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Preparation of Fe-As alloys by mechanical alloying and vacuum hot-pressed sintering:microstructure evolution,mechanical properties,and mechanisms

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Rare Metals 2024年第8期43卷 3876-3892页

作者： Fei Chai Fei-Ping Zhao Zhan Hu Shi-Yi Wen Ben-Hammouda Samia Ze-Lin Fu Xin-Ting Lai Yan-Jie Liang Xiao-Bo Min Li-Yuan Chai School of Metallurgy and Environment Central South UniversityChangsha 410083China Chinese National Engineering Research Center for Control&Treatment of Heavy Metal Pollution Institute of Environmental EngineeringCentral South UniversityChangsha 410083HunanChin State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083China Department of Building Civiland Environmental EngineeringConcordia UniversityMontreal H3G 1M8Canada

Arsenic materials have attracted great attention due to their unique ***,research concerning iron-arsenic(Fe-As) alloys is very scarce due to the volatility of As at low temperature and the high melting point of ***,a new Fe-As alloy was obtained by mechanical alloying(MA) followed by vacuum hot-pressed sintering(VHPS).Moreover,a systematic study was carried out on the microstructural evolution,phase composition,leaching toxicity of As,and physical and mechanical properties of Fe-As alloys with varying weight fractions of As(20%,25%,30%,35%,45%,55%,65%,and 75%).The results showed that pre-alloyed metallic powders(PAMPs) have a fine grain size and specific supersaturated solid solution after MA,which could effectively improve the mechanical properties of Fe-As alloys by VHPS.A high density(> 7.350 g·cm^(-3)),low toxicity,and excellent mechanical properties could be obtained for FeAs alloys sintered via VHPS by adding an appropriate amount of As,which is more valuable than commercial Fe-As *** Fe-25% As alloy with low toxicity and a relatively high density(7.635 g·cm^(-3)) provides an ultra-high compressive strength(1989.19 MPa),while the Fe-65% As alloy owns the maximum Vickers hardness(HVo.5 899.41).After leaching by the toxicity characteristic leaching procedure(TCLP),these alloys could still maintain good mechanical performance,and the strengthening mechanisms of Fe-As alloys before and after leaching were *** in the grain size,micro structure,and phase distribution induced significant differences in the compressive strength and hardness.

关键词： mechanical alloying Vacuum hot-pressed sintering High-pressure Arsenic-iron alloys mechanical properties

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Enhanced mechanical property by introducing bimodal grains structures in Cu-Ta alloys fabricated by mechanical alloying

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Journal of Materials Science & Technology 2024年第5期172卷 104-112页

作者： Ningyu Li Yongqin Chang Mingyang Li Yuxiang Chen Xinrui Luo Shichao Pei Fan Yang School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China Xi’an Rare Metal Materials Institute Co.Ltd Xi’an 710016China

Dispersion-strengthened copper alloys can achieve ultra-high strength,but usually at the expense of *** this study,a strategy for overcoming strength-ductility tradeoffof Cu alloys is realized through the introduction of bimodal grains ***-Ta alloys with only 0.5 at.%Ta content were successfully prepared by mechanical alloying combined with spark plasm *** samples prepared by one-step and two-step ball milling methods are named as Cu-Ta(Ⅰ)and Cu-Ta(Ⅱ),*** microstructural characterizations revealed that ultra-fine equiaxed grains with uniformly dispersed Ta precipitates were obtained in the Cu-Ta *** strength of 377 MPa for yield strength together with elongation of∼8%was obtained in Cu-Ta(Ⅰ).Bimodal grains structures composed of fine-grain zones and coarse-grain zones were successfully introduced into Cu-Ta(Ⅱ)by a two-step ball milling approach,and both yield strength(463 MPa)and elongation(∼15%)were significantly synergistic *** hardness values of both Cu-Ta(Ⅰ)and Cu-Ta(Ⅱ)were almost kept nearly constant with the increase of annealing time,and the softening temperatures of Cu-Ta(Ⅰ)and Cu-Ta(Ⅱ)are 1018 and 1013℃,reaching 93.9%and 93.5%T m of pure Cu(1083℃),*** reveals that the Cu-0.5 at.%Ta alloys exhibit excellent thermal stability and exceptional softening *** nanoclusters with semi-coherent structures play an essential role in enhancing the strength and microstructural stability of *** structures are beneficial to the activation of back stress strengthening and the initiation and propagation of microcracks,thus obtaining the extraordinary combination of strength and *** study provides a new way to fabricate dispersion-strengthened Cu alloys with high strength,high elongation,excellent thermal stability and softening resistance,which have potential application value in the field of the future fusion reactor.

