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Calibration of DEM Parameters to Simulate a planetary ball mill

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Advances in Materials Physics and Chemistry 2022年第7期12卷 155-162页

作者： Mohsen Mhadhbi Laboratory of Useful Materials National Institute of Research and Physicochemical Analysis Ariana Tunisia

planetary ball mill is a powerful tool, which has been used for milling various materials for size reduction. The discrete element method (DEM) was used to simulate the dynamics of particle processes in a planetary ball mill. This work includes the calibration of DEM parameters to simulate a planetary ball mill using EDEM Altair 2021.2 software, which provides both faster workflows and results. The iterative input parameters changed to a close correlation between the simulation and experimental results are attained. The results showed that the standard tests could be used to generate various experimental reference values for the calibration. The numerical modeling results agree with theexperimental, indicating that the calibrated parameters are accurate.

关键词： Discrete Element Method (DEM) Calibration planetary ball mill Parameters

Synthesis of Fe_3O_4 nanoparticles by wet milling iron powder in a planetary ball mill

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China Particuology 2007年第5期5卷 357-358页

作者： Ding Chen Song Ni Zhenhua Chen Institute for Materials Research Hunan University Changsha 410082 China

Fe3O4 nanoparticles with sizes ranging from 30 to 80 nm were synthesized by wet milling iron powders in a planetary ball mill. The phase composition and the morphologies of the as-synthesized products were measured by X-ray diffraction （XRD）, scanning electron microscopy （SEM） and transmission electron microscopy （TEM）. Nanosized Fe3O4 particles were prepared by wet milling metallic iron powder （-200 mesh, 99%） in a planetary ball mill equipped with stainless steel vials using iron balls under distilled water with a ball-to-powder mass ratio of 50：1 and at a rotation speed of 300 rpm. The use of the iron balls in this method played a key role in Fe3O4 formation. The present technique is simple and the process is easy to carry out.

关键词： Fe3O4 Wet milling planetary ball mill

Advantageous mechanochemical synthesis of copper(Ⅰ)selenide semiconductor,characterization,and properties

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Frontiers of Chemical Science and Engineering 2022年第3期16卷 433-442页

作者： Katarína Gáborová Marcela Achimovičová Michal Hegedüs Vladimír Girman Mária Kaňuchová Erika Dutková Institute of Geotechnics Slovak Academy of SciencesKošice04001Slovakia Institute of Metallurgy Faculty of MaterialsMetallurgy and RecyclingTechnical UniversityKošice04201Slovakia Synthon s.r.o.Blansko67801Czech Republic Faculty of Science Pavol JozefŠafárik UniversityKošice04154Slovakia Institute of Earth Resources Faculty of MiningEcologyProcess Control and GeotechnologiesTechnical UniversityKošice04200Slovakia

Copper(I)selenide-nanocrystalline semiconductor was synthesized via one-step mechanochemical synthesis after 5 min milling in a planetary ball mill.The kinetics of synthesis was followed by X-ray powder diffraction analysis and specific surface area measurements of milled 2Cu/Se mixtures.The X-ray diffraction confirmed the orthorhombic crystal structure of Cu_(2)Se with the crystallite size∼25 nm.The surface chemical structure was studied by X-ray photoelectron spectroscopy,whereby the binding energy of the Cu 2p and Se 3d signals corresponded to Cu^(+)and Se^(2−)oxidation states.Transmission electron microscopy revealed agglomerated nanocrystals and confirmed their orthorhombic structure,as well.The optical properties were studied utilizing ultraviolet-visible spectroscopy and photoluminescence spectroscopy.The direct bandgap energy 3.7 eV indicated a blue-shift phenomenon due to the quantum size effect.This type of Cu_(2)Se synthesis can be easily adapted to production dimensions using an industrial vibratory mill.The advantages of mechanochemical synthesis represent the potential for inexpensive,environmentally-friendly,and waste-free manufacturing of Cu_(2)Se.

关键词： Cu_(2)Se berzelianite nanocrystalline semiconductor mechanochemical synthesis planetary ball mill

Grinding Characteristic of Multi-walled Carbon Nanotubes-alumina Composite Particle

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Journal of Wuhan University of Technology(Materials Science) 2012年第6期27卷 1009-1013页

作者： B MUNKHBAYAR Nasan BAYARAA Hafizur REHMAN Junhyo KIM Hanshik CHUNG Hyomin JEONG Department of Energy and Mechanical Engineering Gyeongsang National University Department of Marine Engineering Mokpo National Maritime University Department of Energy and Mechanical Engineering Institute of Marine Industry Gyeongsang National University

The synthesis of new materials containing multi-walled carbon nanotubes （MWCNTs） and the microstructure of alumina particles were investigated and characterized. The MWCNTs and alumina particles were ground under both the dry and wet conditions with various rotation speeds （200 - 400 r/min） in planetary ball milling machine, and their combination characteristics were described. The experimental results were examined by scanning electron microscopy （SEM）, X-ray diffraction （XRD）, transmission electron microscopy （TEM） and particle sizing analysis （PSA）. SEM result revealed that the combination of MWCNTs - Alumina particles mixed quite well under both the dry and wet grinding with rotation speed of 400 r/rain. XRD characterization indicated the better result could get in ground samples at a rotation speed of 400 r/min. PSA result showed the particle size decreased with increase the grinding speeds. From the overall results, we observed that the grinding method can be used to synthesize new material with high efficiency.

关键词： carbon nanotubes alumina microstructure nanoparticle planetary ball mill

Modelling of the High-Energy ball milling Process

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Advances in Materials Physics and Chemistry 2021年第1期11卷 31-44页

作者： Mohsen Mhadhbi Laboratory of Useful Materials National Institute of Research and Physical-chemical Analysis Ariana Tunisia

In this paper, the milling parameters of high energy ball mill (Fritsch Pulverisette 7) like vial geometry, number and size of balls and speed of the mill were modelled and discussed. Simulations through discrete element method (DEM) provide correlation between the milling parameters. A mathematical model is used to improve and develop this process. The results show that the loss of powder mass can remarkably improve the performance of milling. The balls made of stainless-steel have a positive effect on the milling efficiency. The simulation shows that the high ball milling velocities can contribute to faster particle size reduction.

关键词： ball mill Modelling Discrete Element Method planetary ball mill High-Energy ball milling

Simulation of a Laboratory Scale ball mill via Discrete Element Method Modelling

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Advances in Materials Physics and Chemistry 2021年第10期11卷 167-175页

作者： Mohsen Mhadhbi Laboratory of Useful Materials National Institute of Research and Physicochemical Analysis Technopole Sidi Thabet Ariana Tunisia

Discrete Element Method (DEM) is a powerful tool for simulating different types of mills. It also used for computing different types of particles such as rocks, grains, and molecules. DEM has been widely used in the field of rock mechanics. In the present work, DEM approach is applied to model the milling media (powder particles and balls) inside a planetary ball mill and to estimate the distribution of particles of a dry powder during milling. In fact, the efficiency of the DEM strongly depends on the input parameters. The DEM simulation results indicated that DEM is a promising tool for the simulation of the dynamic particles motion and interactions within planetary ball mill. These results could be utilized to further develop the synthesis performance, anticipate the reaction, and reduce the wear in the dry milling reactions.

关键词： Modelling Discrete Element Method milling Media planetary ball mill Simulation