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Influence of Microstructures on polarization resistance and Hydrogen-Induced Cracking of a Micro-Alloyed Steel Submitted to Different Cooling Rates

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Journal of Iron and Steel Research International 2011年第S1期18卷 168-172页

作者： González M R Martins de Araújo D S Goldenstein H Alonso-Falleiros N Departamento de Engenharia Metalúrgica e de Materiais EscolaPolitécnicaUniversidade de Sao Paulo-SP-Brasil

The effect of different microstructures on the polarization resistance (Rp) and the hydrogen-induced cracking (HIC) of a micro-alloyed steel austenitized and submitted to different cooling rates was *** 19.1 x 6 x 2 mm,containing the whole thickness of the plate were extracted from a 20 mm plate and heat treated on a quenching dilatometer,were submitted to Rp and HIC corrosion *** Rp and HIC tests followed as close as possible ASTM G59 and NACE standard TM0284-2003,in this case,modified only with regard to the size of the *** samples transformed from austenite by a slow cooling (cooling rate of 0.5℃.s-1) showed higher susceptibility to hydrogen-induced cracking,with large cracks in the middle of the sample propagating along segregation bands,corresponding to the centerline of the plate *** cooling rates of 10℃.s-1,only small cracks were found in the matrix and micro cracks nucleated at non-metallic *** higher cooling rates (40℃.s-1) very few small cracks were detected,linked to non-metallic *** result suggests that structures formed by polygonal structures and segregation bands (were eutectoid microconstituents predominate) have higher susceptibility to *** predominantly formed by acicular ferrite make it difficult to propagate the cracks among non-oriented and interlaced acicular ferrite *** segregation bands containing eutectoid products also help inhibit cracking and crack propagation;segregation bands can function as pipelines for hydrogen diffusion and offer a path of stress concentration for the propagation of cracks,frequently associated to non-metallic *** resistance essays performed on the steel in theas received condition,prior to any heat treatment,showed larger differences between the regions of the plate,with a considerably lower Rp in the *** austenitization heat treatments followed by cooling rates of 0.5 e 10℃.s-1 made more uniform the

关键词： hydrogen induced cracking polarization resistance micro-alloyed steel control cooling

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Improved cell performance and sulphur tolerance using A-site substituted Sr_(2)Fe_(1.4)Ni_(0.1)Mo_(0.5)O_(6-δ)anodes for solid-oxide fuel cells

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Clean Energy 2023年第1期7卷 70-83页

作者： Haixia Li Wanhua Wang Jie Lin Ka-Young Park Taehee Lee Andreas Heyden Dong Ding Fanglin Chen Department of Mechanical Engineering University of South CarolinaColumbiaSC29208USA Department of Chemical Engineering University of South CarolinaColumbiaSC29208USA Energy&Environmental Science and Technology Idaho National LaboratoryIdaho FallsID83401USA

Solid-oxide fuel cells(SOFCs)offer great promise for producing electricity using a wide variety of fuels such as natural gas,coal gas and gasified carbonaceous solids;however,conventional nickel-based anodes face great challenges due to contaminants in readily available fuels,especially sulphur-containing ***,the development of new anode materials that can suppress sulphur poisoning is crucial to the realization of fuel-flexible and cost-effective *** this work,La_(0.1)Sr_(1.9)Fe_(1.4)Ni_(0.1)Mo_(0.5)O_(6-δ)(LSFNM)and Pr_(0.1)Sr_(1.9)Fe_(1.4)Ni_(0.1)Mo_(0.5)O_(6-δ)(PSFNM)materials have been synthesized using a sol-gel method in air and investigated as anode mater-ials for *** nanoparticle-decorated ceramic anodes were obtained by the reduction of LSFNM and PSFNM in H_(2)at 850℃,forming a Ruddlesden-Popper oxide with exsolved FeNi3 bimetallic *** electrochemical performance of the Sr_(2)Fe_(1.4)Ni_(0.1)Mo_(0.5)O_(6-δ)ceramic anode was greatly enhanced by La doping of A-sites,resulting in a 44%decrease in the polarization resistance in reducing *** maximum power densities of Sr-and Mg-doped LaGaO_(3)(LSGM)(300μm)electrolyte-supported single cells with LSFNM as the anode reached 1.371 W cm^(-2)in H_(2)and 1.306 W cm^(-2)in 50 ppm H_(2)S-H_(2)at 850℃.Meanwhile,PSFNM showed improved sulphur tolerance,which could be fully recovered after six cycles from H_(2)to 50 ppm H_(2)S-H_(2)*** study indicates that LSFNM and PSFNM are promising high-performance anodes for SOFCs.

