergetic effects of RGO and CNT,leading to a uniform dispersion and integrated structure as well as the enhanced interfacial bonding with *** strengthening ability of RGO and CNT was calculated to quantify their individual contribution to the improvement in mechanical and thermal properties of the ZK61 matrix *** RGO+CNT hybrids provide a promising way to develop Mg matrix composites with impressive performances.

关键词： Mg matrix composite Carbon nanotube Reduced graphene oxide Mechanical performance Thermal conductivity

Microstructure and damping properties of LPSO phase dominant Mg-Ni-Y and Mg-Zn-Ni-Y alloys

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Journal of Magnesium and Alloys 2024年第3期12卷 1131-1153页

作者： Ruopeng Lu Kai Jiao Nanting Li Hua Hou Jingfeng Wang Yuhong Zhao college of materials {2. and engineering North University of ChinaTaiyuan 030051China college of materials {2. and engineering Taiyuan University of TechnologyTaiyuan 030024China National engineering Research Center for Magnesium Alloys Chongqing UniversityChongqing 400044China college of materials {2. and engineering Chongqing UniversityChongqing 400044China

This work studied the microstructure,mechanical properties and damping properties of Mg_(95.34)Ni_(2.Y_(2.66) and Mg_(95.34)Zn_(1)Ni_(1)Y_(2.66)alloys *** difference in the evolution of the long-period stacked ordered(LPSO)phase in the two alloys during heat treatment was the *** morphology of the as-cast Mg_(95.34)Ni_(2.Y_(2.66)presented a disordered *** heat treatment at 773 K for 2.hours,the eutectic phase was integrated into the matrix,and the LPSO phase maintained the 18R *** Zn partially replaced Ni,the crystal grains became rounded in the cast alloy,and lamellar LPSO phases and more solid solution atoms were contained in the matrix after heat treatment of the Mg_(95.34)Zn_(1)Ni_(1)Y_(2.66)*** Zn and the heat treatment had a significant effect on *** dislocation internal friction peaks and grain boundary internal friction peaks were found after temperature-dependent damping of the Mg_(95.34)Ni_(2.Y_(2.66)and Mg_(95.34)Zn_(1)Ni_(1)Y_(2.66)*** heat treatment,the dislocation peak was significantly increased,especially in the alloy Mg_(95.34)Ni_(2.Y_(2..*** annealed Mg_(95.34)Ni_(2.Y_(2.66)alloy with a rod-shaped LPSO phase exhibited a good damping performance of 0.14 atε=10^(−3),which was due to the difference between the second phase and solid solution atom *** factors also affected the dynamic modulus of the *** results of this study will help in further development of high-damping magnesium alloys.

关键词： Mg-Ni-Y alloys Mg-Zn-Ni-Y alloys LPSO phase Heat treatment Microstructure Damping properties.

Deterioration Reason and Improvement Measure of the Retarding Effect of Protein Retarder on Phosphorus Building Gypsum

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Journal of Wuhan University of Technology(materials science) 2024年第4期39卷 962-967页

作者：刘志刚 TANG Zezheng 杨立荣 WANG Chunmei XIE Yuantao LIU Yisen college of materials {2. and engineering North China University of Science and TechnologyTangshan 063210China

The retarding effect of protein retarder on phosphorus building gypsum(PBG)and desulfurization building gypsum(DBG)was investigated,and the results show that protein retarder for DBG can effectively prolong the setting time and displays a better retarding effect,but for PBG shows a poor retarding ***,the deterioration reason of the retarding effect of protein retarder on PBG was investigated by measuring the pH value and the retarder concentration of the liquid phase from vacuum filtration of PBG slurry at different hydration time,and the measure to improve the retarding effect of protein retarding on PBG was *** pH value of PBG slurry(2.0 min,but little effect on the absolute dry flexural strength was observed.

