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Design and Development of Composite plywood that Integrates Fire Resistance,Water Resistance and Wear Resistance

Journal of Renewable Materials 2023年第5期11卷 2333-2344页

作者： Xingyu Liang Xiaoyu Gu Myint Myint Paing Hsu Yuhang He Rongzhuo Zhang Conghui Cai Zheng Wang College of Materials Science and Engineering Nanjing Forestry UniversityNanjing210037China College of Civil Engineering Nanjing Forestry UniversityNanjing210037China Jiangsu Shancong Wood Co. Ltd.Lianyungang222505China

In order to improve the fire resistance,water resistance and wear resistance of ordinary plywood products in the wood processing industry,three composite structures of plywood products S1,S2 and S3 were designed in this paper,and a reasonable production process was proposed.Through the physical and mechanical properties and fire resistance testing and technical and economic analysis,the applicability of composite plywood was evaluated.The results of the study showed that the physical mechanics of the three kinds of composite structure plywood met the standard requirements,and their fire resistance was far better than that of ordinary plywood.Among them,the S1 structural board had the best overall physical and mechanical properties.The S3 structural board showed the best fire resistance,which was about 1.9 times more than that of ordinary plywood,and the added cost was the lowest.The thin cork board added to the S2 structural board had poor fire performance since the air in the cork board cavities had a certain combustion-supporting effect,which inhibited the fire resistance of high-pressure laminate(HPL)layer.Moreover,the additional cost of the S2 board was the highest,and its comprehensive performance was the worst.The S3 structural plywood product composed of HPL fireproof board with a thickness of about 1 mm in the surface layer and ordinary plywood with a thickness of about 12 mm in the core layer was the most cost-effective product,which could meet the needs of various fields such as construction,home furnishing,decoration and transportation.

关键词： Wear resistance plywood structural design and development physical and mechanical properties fire resistance

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Curing Process of Phenol Formaldehyde Resin for plywood under Vacuum Conditions

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Journal of Renewable Materials 2023年第9期11卷 3447-3461页

作者： Guobing Xiong Lu Hong Zehui Ju Xiaoning Lu Juwan Jin College of Furnishings and Industrial Design Nanjing Forestry UniversityNanjing210037China School of Forestry&Landscape Architecture Anhui Agricultural UniversityHefei230036China College of Materials Science and Engineering Nanjing Forestry UniversityNanjing210037China

The study characterized the curing behaviors of phenol formaldehyde(PF)resin under different vacuum degrees and explored the properties of 9-ply plywood panels hot-pressed under both vacuum and atmospheric conditions.The changes in core temperature and moisture content of the plywood mats during hot pressing were investigated as well.It was found that the gel times and gel temperatures of PF resin decreased with the increase of vacuum degree using a self-made device.FTIR spectra indicated the degree of polycondensation of hydroxymethyl gradu-ally increased with the increase in temperature.It was also observed that a higher degree of vacuum led to a slower polycondensation reaction rate of PF resin.During different hot-pressing processes,the bonding strengths in the innermost and uppermost gluelines of the vacuum hot-pressed plywood panels were up to 30%–50%higher than their counterparts of conventional hot-pressed products.A less difference in the bonding strengths between these two gluelines was also observed for vacuum hot-pressed products.In addition,the core of vacuum hot-pressed plywood was found to have a greater heating rate and higher temperature at thefinal stage of hot pressing,which was beneficial to cure the PF resin.The results from this study indicate a promising potential of introducing a vacuum during hot pressing to improve the quality and productivity of plywood products and provide a basis for adopting vacuum to hot press wood composites.

关键词： Phenol formaldehyde resin vacuum gel time FTIR plywood bonding strength

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Synthesis of Lignin-Based Polyacid in an Acidic Ionic Liquid: A Green Method to Improve the Performance of Lignin as Catalyst in Urea-Formaldehyde Resin

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Journal of Renewable Materials 2022年第2期10卷 237-246页

作者： Hamed Younesi-Kordkheili Antonio Pizzi Department of Wood and Paper Sciences Faculty of Natural ResourcesSemnan UniversitySemnanIran LERMAB University of LorraineEpinalFrance

