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Selecting the Technology of sodium silicate Modified Poplar with the Highest Performance by Fuzzy Orthogonal Method

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Journal of Renewable Materials 2023年第5期11卷 2399-2415页

作者： Xiaoqian Bi Pengfei Guan Ping Li Yuan Zhang Xingong Li Yingfeng Zuo College of Materials Science and Engineering Central South University of Forestry and TechnologyChangsha410004China College of Furniture and Art Design Central South University of Forestry and TechnologyChangsha410004China

sodium silicate modification can improve the overall performance of wood.The modification process has a great influence on the properties of modified wood.In this study,a new method was introduced to analyze the wood modification process,and the properties of modified wood were studied.Poplar wood was modified with sodium silicate by vacuum-pressure impregnation.After screening using single-factor experiments,an orthogonal experiment was carried out with solution concentration,impregnation time,impregnation pressure,and the cycle times as experimental factors.The modified poplar with the best properties was selected by fuzzy mathematics and characterized by SEM,FT-IR,XRD and TG.The results showed that some lignin and hemicellulose were removed from the wood due to the alkaline action of sodium silicate,and the orderly crystal area of poplar became disorderly,resulting in the reduction of crystallinity of the modified poplar wood.FT-IR analysis showed that sodium silicate was hydrolyzed to form polysilicic acid in wood,and structural analysis revealed the formation of Si-O-Si and Si-O-C,indicating that sodium silicate reacted with fibers on the wood cell wall.TG-DTG curves showed that the final residual mass of modified poplar wood increased from 25%to 67%,and the temperature of the maximum loss rate decreased from 343℃ to 276℃.The heat release and smoke release of modified poplar wood decreased obviously.This kind of material with high strength and fire resistance can be used in the outdoor building and indoor furniture.

关键词： Poplar wood sodium silicate impregnation modification fuzzy orthogonal method process optimization flame retardant

Effectiveness of sodium silicate as gangue depressants in iron ore slimes flotation

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International Journal of Minerals,Metallurgy and Materials 2011年第5期18卷 515-522页

作者： Danda Srinivas Rao Tadiparthi Venkata VijayaKumar Sripada Subba Rao Swarna Prabhakar Guntamadugu Bhaskar Raju National Metallurgical Laboratory-Madras Centre Council of Scientific and Industrial Research-Madras ComplexChennai 600 113India

The recovery of iron from the screw classifier overflow slimes by direct flotation was studied. The relative effectiveness of sodium silicates with different silica-to-soda mole ratios as depressants for silica and silicate bearing minerals was investigated. Silica-to-soda mole ratio and silicate dosage were found to have significant effect on the separation efficiency. The results show that an increase of Fe content in the concentrate is observed with concomitant reduction in SiO2 and A1203 levels when a particular type of sodium silicate at a proper dosage is used. The concentrate of 58.89wt% Fe, 4.68wt% SiO2, and 5.28wt% A1203 with the weight recovery of 38.74% and the metal recovery of 41.13% can be obtained from the iron ore slimes with 54.44wt% Fe, 6.72wt% SiO2, and 6.80wt% A1203, when NazSiO3 with a silica-to-soda mole ratio of 2.19 is used as a depressant at a feed rate of 0.2 kg/t.

关键词： iron ores sodium silicate depressants flotation

Determination of Iron in Layered Crystal sodium Disilicate and sodium silicate by Flame Atomic Absorption Spectrometry with Boric Acid as a Matrix Modifier

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Chinese Chemical Letters 2006年第6期17卷 809-812页

作者： Zhi Hua WANG Min CAI Shu Jun WANG State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical Technology Beijing 100029

The effects of matrix silicate and experimental conditions on the determination of iron in flame atomic absorption spectrometry （FAAS） were investigated. It was found that boric acid as a matrix modifier obviously eliminated silicate interference. Under the optimum operating conditions, the determination results of iron in layered crystal sodium disilicate and sodium silicate samples by FAAS were satisfactory. The linear range of calibration curve is 0-10.5 μg.mL^-1, the relative standard deviation of method is 1.2%-2.2%, the recovery of added iron is 96.0%- 101%, the sensitivity is 0.19 μg.mL^-l and the detection limit is 77 ng.mL^-1. The effect of the determination of iron of the standard curve method, standard addition calibration and colorimetry method was the same, but the first has the merits of rapid sample preparation, reduced contamination risks and fast analysis.