关键词： protein retarder phosphorus building gypsum deterioration reason improvement measure

Interfacial Reaction of Ti6Al4V Lattice Structure-Reinforced VW92.Alloy Matrix Composites

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Acta Metallurgica Sinica(English Letters) 2024年第3期37卷 570-576页

作者： Haijun Wang Renju Cheng Xianhua Chen Mingbo Yang Daiyi Deng Lirui Liu Yongfeng Zhou Yanlong Ma Kaihong Zheng Fusheng Pan college of materials {2. and engineering Chongqing University of TechnologyChongqing 400054China college of materials {2. and engineering Chongqing UniversityChongqing 400044China Institute of New materials Guangdong Academy of SciencesGuangzhou 510650China

A novel melting infiltration by ultrasonic vibration was investigated and applied to fabricate Ti6Al4V(TC4)lattice structure-reinforced Mg-10Gd-2.-1Zn-xZr(refer to VW92.hereafter,x=0,0.5 wt%)alloy matrix *** edge-to-edge matching model indicates that the well-matching and possible orientation relationships(ORs)between theα-Mg andα-Ti,[10-10]_(α-Mg)//[11-2.]_(α-Ti) in(0002._(α-Mg)//(10-10)_(α-Ti) possesses the smallest misfit of 0.4%(f_(r)),and thus theα-Mg grains can nucleate on the TC4 lattice *** reaction occurred in the TC4/VW92.0.5 wt%Zr composites,and the reaction product was confirmed to be Al_(2.Zr_(3),AlZr_(2. andα-Ti(Zr)particles formed by continuous solution of *** the interfacial products,the AlZr_(2. phase is a brittle phase with high-volume fraction,which is not conducive to the load *** generally speaking,theα-Ti(Zr)and theα-Mg tend to form a coherent interface,which is beneficial for improving the interfacial bonding strength of composites.

关键词： TC4 VW92.composites TC4 lattice structure Interfacial reaction Mismatch

B-N covalent bond-involved π-extension of multiple resonance emitters enables high-performance narrowband electroluminescence

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National science Review 2024年第06期11卷 243-253页

作者： Xingyu Huang Jiahui Liu Yulin Xu Guohao Chen Manli Huang Mingxin Yu Xialei Lv Xiaojun Yin Yang Zou Jingsheng Miao Xiaosong Cao Chuluo Yang Shenzhen Key Laboratory of New Information Display and Storage materials College of Materials Science and EngineeringShenzhen University college of Physics and Optoelectronic engineering Shenzhen University

Multi-boron-embedded multiple resonance thermally activated delayed fluorescence（MR-TADF） emitters show promise for achieving both high color-purity emission and high exciton utilization ***, their development is often impeded by a limited synthetic scope and excessive molecular weights,which challenge material acquisition and organic light-emitting diode（OLED） fabrication by vacuum deposition. Herein, we put forward a B–N covalent bond-involved π-extension strategy via post-functionalization of MR frameworks, leading to the generation of high-order B/N-based motifs. The structurally and electronically extended π-system not only enhances molecular rigidity to narrow emission linewidth but also promotes reverse intersystem crossing to mitigate efficiency roll-off. As illustrated examples, ultra-narrowband sky-blue emitters（full-width at half-maximum as small as 8 nm in n-hexane）have been developed with multi-dimensional improvement in photophysical properties compared to their precursor emitters, which enables narrowband OLEDs with external quantum efficiencies(EQEmax) of up to 42.6%, in company with alleviated efficiency decline at high brightness, representing the best efficiency reported for single-host OLEDs. The success of these emitters highlights the effectiveness of our molecular design strategy for advanced MR-TADF emitters and confirms their extensive potential in high-performance optoelectronic devices.

