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Manganese removal from the Qiantang River source water by pre-oxidation:A case study

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Journal of Zhejiang University-Science A(Applied Physics & Engineering) 2009年第3期10卷 450-457页

作者： Jian-wen ZHU Zhen ZHANG Xiao-min LI Xin-hua XU Da-hui WANG Department of Environmental Engineering Zhejiang University Hangzhou 310027 China Hangzhou Water Group Company Ltd. Hangzhou 310009 China School of Bioscienee Taizhou University Linhai 317000 China

We evaluated several different pre-oxidation treatments, namely the introduction of either potassium permanganate (KMnO4), chlorine (Cl2), or both to remove manganese (Mn) from the Qiantang River source water. Our results showed that Mn removal percentages were 12.7%, 71.0%, 17.4% and 58.7% when none of the oxidants, KMnO4 only, Cl2 only, or both oxidants were added, respectively. Furthermore, a field study showed that when the available Mn concentration in the source water was 0.14 mg/L, it could be reduced to less than 0.05 mg/L when a solution of KMnO4 (0.47 mg/L) was added as the oxidant.

关键词： pre-oxidation Potassium permanganate (KMnO2) Chlorine (Cl2) Manganese (Mn) removal

Effect of pre-oxidation degree on gaseous reduction of pre-oxidized ilmenite concentrate by CO

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Journal of Iron and Steel Research International 2022年第6期29卷 881-890页

作者： Shi-qing Zhao Xiao-dong Lv Zhi-ming Yan Xue-wei Lv Wei Lv Chen-guang Bai College of Materials Science and Engineering Chongqing UniversityChongqing 400044China Advanced Manufacturing&Materials Centre University of WarwickCoventry CV47ALUK School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina

The effect of pre-oxidation degree of Panzhihua ilmenite concentrate on the gaseous reduction by carbon monoxide was *** raw ilmenite concentrates were pre-oxidized at 600,700,800,900,and 1000°C for 2 h,*** phase change,FeO content,and morphology after the oxidation at various temperatures were *** oxidation degree was calculated according to the change of FeO *** was performed on the oxidized ilmenite concentrate samples(oxidized at 600,800,and 1000°C)at 850,900,and 950°C,*** results show that the pre-oxidation of ilmenite concentrate can accelerate the reduction process:the higher pre-oxidation degree,the faster reduction *** high pre-oxidation degree of ilmenite concentrate is beneficial to accelerate the subsequent reduction process in two *** stages of the reduction process were divided via the first derivatives of reduction degree,and the reduction mechanism and apparent activation energy were discussed subsequently.

关键词： Ilmenite pre-oxidation Reduction Kinetic Titanium slag

Complete stabilization of severely As-contaminated soil by a simple H2O2 pre-oxidation method combined with non-toxic TMT-15 and FeCl3·6H2O

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International Journal of Minerals,Metallurgy and Materials 2019年第9期26卷 1105-1112页

作者： Chang-sheng Yue Ben Peng Wei Tian Guang-hua Lu Gui-bo Qiu Mei Zhang Central Research Institute of Building and Construction Co. Ltd.Metallurgical Corporation of China Group (MCC Group)Beijing 100088China National Engineering Research Center for Industrial Environmental Protection Beijing 100088China School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China

The stabilization of severely As-polluted soil has been a challenge, especially for the extremely toxic As(Ⅲ) contaminants. In this study, soil with a high As concentration(26084 mg/kg) was availably stabilized by a H2O2 pre-oxidation assisted TMT-15(Na3S3C3N3 solution with a mass fraction of 15%) and FeCl3·6 H2O stabilization method. The results showed that the combination of the two stabilizers(i.e., TMT-15 and FeCl3·6 H2O) presented a better stabilization behavior than either stabilizer used individually. The use of the H2O2 pre-oxidation assisted TMT-15 and FeCl3·6 H2O stabilization approach not only converted the As(Ⅲ) to As(Ⅴ) but also reduced the toxic leaching concentration of As to 1.61 mg/L, which is a safe level, when the additions of TMT-15 and FeCl3·6 H2O were 2 mL and 0.20 g, respectively. Thus, using only a simple H2O2 pre-oxidation to combine clean stabilization with non-toxic stabilizers TMT-15 and FeCl3·6 H2O could render the severely As-contaminated soil safe for disposal in a landfill.