The aim of this research was to investigate the effect of ionic liquid treated lignin-based polyacid as a catalyst for urea-formaldehyde(UF)resins.Esterification of lignin was carried out,without any catalyst,with anhydride maleic and 1-butyl-3-methylimidazolium hydrogen sulfate[Bmim][HSO 4]as acidic ionic liquid to form maleated lignin-based polyacids(MA-IL).The performance of MA-IL as UF resin catalyst was respectively compared to hyroxymethylated lignin-based polyacid(MA-HL)and to NH 4 Cl.The FTIR analysis indicated that the propor-tion of-COOH and C-O bonds increased due to the esterification of lignin with ionic liquid rather than its hyr-oxymethylation.Physicochemical tests indicated that the gelation time of the UF resin was shorter by adding MA-IL when compared to NH 4 Cl and MA-HL,respectively.DSC analysis showed that the addition of MA-IL significantly decreased the temperature peak(Tp)of the UF resin;as the Tp of the UF resin with 2 wt%MA-IL was lower than with MA-HL and NH 4 Cl,respectively.The panel test results of plywood bonded with a UF resin with a MA-IL level increasing from 1%to 3%,effectively improved the mechanical strength,water resistance and formaldehyde emission even higher than with MA-HL and NH 4 Cl,respectively.

关键词： Lignin-based polyacid maleic anhydride ionic liquid esterification plywood

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MALDI ToF Investigation of the Reaction of Soy Protein Isolate with Glutaraldehyde for Wood Adhesives

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Journal of Renewable Materials 2023年第3期11卷 1439-1450页

作者： Qianyu Zhang Antonio Pizzi Hong Lei Xuedong Xi Ming Cao Long Cao Yunnan key Laboratory of Wood Adhesives and Glue Products College of Material Science and EngineeringSouthwest Forestry UniversityKunming650224China International Joint Research Center for Biomass Materials Southwest Forestry UniversityKunming650224China Universitéde Lorraine LERMAB-ENSTIB 27 rue Philippe SeguinEpinal88000France

Soy protein adhesives are currently a hot research topic in the wood panels industry for the abundant raw material reserves,reasonable price and outstanding environmental features.But their poor water resistance,low bonding strength and intolerance to mold are major drawbacks,so that proper modification before use is essential.Glutaraldehyde is one of the more apt cross-linking agents for soybean protein adhesives,which can effectively improve the bonding strength and water resistance of the adhesive.Equally,glutaraldehyde is also an efficient and broad-spectrum fungicide that can significantly improve the anti-fungal properties of a soy protein adhesive.In the work presented here,matrix assisted laser desorption ionization(MALDI-ToF)mass spectrometry and Fourier transform infrared spectroscopy techniques were used to analyze the reaction mechanism of glutaraldehyde cross-linking soybean protein.The results confirmed the reaction of the aldehyde group with amino groups of the side chains and the amide groups of the peptide linkages constituting the skeletal chain of the protein.The laboratory plywood and particleboard bonded with glutaraldehyde-soy bean protein adhesives were prepared to determine the adhesive bonding properties,the dry strength,24 h cold water soaking wet strength and 3 h hot water(63°C)wet strength of plywood were 2.03,1.13 and 0.75 MPa,respectively,which satisfied the requirements of industrial production.

关键词： Bio-based adhesives soy bean protein MALDI-ToF particleboard plywood

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Study of Burning Behaviors and Fire Risk of Flame Retardant plywood by Cone Calorimeter and TG Test

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Journal of Renewable Materials 2021年第12期9卷 2143-2157页

作者： Liping Yu Zhongyou Luo Lifen Li Xuedong Xi Zhigang Wu Bengang Zhang College of Forestry Guizhou UniversityGuiyang550025China Yunnan Provincial Key Laboratory of Wood Adhesives and Glued Products Southwest Forestry UniversityKunming650224China ENSTIB-LERMAB University of LorraineEpinal88051France IUT-LERMAB University of LorraineEpinal88000France

