检索结果-南通市图书馆

Novel technique for measurement of coating layer thickness of fine and porous particles using focused ion beam

Particuology 2019年第1期17卷 190-198页

作者： M. Goslinska I. Selmer C. Kleemann U.Kulozik I. Smirnova S. Heinrich Hamburg University of Technology Institute of Solids Process Engineering and Particle TechnologyDenickestr1521073 HamburgGermany Hamburg University of Technology Institute of Thermal Separation ProcessesEiJ^endorfer Str. 3821073 HamburgGermany Technical University of Munich Chair of Food and Bioprocess EngineeringWeihenstephaner Berg 185354 FreisingGermany

A novel technique for the measurement of the coating layer thickness of fine particles was developed in this work based on cross-sectioning of micrometre-sized single coated particles using focused ion beam (FIB) milling. This technique was tested on two batches of aerogel particles coated with thin coatings in a spouted bed. The FIB milling procedure consisted of two steps. First, the desired part of the coated particle was removed using a high ion beam current. The resulting cross-sectioned area was then polished using a lower ion beam current to make the cross-section clearly visible. The FIB milling process was controlled with simultaneous scanning electron microscopy (SEM). Afterwards, the coating layer thickness was evaluated using the SEM images. The coating layer was successfully applied on the porous aerogel microparticles in the spouted bed. The coating uniformity of the highly porous particles increased with increasing sprayed coating solution amount, with up to 91% of the particle pores being covered. The FIB-cross-sectioning technique using an ion beam of 2.50 nA for the first milling and 0.43 nA for polishing of the surface resulted in successful generation of cross-sections of representative particles with a visible particle core and coating layer. A coating layer thickness of approximately 700 nm was achieved on particles with sizes of below 45 μm.

关键词： Coating layer thickness Focused ion beam Microparticle Aerogel Spouted bed Dilute spouting

来源：

维普期刊数据库评论

在线全文

维普期刊数据库

学校读者我要写书评

暂无评论

Optimization of Draft Tube Position in a Spouted Bed Reactor using Response Surface Methodology

引用

Advances in Materials Physics and Chemistry 2012年第4期2卷 233-236页

作者： Elaheh Baghban Arjomand Mehrabani-Zeinabad Chemical Engineering Department Isfahan University of Technology Isfahan Iran

Optimization of draft tube position in a spouted bed reactor used for treatment of wastewater containing low concentration of heavy metals is investigated in this paper. Response surface methodology is used to optimize the draft tube height, the draft tube width and the gap between the bottom of the draft tube and the inlet nozzle. It is observed that the draft tube with a height of 60 millimeter, width of 12 millimeter and the gap of 13 millimeter between its bottom and inlet nozzle, results in optimum value of minimum spouting velocity, measured 45 cubic centimeter per second (2.7 Liter per minute) .

关键词： Spouted Bed Draft Tube Minimum spouting Velocity Response Surface Methodology

来源：

维普期刊数据库评论

在线全文

维普期刊数据库

学校读者我要写书评

暂无评论

On the stabil让y of Wiirster fluid bed of pharmaceutical pellets

引用

Particuology 2019年第4期17卷 81-90页

作者： Mohammad Foroughi-Dahr Rahmat Sotudeh-Gharebagh Navid Mostoufi Multiphase Systems Research Lab School of Chemical Engineering College of Engineering University of Tehran P.O. Box 11365/4563 Tehran Iran

The flow of pharmaceutical pellets in a Wiirster fluid bed (WFB) was characterized by a frequency domain analysis of pressure fluctuations. Pellets with a diameter of 0.780 mm and density of 1.225 kg/m^3 were used in the experiments. Different flow structures were identified in the bed, including bulk movement of pellets in the annulus (fspouting velocity was also measured experimentally. Effects of bed height, distanee of the entrainment zone, and distributor hole pitch on minimum spouting velocity were investigated. It was Found that the minimum spouting velocity increased with increasing bed height and distance of the entrainment zone while it decreased w ith in creasing distributor hole pitch. A correlation was developed for estimating the minimum spouting velocity in WFBs containing pharmaceutical pellets. The correlation fit the experimental data satisfactorily. Studying the WFB hydrodynamics and determining the minimum spouting velocity provides information that can be used to properly design, operate, and scale up such systems.

关键词： Pharmaceutical pellets Wiirster fluid bed Draft tube Minimum spouting velocity

来源：

维普期刊数据库评论

在线全文

维普期刊数据库

学校读者我要写书评

暂无评论

欢迎您,

建议与咨询留下您的常用邮箱和电话号码，以便我们向您反馈解决方案和替代方法

时间限定

文献类型

馆藏选择

核心期刊

语言

文献类型

帮助

文字说明：

检索规则说明：

检索范例：

分类表

所选分类

限定检索结果

文献类型

馆藏范围

日期分布

学科分类号

主题

机构

作者

语言

在线全文

在线全文

在线全文

请选择保存的检索档案：

请选择收藏分类：

通借通还

欢迎您,

建议与咨询 留下您的常用邮箱和电话号码，以便我们向您反馈解决方案和替代方法

时间限定

文献类型

馆藏选择

核心期刊

语言

文献类型

帮助

文字说明：

检索规则说明：

检索范例：

分类表

所选分类

限定检索结果

文献类型

馆藏范围

日期分布

学科分类号

主题

机构

作者

语言

在线全文

在线全文

在线全文

请选择保存的检索档案： 新增检索档案 确定 取消

请选择收藏分类： 新增自定义分类 确定 取消

通借通还

建议与咨询留下您的常用邮箱和电话号码，以便我们向您反馈解决方案和替代方法

请选择保存的检索档案：

请选择收藏分类：