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Experimental study on mercury content in flue gas of coal-fired units based on laser-induced breakdown spectroscopy

Plasma Science and Technology 2020年第7期22卷 75-82页

作者： Kai RONG Zhenzhen WANG Ruomu HU Renwei LIU Yoshihiro DEGUCH Junjie YAN Jiping LIU State Key Laboratory of Multiphase Flow in Power Engineering Xi'an Jiaotong UniversityXi'an 710049People’s Republic of China Graduate School of Technology Industrial and Social SciencesTokushima UniversityTokushima 770-8501Japan Moe Key Laboratory of Thermo-Fluid Science and Engineering Xi'an Jiaotong UniversityXi'an 710049People’s Republic of China

Accurate measurement of trace heavy metal mercury(Hg) in flue gas of coal-fired units is great significance for ecological and environmental *** gas was used to simulate the actual flue gas of a power plant in this study.A laser-induced breakdown spectroscopy(LIBS)system for Hg measurement in mixed gas was built to study the effect of mixed gas pressure,Hg concentration in mixed gas and delay time on Hg *** experimental results show that the appropriate low mixed gas pressure can obtain high Hg signal intensity and signal to noise *** Hg signal intensity and signal to noise ratio increased with the increase of Hg concentration in mixed *** Hg signal intensity and signal to noise ratio decreased with the increase in delay *** to the above results,the optimized measurement conditions can be *** Hg concentrations in mixed gas were quantitatively analyzed by the internal standard method and traditional calibration method *** relative error of prediction of the test sample obtained by the internal standard method was within 11.11%.The relative error of prediction of the traditional calibration method was less than 14.54%.This proved that the internal standard method can improve the accuracy of quantitative analysis of Hg concentration in flue gas using LIBS.

关键词： laser-induced breakdown spectroscopy flue gas trace heavy metal quantitative analysis

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