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Preparation,Performance and Slag Resistant Mechanism of Low Thermal Conductivity microporous corundum

China's Refractories 2015年第4期24卷 23-30页

作者： FU Lyuping HUANG Ao GU Huazhi ZHANG Meijie LI Zhengkun ZHAO Yi The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and Technology Jiangsu Jingxin New Material Co. Ltd. Zhejiang Zili Co. Ltd.

The microporous corundum material was prepared using alumina micro-powder as the main raw material, alumina sol and starch as binders by a wet process, achieving the bulk density of 3.05 g · cm^-3, the apparent porosity of 9. 1%, the closed porosity of 12.3%, the median pore diameter of 0. 43 μm, and the thermal conductivity of 6. 5 W· m^-1· K^-1 at 800 ℃ which is 41.6% lower than that of common corundum. The slag resistance of the microporous corundum material was studied by immersion and compared with that of the common corundum aggregate, and the slag resistant mechanism of microporous corundum material was revealed. The results show that the slag resistance of the microporous corundum material is superior to that of the common corundum aggregate, the SEM and EDX show that on the reaction interface between microporous corundum and molten, slag, a continuous isolation layer with a large quantity of CA2 and CA6 columnar crystals is formed; while the common corundum aggregate reacts with the molten slag interface to form a discontinuous isolation layer of columnar crystals, through which a lot of molten slag corrodes or permeates into the aggregate. The mechanism is mainly that the microporous structure is more advantageous to nucleation and growth of CA2 and CA6 columnar crystals; in the reaction with the aggregate, the molten slag gets saturated and the critical solution thickness of the microporous corundum and the common corundum is 0. 16 μm and 0. 34 μm, respectively, this is caused by the smaller microporous corundum aggregate pores; and the smaller pores also increase the second phase ripening rate of microporous corundum, which is 9. 7 times of that of the common corundum.

关键词： low thermal conductivity microporous corundum preparation performance slag resistant mechanism

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Fabrication and Improving Properties of Lightweight Al_(2)O_(3)-MgO Castables for L adle Working Lining

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China's Refractories 2023年第1期32卷 6-13页

作者： WANG Zhiqiang LEI Zhongxing XU Guotao PENG Xiaoqian ZHU Boquan LIU Li GUO Zongqi Wugang Refractory Co. Ltd.Wuhan 430080China R&D Center of Wuhan Iron and Steel Co. Ltd.Baosteel Central Research InstituteWuhan 430080China Wuhan University of Science and Technology Wuhan 430081China Xi’an University of Architecture and Technology Xi’an 710055ChinaAbstract

Three lightweight Al_(2)O_(3)-MgO castables were fabricated with tabular alumina or microporous corundum as the aggregates,reactiveα-Al_(2)O_(3)micropowder,tabular alumina powder,and fused magnesia powder as the matrix,calcium aluminate cement as the binder,and MgO ultrafine powder(d50=5.4μm)and Al(OH)3 ultrafine powder(d50=8.2μm)as additives.The influence of aggregates and ultrafine powders on the properties,including pore size distribution,heat conductivity,thermal shock resistance,and slag resistance of lightweight refractory castables was investigated.The results show that the incorporation of microporous corundum reduces the bulk density of Al_(2)O_(3)-MgO castables,and MgO and Al(OH)3 ultrafine powders further increases the proportion of micropores in castables,which is beneficial to reducing the heat conductivity,and improving the thermal shock resistance and slag resistance of castables.Additionally,MgO ultrafine powder and Al(OH)3 ultrafine powder increase the fluidity and the strength of castables.

关键词： lightweight alumina-magnesia castables microporous corundum ultrafine powder1

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