关键词： Layered crystal sodium disilicate sodium silicate flame atomic absorption spectrometry determination of iron boric acid.

Synergistic Inhibition Effect of sodium silicate and Acrylamide on the Corrosion of Carbon Steel in a High-concentration KCI Solution

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Chemical Research in Chinese Universities 2017年第1期33卷 100-106页

作者： ZHAO Jingmao ZHANG Manlu TIE Zhiwei College of Material Science and Engineering Beijing University of Chemical Technology Beijing 100029 P. R. China Beijing Key Laboratory of Electrochemical Process and Technology for Materials Beijing University of Chemical Technology Beijing 100029 P. R. China

The corrosion inhibition performances of sodium silicate（Na2SiO3） and acrylamide（AM） for Q235 carbon steel in a high-concentration KCl solution（25%, mass fraction） were investigated via static mass loss method, elec- trochemical measurements, scanning electron microscopy（SEM）, X-ray photoelectron spectroscopy（XPS） and Auger electron spectroscopy（AES）. AM shows poor inhibition performance, while Na2SiO3 exhibits a better inhibition per- formance. Moreover, the steel gains mass instead of losing mass in the presence of 0.5% Na2SiO3 and 0.5% AM, in- dicating that the corrosion is completely inhibited~ SEM analysis indicates that a compact protective film is formed on the steel surface by the combined use of inhibitors. Our results demonstrate that Na2SiO3 and AM could have a synergistic effect on steel corrosion in high concentrations of KCl. The synergistic inhibition mechanism is further conjectured by the XPS and AES analysis.

关键词： KCl solution sodium silicate Acrylamide synergistic inhibition effect Corrosion inhibitor

Evaluation of the effect of sodium silicate addition to mine backfill,Gelfill-Part 2:Effects of mixing time and curing temperature

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Journal of Rock Mechanics and Geotechnical Engineering 2015年第3期7卷 668-673页

作者： M.Kermani F.P.Hassani E.Aflaki M.Benzaazoua M.Nokken Mining Engineering Department McGill University Amirkabir University of Technology Universite du Quebec en Abitibi Temiscamingue Department of Building Civil & Environmental EngineeringConcordia University

The effects of mixing time and curing temperature on the uniaxial compressive strength （UCS） andmicrostructure of cemented hydraulic fill （CHF） and sodium silicate-fortified backfill （Gelfill） wereinvestigated in the laboratory. A series of CHF and Gelfill samples was mixed for time periods rangingfrom 5 min to 60 min and cured at temperatures ranging from 5 C to 50 C for 7 d, 14 d or 28 d.Increasing the mixing time negatively influenced the UCS of Gelfill samples, but did not have a detectableeffect on CHF samples. The curing temperature had a strong positive impact on the UCSs of both Gelfilland CHF. An elevated temperature caused rapid UCS development over the first 14 d of curing. Mercuryintrusion porosimetry （MIP） indicated that the pore size distribution and total porosity of Gelfill werealtered by curing temperature.

关键词： Gelfill Cemented hydraulic fill(CHF) sodium silicate Mercury intrusion porosimetry(MIP) Drainage

Wet reclamation of sodium silicate used sand and biological treatment of its wastewater by Nitzschia palea

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China Foundry 2012年第1期9卷 34-38页

作者： Wang Huafang Fan Zitian Yu Shaoqiang Liu Fuchu Li Xuejie State Key Laboratory of Material Process and Die and Mould Technology Huazhong University of Science and TechnologyWuhan 430074China

