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Compatibility evaluation between waterborne epoxy resin and SBR latex modified asphalt emulsion

Journal of Traffic and Transportation Engineering(English Edition) 2024年第1期11卷 160-171页

作者： Jianhua Yang Zhengqi Zhang Ying Fang Key Laboratory for Special Area Highway Engineering of Ministry of Education Chang'an UniversityXi'an 710064China

Good compatibility between waterborne epoxy resin(WER)modifier and styrene-butadiene rubber(SBR)latex modified asphalt emulsion(SBRE)is an essential premise for good pavement performance of WER and SBR latex compositely modified asphalt emulsion(WSAE).This study aims to explore the compatibility between WER modifier and *** achieve the goal,several WER modifiers produced by two methods were first selected to modify SBRE,thus the WSAEs were ***,storage stability and workability of the WSAEs themselves,and high-temperature performance,rheological behavior and temperature sensitivity of their evaporated residues were compared and evaluated via performing a series of experiments,respectively,thus the WER modifier possessing an optimal modification effect was *** show that the storage stability of WSAEs is sensitive to the amount of *** incorporation of 1%WERs by the mass of SBRE improves the storage stability of SBRE,while WERs that exceed 1%weaken its storage *** the WERs reach 3%and 4%,the 5 d storage stability of prepared WSAEs will be beyond the limitation of *** WERs into SBRE negatively affects the workability of SBRE,and the workability of WSAEs is adversely influenced by the WERs content and the storage *** ensure the construction,the WSAEs with 3%and 4%WERs should not be stored for more than 36 h and 48 h,*** WERs effectively improve the high-temperature performance of SBRE residue,especially the 3%***,the WERs notably enhance the rheological property and thermal stability of SBRE *** contrast,the WER modifier produced by chemically modified method has a smaller adverse impact on the storage stability and workability of WSAE,and a larger enhancement on the high-temperature performance,rheological property and thermal stability of SBRE residue,which is thus recommended to modify SBRE.

关键词： waterborne epoxy resin SBR modified asphalt emulsion Workability Rheological property Temperature sensitivity Compatibility evaluation

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waterborne epoxy resin Modified by AMPS

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Journal of Wuhan University of Technology(Materials Science) 2007年第4期22卷 649-652页

作者：马承银 School of Chemistry and Chemical Engineering Central South University

A stable epoxy emulsion was prepared with epoxy resin （EP） as raw material, 2-acrylamido-2- methyl-l-propanesulfonic acid （AMPS） as modifier and benzoyl peroxide as initiator. By criterion of yield of the copolymer AMPS-EP, water-solubility, change of the acid value and intrinsic viscosity [η] along with reaction time, the copolymerization course was deduced. It is found that during the process, AMPS takes part in both the grafting copolymerization with epoxy principal chain and the ring-opening polyaddition with epoxy group. It is also discovered that the yield of AMPS-EP and water dispersing varies with reaction time. When it reaches 1.5 h, AMPS-EP can obtain good water-solubility; but the water-solubility will go bad gradually if it exceeds 3.5 h.. R spectrum analysis indicates that partial epoxy group partially remains and the others create sulfonic ester.

关键词： waterborne epoxy resin 2-acrylamido-2-methyl-l-propanesulfonic acid grafting copolymerization ring-opening polyaddition soap-free emulsion

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Mechanism Analysis of Stiffness Improvement by waterborne epoxy resin Surface Sizing Agent

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Paper And Biomaterials 2016年第1期1卷 44-50页

作者： Hui Xu ShuMei Wang YuanYuan Li HongQi Dai Jiangsu Provincial Key Lab of Pulp and Paper Science and Technology Nanjing Forestry University

Low-basis-weight paper lacks normal strength and stiffness. waterborne epoxy resin could be employed with oxidized starch to improve paper stiffness through surface sizing. In this study,the mechanism of enhancing stiffness by adding waterborne epoxy resin was fully investigated. The results indicated that through surface sizing with epoxy resin,the paper thickness was preserved,whereas the elastic modulus increased significantly and the epoxy resin had positive impact on single fiber strength. A rigid resin layer and interpenetrating polymer network formed on the surface and in the inner layer of the paper,respectively. The formed resin layer and interpenetrating polymer network strongly supported the paper,leading to the improvement of the elastic modulus and stiffness. The stiffness improvement through surface sizing was mainly due to the formation of a fibrous composite layer and penetration of the sizing agent into the inner layers of the paper. The better the combination between fiber and sizing agent,the higher were the elastic modulus and the stiffness of the whole paper.

关键词： surface sizing stiffness mechanism analysis waterborne epoxy resin

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