A flame retardant composition was prepared by using phosphoguanidine,guanidine sulfamate,disodium octaborate tetrahydrate and dodecyl dimethyl benzyl ammonium chloride.Veneers were immersed in such flame retardant mixture to prepare plywood.The combustion characteristics and thermal stability of plywood were assessed using a cone calorimeter and TG.Results showed that:(1)High concentration and loading of flame retardant were beneficial for the fire resistance of the plywood.(2)The limiting oxygen index(LOI)and residual mass of plywood processed using the flame retardant was increased by 87.52%and 58.66%compared to those of the untreated plywood,while the average heat release rate(av-HRR),total heat release(THR),effective heat of combustion(EHC),total smoke release(TSR),CO yield(COY),CO_(2) yield(CO_(2)Y)and oxygen consumption were decreased by 44.3%,82.9%,47.0%,86.0%,89.9%,50.1%and 83.1%,respectively.(3)Treated plywood which had a low fire growth index(FGI)displayed a later combustion heat release rate peak and slower flame spread than observed for the untreated material.Combustion of treated plywood displayed a higher fire performance index(FPI),indicating a longer time to ignition.This suggests that burning structures from this material would be subject to a longer time for escape from the structure and would present lower fire risk than similar structures containing treated plywood.(4)TG results demonstrated that the presence of the flame retardant can decrease the pyrolysis temperature for hemicellulose and cellulose,change the decomposition and reaction progress for plywood degradation and promote dehydration carbonization and accelerated charformation.Moreover,the formed char was more stable than that combustion of untreated plywood.(5)The flame retardant contains nitrogen(N),phosphorus(P),boron(B),chlorine(Cl)and guanidine(Gu)compounds.The adhesive also contains N and P compounds.These substances display flame resistance and supplement each other to generate flame retardance than any one used alone.By chan

关键词： Flame retardant plywood cone calorimeter burning behaviors fire risk

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LARIX GMELINI TANNIN-BASED ADHESIVE FOR plywood

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Journal of Northeast Forestry University 1994年第3期5卷 65-68页

作者：卢跃斌史强陈俊高振中 Northeast Forestry University China Xinlin Forest Bureau Heilongjiang Province Notheast Foresty University China

Larix tannin-phenol-formaldehyde (TPF) adhesive, having 60% by weight of phenol bcing replaced, was evaluated for its utilization in plywood. The kinetic characteristic of the TPF resin was investigated through differential scanning calorimetry (DSC) and the results obtained from the DSC scans show that the resin has a little bit different thermochemical behavior from that of phenol-formaldehyde (PF) resin. Two kinds of plywood panels wcre produced using the TPF adhesive in laboratory. The desired test results met the Chinese GB 9846-88 and ZB B70006-88, respectively, and the long assembly time of TPF resin in preparing plywood can be improved by mixing with the filler.All the properties of plywoods bonded with the TPF adhesive were compared with those obtaincd with synthetic PF adhesive.

关键词： Larix gmelini Tannin-phenol-formaldehyde Phenol-formaldehyde Differential scanning calorimetry plywood

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Bending moment resistance of dowel corner joints in case-type furniture under diagonal compression load

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Journal of Forestry Research 2014年第4期25卷 981-984页

作者： Mosayeb Dalvand Ghanbar Ebrahimi Mehdi Tajvidi Mohammad Layeghi Department of Wood and Paper Science and Technology College of Natural Resources University of Tehran Karaj Iran

We investigated bending moment resistance under diagonal compression load of comer doweled joints with plywood members. Joint members were made of ll-ply hardwood plywood of 19 mm thickness. Dowels were fabricated of Beech and Hornbeam species. Their diameters （6, 8 and 10 mm） and depths of penetration （9, 13 and 17 ram） in joint members were chosen variables in our experiment. By increasing the connector＇s diameter from 6 to 8 mm, the bending moment resistance under diagonal compressive load was increased, while it decreased when the diameter was increased from 8 to 10 mm. The bending moment re- sistance under diagonal compressive load was increased by increasing the dowel＇s depth of penetration. Joints made with dowels of Beech had higher resistance than dowels of Hornbeam. Highest resisting moment （45.18 N.m） was recorded for joints assembled with 8 mm Beech dowels penetrating 17 mm into joint members Lowest resisting moment （13.35 N.m） was recorded for joints assembled with 6 mm Hornbeam dowels and penetrating 9 mm into joint members.

关键词： bending moment resistance plywood dowel diameter cor-ner joint, case-type furniture

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Effect of moisture and fungal exposure on the mechanical properties of hem-fir plywood

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Journal of Forestry Research 2005年第4期16卷 299-300页

作者： WANG Wei-hong Scott Kent Camille Freitag Rorbert J. leichti Jeffrey J. Morrell Key Lab. of Bio-based Material Science and Technology of Ministry of Education Northeast Forestry University Harbin 150040 P. R. China Department of Wood Science and Engineering Oregon State University USA

Hem-fir plywood were exposed to two brown rot fungi, Gloeophyllum trabeum and Postia placenta, and one white rot fungus, Trametes versicolor, to investigate the effect of fungal decay on mechanical properties of plywood. Results showed that modulus of rupture （MOR） and modulus of elasticity （MOE） of hem-fir plywood declined significantly by inoculating fungi, and weight loss of sample had a modest decrease. The fungi also made a greater effect on MOR than on MOE. Of three fungi, Postia placenta caused a most significant weight loss, and Gloeophyllum trabeum resulted in a largest flexural properties loss. Substantial declines in MOR and MOE of hem-fir plywood were also observed when the plywood samples were stored under wet conditions over 15 weeks, even in the absence of fungal attack.