关键词： severely As-contaminated soil non-toxic stabilizers combining stabilization pre-oxidation

Impact of pre-oxidation on the formation of byproducts in algae-laden water disinfection:Insights from fluorescent and molecular weight

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Journal of Environmental Sciences 2022年第7期34卷 21-27页

作者： Da Sheng Lingjun Bu Shumin Zhu Yangtao Wu Jue Wang Nan Li Shiqing Zhou Key Laboratory of Building Safety and Energy Efficiency Ministry of EducationDepartment of Water Engineering and ScienceCollege of Civil EngineeringHunan UniversityChangsha 410082China

pre-oxidation has been reported to be an effective way to remove algal cells in water, but the released algal organic matter (AOM) could be oxidized and lead to the increment in disinfection by-product (DBP) formation. The relationship between pre-oxidation and AOM-derived DBP formation needs to be approached more precisely. This study compared the impact of four pre-oxidants, ozone (O), chlorine dioxide (ClO), potassium permanganate(KMnO) and sodium hypochlorite (NaClO), on the formation of nitrogenous (N-) and carbonaceous (C-) DBPs in AOM chlorination. The characterization (fluorescent properties,molecular weight distribution and amino acids concentration) on AOM samples showed that the characterization properties variations after pre-oxidation were highly dependent on the oxidizing ability of oxidants. The disinfection experiments showed that Oincreased DBP formation most significantly, which was consistent with the result of characterization properties variations. Then canonical correspondent analysis (CCA) and Pearson’s correlation analysis were conducted based on the characterization data and DBP formation. CCA indicated that C-DBPs formation was highly dependent on fluorescent data. The formation of haloacetic acids (HAAs) had a positive correlation with aromatic protein-like component while trichloromethane (TCM) had a positive correlation with fulvic acid-like ***’s correlation analysis showed that low molecular weight fractions were favorable to form N-DBPs. Therefore, characterization data could provide the advantages in the control of DBP formation, which further revealed that KMnOand ClOwere better options for removing algal cells as well as limiting DBP formation.

关键词： Algal organic matters pre-oxidation Disinfection by-products

Hot Corrosion Behavior of Ti45Al8.5Nb Alloy: Effect of Anodization and pre-oxidation

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Acta Metallurgica Sinica(English Letters) 2022年第9期35卷 1531-1546页

作者： Hao-Jie Yan Jun-Jie Xia Lian-Kui Wu Fa-He Cao School of Materials Shenzhen Campus of Sun Yat-sen UniversityShenzhen518107China College of Materials Science and Engineering Zhejiang University of TechnologyHangzhou310014China

The hot corrosion behavior of Ti45 A18.5 Nb alloy was studied in the salt of Na_(2)SO_(4)and/or NaCl at 700℃.To improve the hot corrosion resistance,Ti45 A18.5 Nb alloy was anodized in fluorine-containing solution and pre-oxidized in *** showed that the combination of anodization and pre-oxidation can efficiently enhance the hot corrosion resistance of Ti45 A18.5 Nb alloy contaminated with Na_(2)SO_(4)or Na_(2)SO_(4)+NaCl *** is because anodization and pre-oxidation result in the formation of compact AlOlayer which can act as a diffusion barrier to prevent sulfur,chlorine,and oxygen from attacking the alloy,therefore providing good resistance against hot *** exposed to NaCl deposit,however,no obvious improvement was achieved on the hot corrosion behavior no matter the alloy was anodized or further pre-oxidized in air.

关键词： Hot corrosion TiAl alloy Anodization pre-oxidation Halogen effect

Behavior and mechanism of pre-oxidation improvement on fluidization in the fluidized reduction of titanomagnetite

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International Journal of Minerals,Metallurgy and Materials 2024年第11期31卷 2458-2465页

作者： Haoyan Sun Ajala Adewole Adetoro Zhiqiang Wang Qingshan Zhu State Key Laboratory of Mesoscience and Engineering Institute of Process EngineeringChinese Academy of SciencesBeijing 100190China School of Chemical Engineering University of Chinese Academy of SciencesBeijing 100049China Data Science AI modeling CentreUniversity of HullHull HU67RXUK

The direct reduction process is an important development direction of low-carbon ironmaking and efficient comprehensive utilization of poly-metallic iron ore,such as ***,the defluidization of reduced iron particles with a high metallization degree at a high temperature will seriously affect the operation of fluidized bed *** the pre-oxidation enhancing reduction and the particle surface modification of titanomagnetite,the behavior and mechanism of pre-oxidation improvement on fluidization in the fluidized bed reduction of titanomagnetite are systematically studied in this ***-oxidation treatment of titanomagnetite can significantly lower the critical stable reduction fluidization gas velocity to 0.17 m/s,which is reduced by 56%compared to that of titanomagnetite reduction without pre-oxidation,while achieving a metallization degree of>90%,Corresponding to the different reduction fluidization behaviors,three pre-oxidation operation regions have been divided,taking oxidation degrees of 26%and 86%as the *** on the particle surface morphology evolution in the pre-oxidation-reduction process,the relationship between the surface morphology of pre-oxidized ore and the reduced iron with fluidization properties is *** improving method of pre-oxidation on the reduction fluidization provides a novel approach to prevent defluidization by particle surface modification,especially for the fluidized bed reduction of poly-metallic iron ore.

