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Influence of TiO2 on the melting property and viscosity of Cr-containing high-Ti melting slag

International Journal of Minerals,Metallurgy and Materials 2020年第3期27卷 310-318页

作者： Jing Ma Gui-qin Fu Wei Li Miao-yong Zhu School of Metallurgy Northeastern University

A study on the melting and viscosity properties of the chromium-containing high-titanium melting slag(CaO–SiO2–MgO–Al2O3–TiO2–Cr2O3) with TiO2 contents ranging from 38.63 wt% to 42.63 wt% was conducted. The melting properties were investigated with a meltingpoint apparatus, and viscosity was measured using the rotating cylinder method. The FactSage 7.1 software and X-ray diffraction, in combination with scanning electron microscopy–energy-dispersive spectroscopy(SEM–EDS), were used to characterize the phase equilibrium and microstructure of chromium-containing high-titanium melting slags. The results indicated that an increase in the TiO2 content led to a decrease in the viscosity of the chromium-containing high-titanium melting slag. In addition, the softening temperature, hemispheric temperature, and flowing temperature decreased with increasing TiO2 content. The amount of crystallized anosovite and sphene phases gradually increased with increasing TiO2 content, whereas the amount of perovskite phase decreased. SEM observations revealed that the distribution of the anosovite phase was dominantly influenced by TiO2.

关键词： titanium dioxide Cr-containing high-titanium melting slag melting property viscosity vanadium titanomagnetite

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Microstructure and melting properties of Ag–Cu–In intermediate-temperature brazing alloys

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Rare Metals 2015年第5期34卷 324-328页

作者： Xue Ma Liang-Feng Li Zu-Hua Zhang Hao Wang En-Ze Wang Tai Qiu School of Materials Science and Engineering Southwest University of Science and Technology Centre of Excellence in Engineered Fibre Composites (CEEFC) Faculty of Health Engineering and Sciences University of Southern Queensland College of Materials Science and Engineering Nanjing University of Technology

The microstructure and melting properties of ternary Ag-Cu-In intermediate-temperature alloys （400-600 ℃） prepared by electric arc melting were investigated in this work. The melting properties, phase compositions, microstructure and hardness were charac- terized by differential scanning calorimetry （DSC）, X-ray diffraction （XRD）, scanning electron microscopy （SEM） and micro-hardness tester, respectively. The results show that the melting properties, phase compositions, microstructure and hardness of Ag-Cu-In brazing alloys are substantially different when adding different levels of indium. Indium element could effectively reduce the melting temperatures of （Ag-Cu28）-xIn alloys, and the melting temperatures of （Ag-Cu28）-25In alloy are located at 497.86 and 617.48 ℃. When the indium content varies from 5 wt% and 10 wt%, the dominant phases in the alloys are Ag-rich and Cu-rich phases, and their granular crystals are smaller than 0.5 ktm. When the indium content is higher than 15 wt%, the phase compositions of the alloy are Ag4In and Cu11In9, and the microstructure exhibits dendritic crystals with a uniform distribution. The hardness of （Ag- Cu28）-xIn alloy decreases first and then increases with the content of indium increasing, and the highest hardness of （Ag-Cu28）-25In alloy is HV 266.0.

关键词： Ag-Cu-In alloy Arc melting melting property Microstructure Hardness

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维普期刊数据库

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Optimization of BF Slag for High Cr_2O_3 Vanadium-titanium Magnetite

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Journal of Iron and Steel Research International 2014年第2期21卷 144-150页

作者： Yong ZHANG Jue TANG Man-sheng CHU Yang LIU Shuang-yin CHEN Xiang-xin XUE School of Material and Metallurgy Northeastern University

In order to clarify the slag system of high Cr2O3 vanadium-titanium magnetite smelting in BF （blast furnace）, the melting properties of slag samples prepared by analytically pure reagents were measured. By means of orthogonal test synthetic weighted score method, the optimal slag for high Cr2O3 vanadium-titanium magnetite was obtained, which contained 10% MgO, 8% TiO2 and 15% Al2O3, with the binary basicity being 1.15. In addition, the effects of basicity, MgO, TiO2 and A12 03 on slag melting properties were investigated by single factor test, and the results showed that, with increasing the basicity or TiO2 content, melting temperature （Tin） increased, whereas initial vis- cosity （r/0） and high temperature viscosity （r/h） decreased. With increasing the MgO content, Tm decreased firstly and then increased. With increasing the Al2 O3 content, Tm increased, and η0 and r/h decreased firstly and then increased.

关键词： high Cr2 03 vanadium-titanium magnetite melting property slag optimization synthetic weighted scoremethod

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