关键词： narrowband electroluminescence thermally activated delayed fluorescence (TADF) multiple resonance emitters ultra-high external quantum efficiency

MOF-derived porous graphitic carbon with optimized plateau capacity and rate capability for high performance lithium-ion capacitors

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International Journal of Minerals,Metallurgy and materials 2024年第2期31卷 395-404页

作者： Ge Chu Chaohui Wang Zhewei Yang Lin Qin Xin Fan college of materials {2.&engineering Guilin University of TechnologyGuilin 541004China Institute of Energy Innovation College of Materials Science and EngineeringTaiyuan University of TechnologyTaiyuan 030024China

The development of anode materials with high rate capability and long charge-discharge plateau is the key to improve per-formance of lithium-ion capacitors(LICs).Herein,the porous graphitic carbon(PGC-1300)derived from a new triply interpenetrated co-balt metal-organic framework(Co-MOF)was prepared through the facile and robust carbonization at 1300°C and washing by HCl *** as-prepared PGC-1300 featured an optimized graphitization degree and porous framework,which not only contributes to high plateau capacity(105.0 mAh·g^(−1)below 0.2.V at 0.05 A·g^(−1)),but also supplies more convenient pathways for ions and increases the rate capability(12..5 mAh·g^(−1)at 3.2.A·g^(−1)).According to the kinetics analyses,it can be found that diffusion regulated surface induced capa-citive process and Li-ions intercalation process are coexisted for lithium-ion ***,LIC PGC-1300//AC constructed with pre-lithiated PGC-1300 anode and activated carbon(AC)cathode exhibited an increased energy density of 102.8 Wh·kg^(−1),a power dens-ity of 6017.1 W·kg^(−1),together with the excellent cyclic stability(91.6%retention after 10000 cycles at 1.0 A·g^(−1)).

关键词： metal-organic framework porous graphitic carbon optimized plateau capacity kinetic analysis lithium-ion capacitor

Enhanced bright green luminescence from GdOF:Ho^(3+) up-conversion phosphor via Yb^(3+) doping

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Journal of Rare Earths 2024年第2期42卷 263-269,I0002页

作者： Linjun Qin Yue Guo Jing Xu Lixi Wang Qitu Zhang college of materials {2. and engineering Nanjing Tech UniversityNanjing211816China

In this paper,a series of GdOF-based green phosphors doped with Ho^(3+) and Yb^(3+) ions was prepared by a simple co-precipitation *** crystal structure s and optical prope rties were investigated in *** intensity of the emission of GdOF:Yb^(3+),Ho^(3+) phosphors is enhanced by the effective energy transfer from Yb^(3+) to Ho^(3+),and the optimal luminescence is achieved with the Ho^(3+)doping amount of 0.1 mol%as well as Yb^(3+) doping amount of 5 mol%.Tunable UC emission of samples is achieved by adjusting the doping concentration of Ho^(3+) or Yb^(3+).The purity of the green UC emission is further improved by enhancing the excitation pumping *** addition,logarithmic functions of green,red and nearinfrared radiation intensities were calculated versus logarithmic function of pump power for further study.A possible UC luminescence mechanism between Yb^(3+) and Ho^(3+) is discussed based on powerdependent UC luminescence spectrum and decay *** results suggest that GdOF:Yb^(3+),Ho^(3+)phosphors with bright and high-purity green UC emission have potential applications in the fields of bioimaging,display and illumination.

关键词： Up-conversion GdOF Lanthanide ions Rare earths

Microstructure and Mechanical Properties of the Ti_(62.Nb_(12.Mo_(12.Ta_(12.W_(2.Refractory High Entropy Alloy Prepared through Spark Plasma Sintering

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Acta Metallurgica Sinica(English Letters) 2024年第8期37卷 1387-1398页

作者： Zirui Chen Liyuan Wang Jiayu Zhao Guanhua Cui Zhuo Gao Zhiyuan Fan Xiaohui Shi Junwei Qiao college of materials {2. and engineering Taiyuan University of TechnologyTaiyuan 030024China

A refractory high entropy alloy Ti_(62.Nb_(12.Mo_(12.Ta_(12.W_(2.was prepared by mechanical alloying and spark plasma *** microstructure and mechanical properties of the Ti_(62.Nb_(12.Mo_(12.Ta_(12.W_(2.alloy were *** experimental results show that the microstructure of the alloy is composed of two BCC phases,an FCC precipitated phase,and the precipitated phase which is a mixture of TiC,TiN and *** alloy exhibits good room temperature compressive *** plasticity of the sample sintered at 1550℃can reach 10.8%,and for the sample sintered at 1600℃,the yield strength can be up to 2.32.MPa,in the meantime the plasticity is 9.4%.The alloy also shows high strength at elevated *** yield strength of the alloy exceeds 42. MPa at 900℃,and value of which is still above 2.0 MPa when the test temperature reaches 1000℃.Finally,the compressive yield strength model at room temperature is *** prediction error of the model ranges from−7.9%to−12.4%,expressing fair performance.