关键词： Fungus decay Weight loss Flexural properties Moist condition plywood MOR, MOE

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Reinforcement of Lignin-Based Phenol-Formaldehyde Adhesive with Nano-Crystalline Cellulose (NCC): Curing Behavior and Bonding Property of plywood

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Materials Sciences and Applications 2015年第6期6卷 567-575页

作者： Zhenbo Liu Yaolin Zhang Xiangming Wang Denis Rodrigue Key Laboratory of Bio-Based Material Science and Technology (Ministry of Education) & Northeast Forestry University Harbin China FPInnovations-Wood Products Quebec Canada Department of Chemical Engineering Laval University Quebec Canada

The curing behavior of lignin-based phenol-formaldehyde (LPF) resin with different contents of nano-crystalline cellulose (NCC) was studied by differential scanning calorimetry (DSC) at different heating rates (5, 10 and 20°C/min) and the bonding property was evaluated by the wet shear strength and wood failure of two-ply plywood panels after soaking in water (48 hours at room temperature and followed by 1-hour boiling). The test results indicated that the NCC content had little influence on the peak temperature, activation energy and the total heat of reaction of LPF resin at 5 and 10°C/min. But at 20°C/min, LPF0.00% (LPF resin without NCC) showed the highest total heat of reaction, while LPF0.25% (LPF resin containing 0.25% NCC content) and LPF0.50% (LPF resin containing 0.50% NCC content) gave the lowest value. The wet shear strength was affected by the NCC content to a certain extent. With regard to the results of one-way analysis of variance, the bonding quality could be improved by NCC and the optimum NCC content ranged from 0.25% to 0.50%. The wood failure was also affected by the NCC content, but the trend with respect to NCC content was not clear.

关键词： Lignin-Based Phenol-Formaldehyde Resin (LPF) Nano-Crystalline Cellulose (NCC) Curing Behavior Bonding Properties plywood

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Preparation of liquefied wood-based resins and their application in molding material

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Forestry Studies in China 2007年第1期9卷 51-56页

作者： Zhang Qiu-hui Zhao Guang-jie Yu Li-li Jie Shu-jun College of Material Science and Technology Beijing Forestry University Beijing 100083 E R. China Key Laboratory of Wood Science and Engineering ofBeijing Beijing 100083 E R. China

To investigate value in use of liquefied wood-based resin applications in molding material, Chinese fir （Cunninghamia lanceolata） and poplar （Populus tomentosa） wood meal were liquefied in phenol. The reactant was co-condensed with formaldehyde to obtain liquefied wood-based resin. For this paper, we investigated the characterization of the resin and its application in molding material. The result shows that the basic properties of liquefied wood-based resin were satisfactory; the bonding strength of plywood prepared with liquefied Chinese fir and liquefied poplar resin can reach 1.54 and 1.00 MPa, respectively. The compression strengths of the molding material prepared with two kinds of liquefied wood resin were 73.01 and 73.58 MPa, almost the same as that of PF resin molding material. The limiting volume swelling of molding material made with liquefied Chinese resin and liquefied poplar resin were 8.5% and 8.3%, thickness swelling rates of water absorption were 3.3% and 4.2%, and the maximum weight ratios of water absorption were 25.9% and 26.2%, respectively. The soil burial test result shows that the weight loss rate of the molding materials made with liquefied Chinese resin and liquefied poplar resin were 8.3% and 9.1% and that of the PF resin molding material was 7.9%. After the soil internment test, the reduction ratio of compression strength of the two kinds of molding material achieved 16.9% and 17.7%, while that of the PF resin molding material was 15.4%. The test results of wood fungi inoculation on the three surfaces of the molding material indicate the breeding rate of molding material prepared with liquefied Chinese resin and liquefied poplar resin were at level 4 and that of PF resin molding material was at level 1 of the ISO standard.

关键词： liquefied wood-based resin plywood molding material biodegradability

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