关键词： fluidization direct reduction pre-oxidation titanomagnetite iron whisker

Sulfidization regulation of cuprite by pre-oxidation using sodium hypochlorite as an oxidant

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International Journal of Mining Science and Technology 2021年第6期31卷 1117-1128页

作者： Guang Han Shuming Wen Han Wang Qicheng Feng State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization Faculty of Land Resources EngineeringKunming University of Science and TechnologyKunming 650093China

The direct sulfidization of cuprite is inefficient because cuprite is a copper-oxide mineral with a strong surface *** this study,oxidant was used to modify cuprite surfaces to regulate the sulfidization of *** tests showed that the flotation recovery of pre-oxidized cuprite was nearly25% higher than that of direct sulfidization flotation,which indicates that the cuprite surface activity was enhanced after pre-oxidation by Cu(Ⅰ) species(weak affinity with sulfur ions) transformation to Cu(Ⅱ)species(strong affinity with sulfur ions).Zeta potential,scanning electron microscopy-energy dispersive X-ray spectroscopy,X-ray photoelectron spectroscopy,and time-of-flight secondary ion mass spectrometry results showed that pre-oxidation improved cuprite sulfidization and promoted the formation of copper-sulfide species on the cuprite *** mineral surface stability and thus,xanthate species adsorption on the cuprite surfaces were *** surface-adsorption measurements and infrared spectroscopy showed that a large amount of xanthate species was adsorbed onto the sulfidized cuprite surfaces after pre-oxidation,which enhanced the cuprite hydrophobicity and improved the cuprite flotation.

关键词： Cuprite pre-oxidation Enhanced sulfidization Xanthate adsorption

Structural regulation of coal-derived hard carbon anode for sodium-ion batteries via pre-oxidation

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Rare Metals 2024年第6期43卷 2585-2596页

作者： Meng-Yuan Su Kai-Yang Zhang Edison Huixiang Ang Xue-Li Zhang Yan-Ning Liu Jia-Lin Yang Zhen-Yi Gu Faaz A.Butt Xing-Long Wu Faculty of Chemistry Northeast Normal UniversityChangchun 130024China MOE Key Laboratory for UV Light-Emiting Materials and Technology.Northeast Normal University.Ministry of Education Changchun 130024China Natural Sciences and Science Education National Institute of EducationNanyang Technological UniversitySingapore 637616Singapore Materials Engineering Department NED University of Engineering and TechnologyKarachi 75300Pakistan

Hard carbon(HC)is broadly recognized as an exceptionally prospective candidate for the anodes of sodium-ion batteries(SIBs),but their practical implementation faces substantial limitations linked to precursor factors,such as reduced carbon yield and increased ***,a cost-effective approach is proposed to prepare a coal-derived HC anode with simple pre-oxidation followed by a post-carbonization process which effectively expands the d_(002)layer spacing,generates closed pores and increases defect *** these modifications,the resulting HC anode attains a delicate equilibrium between plateau capacity and sloping capacity,showcasing a remarkable reversible capacity of 306.3 mAh·g^(-1)at 0.03 A·g^(-1).Furthermore,the produ ced HC exhibits fast reaction kinetics and exceptional rate performance,achieving a capacity of 289 mAh·g^(-1)at 0.1 A·g^(-1),equivalent to~94.5%of that at 0.03 A·g^(-1).When implemented in a full cell configuration,the impressive electrochemical performance is evident,with a notable energy density of 410.6 Wh·kg^(-1)(based on cathode mass).In short,we provide a straightforward yet efficient method for regulating coal-derived HC,which is crucial for the widespread use of SIBs anodes.

关键词： Sodium-ion batteries Hard carbon Anode Coal pre-oxidation

Effect of chloride ion on bacterial pre-oxidation of arsenic-containing gold concentrate

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Journal of Central South University 2011年第5期18卷 1418-1424页

作者：杨玮覃文庆刘瑞强任允超 School of Resources Processing and Bioengineering Central South University Refinery of Shandong Gold Mining Co. Ltd. Engineering Design and Research Co. Ltd.Shandong Gold Corporation

The bacterial pre-oxidation process of arsenic-containing gold concentrates and the bacterial activity under different chloride ion concentrations were studied by using a mixture of thermophilic strains TCJ domesticated in *** experimental result shows that with different samples and leaching systems,the adaptability and Cl- tolerance of bacteria are different,and that appropriate chloride ion concentration is conductive to bacterial oxidation,while higher chloride ion concentration will inhibit the bacterial activity and affect the pre-oxidation *** the present production conditions,TCJ can adapt to the changes of water quality in the source of water and its critical chloride ion tolerance value is 2.7 g/L.

关键词： chloride ions arsenic-containing gold concentrate pre-oxidation bacterial adaptation critical concentration