关键词： Refractory high-entropy alloy(RHEA) Mechanical alloying Mechanical properties Model Spark plasma sintering

Surface reconstruction of heterostructures in alkaline medium towards enhanced electrocatalytic hydrogen evolution

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Rare Metals 2024年第6期43卷 2636-2647页

作者： Ming-Yang Yang Ji Yuan Xue-Lian Fu Jing-Jing Chen Jing Hu Zhou-Guang Lu Chen Liu Guangdong Research Center for Interfacial engineering of Functional materials Shenzhen Key Laboratory of Polymer Science and TechnologyShenzhen Key Laboratory of Energy Electrocatalytic MaterialsCollege of Materials Science and EngineeringShenzhen UniversityShenzhen 518060China Shenzhen Key Laboratory of Interfacial science and engineering of {2. Department of Materials Science and EngineeringSouthern University of Science and TechnologyShenzhen 518055China

Constructing heterostructures has proved to be a successful strategy to fabricate electrocatalysts with high efficiency for water ***,the structure evolution in alkaline hydrogen evolution reaction lacks investigation and the specific active center remains ***,we take the well-designed Ni_(3)S_(2.@VO_(2. heterostructures as a model to investigate the electrocatalytic activity and the surface reconstruction process of heterostructure catalysts in alkaline *** Ni_(3)S_(2.@VO_(2. heterostructures,with Ni_(3)S_(2. nanorods as the core and VO_(2. nanoflakes as the shell,coupled with the high conductive Ni_(3)S_(2.,the hydrophilic VO_(2. and modulated electronic structures at the interfaces,exhibited prominent activity and superior stability at various current ***,the ex-situ characterizations confirmed that the surface reconstruction from Ni_(3)S_(2.@VO_(2. into Ni_(3)S_(2.@amorphous-Ni(OH)_(2. in alkaline media could optimize the water dissociation barrier and exposed large active area,thereby contributing to improved electrocatalytic *** study not only introduces novel high-performance electrocatalysts for hydrogen evolution reaction(HER),but also provides a new avenue for re-examining hetero-structural catalysts in alkaline solutions.

关键词： Heterostructures Ni_(3)S_(2.@VO_(2. Surface reconstruction Water dissociation Alkaline hydrogen evolution

Hybrid pseudocapacitance/co-intercalation mechanisms of TiO2.graphite anodes for rapid sodium-ion storage

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Rare Metals 2024年第10期43卷 5427-5434页

作者： Ze-Rui Yan Da-Fu Tang Bin-Hao Wang Xiao-Juan Huang Xia Zou Si-Cheng Fan Yan Wu Tong Shu Qiu-Long Wei Department of materials science and {2. College of MaterialsFujian Key Laboratory of Surface and Interface Engineering for High Performance MaterialsXiamen University

Developing anode materials with high specific/volumetric capacities,high-rate capability,long-term cycles and low cost is significant for advanced sodium-ion ***,we report the hybrid TiO2.graphite （TiO2.G） anodes for fast （dis）charging sodium-ion *** advantage of the rapid pseudocapacitive surface-redox on anatase TiO2.anoparticles （NPs） and fast[Na（diglyme）x]+co-intercalation into graphite,the hybrid anodes display excellent rate ***,the TiO2.Ps are able to fill into the interspaces among graphite flakes and the graphite provides continuous electron pathways,which largely boosts the volumetric capacities and rate *** from the synergistic effects,

关键词： Titanium dioxide