The massive amount of sodium silicate in the used sand was a pollution source,especially in the waste water from the wet reclamation of used sand.A new process of wet reclamation by biologically treating the waste water produced during the wet reclamation process of used sand was studied in the paper.In the work,the pre-cultivation of N.palea was performed firstly,and three different scrubbing solutions:(1) tap water,(2) modified medium for N.palea,and (3) filtrate of the broth treated by N.palea for 15 days,were used.The results of the primary investigation show that a de-skinning ratio of 90% is obtained when using the scrubbing solution containing modified medium for N.palea at the ratio 1:2 of sand and scrubbing solution,and the maximal concentrations of Na+ and SiO32are 1.49 g·L-1 and 0.51 g·L-1,respectively.The results of the optimal biomass,pH value decrease and Na+ and SiO32consumption indicate the optimal incubation conditions are at the irradiance of 5,000 lux and 25 oC.Using the filtrate of the broth treated by N.palea for 15 days as the scrubbing solution directly,a de-skinning ratio of 93% is the highest compared to the results of the tap water and the modified medium for N.palea.In the biological process using N.palea,less water is used and little wastewater is produced,which is advantageous to the purpose of green manufacturing and environmental protection.

关键词： sodium silicate used sand biological reclamation method N.palea

The effect of sodium silicate concentration on microstructure and corrosion properties of MAO-coated magnesium alloy AZ31 in simulated body fluid

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Journal of Magnesium and Alloys 2014年第1期2卷 72-77页

作者： B.Salami A.Afshar A.Mazaheri Department of Materials and Engineering Sharif University of TechnologyP.O.Box 11155-9466TehranIran

In recent years,magnesium and its alloys are considered as biodegradable implants.However magnesium implants may rapidly corrode before the natural healing process of the tissue is completed.In this investigation,micro arc oxidation process has been studied for avoiding primary corrosion of the magnesium alloy in simulated body fluid.Anodized coating was formed on AZ31 alloy in nontoxic silicate-alkaline solution at constant current.The effects of silicate concentration and conductivity of electrolyte solution on microstructure and corrosion properties of coating were evaluated.Scanning electron microscopy showed that a thick and condensed coating is formed after enough anodizing period.Energy dispersive spectroscopy showed that Si,O and Mg are the main components of the coating.Corrosion resistance of the coated and uncoated samples was assessed using potentiodynamic polarization and electrochemical impedance spectroscopy tests in SBF at 37℃ and pH of 7.4.Maximum corrosion resistance was achieved at 30 g/L concentration of sodium silicate in anodizing solution.It was observed that further increase in silicate concentration decreased the corrosion resistance.

关键词： Magnesium alloy Micro arc oxidation sodium silicate Conductivity Corrosion properties

The Use of sodium silicate as a Corrosion Inhibitor in a Saline Drilling Fluid: A Nonaggressive Option to the Environment

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Journal of Environmental Protection 2016年第13期7卷 2025-2035页

作者： Fernando B. Mainier Anne A. M. Figueiredo Alan Eduardo R. de Freitas André Armando M. de Alencar Junior Escola de Engenharia Universidade Federal Fluminense Niterói Brazil

The function of a corrosion inhibitor in drilling mud compositions is the corrosion protection of the equipment involved in drilling operations. Many compositions involve environmentally several products such as fatty amines of high molecular weight, polyoxylated amines, amides, imidazolines, nitrogen heterocyclic products, etc. The potential advantages of the use of silicates are the effective protection of carbon steel, especially in aerated saline fluids, low costs and non-aggressive behavior to environment. Gravimetric and electrochemical tests were carried out using an aerated solution of 3.5% NaCl and the addition of sodium silicate (Na2SiO3·9H2O) as a corrosion inhibitor at concentrations of 250 to 2000 mg/L. The efficiencies of the corrosion protection of carbon steel using silicate concentrations greater than 1250 mg/L were greater than 92%.

关键词： sodium silicate Corrosion Inhibitor Environment Aerated Saline Fluid Carbon Steel

Influence of Calcium Chloride and sodium silicate on Index and Engineering Properties of Bentonite

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Influence of Calcium Chloride and Sodium Silicate on Index a...