关键词： A-site doping perovskite Ruddlesden-Popper structure alloy nanoparticles polarization resistance solid oxide fuel cells

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Influence of Surface Treatment on the Corrosion resistance of Stainless Steel in Simulated Human Body Environment

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Journal of Materials Science & Technology 2009年第5期25卷 611-614页

作者： Esmaeil Jafari Mohammad Jafar Hadianfard Dept.of Materials Science and Engineering

In the present research, the influence of chromium enrichment by surface treatment on corrosion resistance of type 316L stainless steel in body environment was investigated. For this study, weight loss test during 18 months, cyclic and liner polarization tests before and after surface treatment and metallography by electron and light microscopy were used to evaluate the effectiveness of the proposed method. In addition, X-ray photoelectron spectroscopy （XPS） method was used to determine the chromium concentration in the surface layer after surface treatment. Results show that the surface treatment has improved corrosion resistance of the type 316L stainless steel in body environment.

关键词： Surface treatment Corrosion Passive film polarization resistance

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Corrosion influence on surface appearance and microstructure of compo cast ZA27/SiC_p composites in sodium chloride solution

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Transactions of Nonferrous Metals Society of China 2016年第6期26卷 1512-1521页

作者： Biljana BOBIC Jelena BAJAT Ilija BOBIC Bore JEGDIC Institute of Chemistry Technology and Metallurgy University of Belgrade Belgrade 11000 Serbia Faculty of Technology and Metallurgy University of Belgrade Belgrade 11000 Serbia "Vinca" Institute of Nuclear Sciences University of Belgrade Belgrade 11000 Serbia

The influence of corrosion on the surface appearance and microstructure of particulate ZA27/SiCp composites was examined after 30 d immersion in a sodium chloride solution with the access of atmospheric oxygen. The composites with different contents of SiC micro-particles were synthesized via compo casting. Microstructural studies by means of optical microscopy （OM） and scanning electron microscopy （SEM） showed that corrosion occurred in the composite matrices, preferentially in regions of the η phase, rich in zinc. The corrosion processes did not affect the silicon carbide particles incorporated in the matrix alloy. According to the results of electrochemical polarization measurements, an increase in the content of SiC particles in the composite matrice has led to the lower corrosion resistance in the composites.

关键词： metal-matrix composites ZA27 alloy corrosion microstructure polarization resistance corrosion rate

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Effect of purification treatment on corrosion resistance of Mg-Gd-Y-Zr alloy

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Transactions of Nonferrous Metals Society of China 2011年第4期21卷 949-954页

作者：王杰杨院生童文辉中国科学院金属研究所沈阳110016

Mg-Gd-Y-Zr alloys were purified by filtering purification with and without vacuum. The type, morphology, size distribution and volume fraction of inclusion were analyzed with OM and SEM. The effect of inclusion in Mg-Gd-Y-Zr alloys on anticorrosion ability was investigated with salt spray test and electrochemical test. The results show that the inclusions in the alloy can be removed effectively by filtering purification. The average size of inclusions in the alloys is decreased from 12.7 μm to 2.0 μm and the volume fraction of inclusions is reduced from 0.30% to 0.04%. With the decrease of the size of inclusions in the alloys, the corrosion rate of the alloys decreases dramatically from 38.8 g/（m 2 ·d） to 2.4 g/（m 2 ·d） in the salt spray test. The corrosion potential increases while the corrosion current decreases and the polarization resistance increases in the electrochemical tests, which indicates that the anticorrosion ability is improved.

关键词： Mg-Gd-Y-Zr alloy filtering purification inclusion corrosion rate polarization curve polarization resistance

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