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Synthesis of NiMoO_4 nanoparticles by sol-gel method and their structural,morphological,optical,magnetic and photocatlytic properties

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Transactions of Nonferrous Metals Society of China 2017年第8期27卷 1785-1793页

作者： V.UMAPATHY P.NEERAJA A.MANIKANDAN P.RAMU Research and Development Centre Bharathiar UniversityCoimbatoreTamil Nadu 641046India Caplin Point Laboratories Limited Chennai 600017India Department of Chemistry NKR Government Arts College for WomenNamakkalTamil Nadu 637001India Department of Chemistry Bharath Institute of Higher Education and ResearchBharath UniversityChennai 600073India Department of Chemistry Meenakshi Academy of Higher Education and ResearchChennaiTamil Nadu 600078India

Nickel molybdate(NiMoO4)nanoparticles(NPs)were synthesized by sol-gel *** water as solvent providescrystalline *** nanocrystals were structurally characterized by X-ray diffraction,energy dispersive X-ray analysis(EDX),and Fourier transform infrared *** stoichiometry was confirmed by EDX *** size and shapewere observed by scanning electron microscopy(SEM)and transmission electron microscope(TEM).It was found that the obtainedNPs were pure and single phase crystalline with monoclinic *** optical properties were studied by ultraviolet-visiblediffuse reflectance spectroscopy(UV-Vis-DRS)and photoluminescence(PL)measurements at room *** magneticproperties were studied by vibrating sample magnetometer(VSM)and results showed superparamagnetic behavior of the *** activity of NiMoO4was *** photocatalytic activity of NiMoO4was enhanced with the additionof *** catalysts NiMoO4,TiO2and NiMoO4-TiO2nanocomposites(NC)were tested for photocatalytic degradation(PCD)of4-chlorophenol(4-CP).It was found that PCD efficiency of NiMoO4-TiO2NC was higher than that of pure NiMoO4and TiO2.

关键词： NiMoO4 TiO2 nanostructure sol-gel synthesis optical properties magnetic properties photo-catalysis monoclinic structure

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