关键词： Cu-Ta alloy mechanical alloying Ta precipitates Bimodal structures mechanical property

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Preparation of La Ni Based Alloys Used in Ni Metal Hydride Batteries by mechanical alloying

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Rare Metals 1997年第4期16卷 54-59页

作者：李东培应启明张健北京有色金属研究总院北京 The University of Western Australia 澳大利亚

La Ni based alloy powders used for Ni metal hydride batteries were synthesized by mechanical alloying starting from the elements. The electrical capacity obtained was up to 320 mAh/g. In addition, the comparison in the microstructure and electrochemical properties was made between the alloy powders produced by mechanical alloying and by melting. It was shown that mechanical alloying is promising in the preparation of practical RE hydrogen storage electrode materials.

关键词： La Ni alloy H storage electrode material Battery mechanical alloying

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Investigation of Nanostructured WC-Co Alloy Prepared by mechanical alloying

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Rare Metals 1998年第2期17卷 9-14页

作者：马学鸣嵇罡赵凌董远达上海大学材料科学与工程所上海

emented carbide of WCCo powder with crystalline size of about 10 nm was directly synthesized from elemental powders by mechanical alloying. Cold compacting was carried out at 800 Mpa using a manual uniaxial press. Sintering of the compacted samples was performed in vacuum in the temperature range of 1040～1350℃. The sintered density, crystallite size and microhardness of sintered samples were measured. The effects of a little VC addition on grain size, density and hardness of WCCo alloy were also presented.

关键词： Nanocrystalline WCCo mechanical alloying

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Phase Transformation in Al/Zn Multilayers during mechanical alloying

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Acta Metallurgica Sinica(English Letters) 2023年第10期36卷 1709-1718页

作者： Chen Chen Junjie Yu Jingyu Lu Jian Zhang Xuan Su Chen-Hao Qian Yulin Chen Weixi Ji Manping Liu Department of mechanical Engineering Jiangnan UniversityWuxi214122China Jiangsu Key Laboratory of Advanced Food Manufacturing Equipment and Technology Jiangnan UniversityWuxi214122China School of Materials Science and Engineering Jiangsu UniversityZhenjiang212013China

In this work,mechanical alloying of the alternating stacked pure Al and Zn thin foils was accomplished via high-pressure torsion(HPT).In the alloyed Al-Zn system,an exotic phase transformation from hexagonal close-packed(HCP)to face-centered cubic(FCC)was *** atomic-scale evolution process and underlying mechanism of phase transformation down to atomic scale are provided by molecular dynamics simulation and high-resolution transmission electron *** HCP→FCC phase transformation was attributed to the sliding of Shockley partial dislocations generated at the Al-Zn grain boundaries,which resulted in an[2110][011]and(0001)/(111)orientation relationship between the two *** work provides a new approach for the in-depth study of the solid phase transformation of Al-Zn alloys and also shed lights on understanding the mechanical properties of the HPT processed Al-Zn alloys.

关键词： High-pressure torsion Phase transformation Al/Zn multilayers mechanical alloying

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Evaluation of the microstructure,thermal and mechanical properties of Cu/SiC nanocomposites fabricated by mechanical alloying

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International Journal of Minerals,Metallurgy and Materials 2021年第3期28卷 475-486页

作者： Essam B.Moustafa Mohammed A.Taha mechanical Engineering Departments Faculty of EngineeringKing Abdulaziz UniversityJeddah 21589Saudi Arabia Solid State Physics Department National Research CentreEl Buhouth St.Dokki12622 GizaEgypt

Nano-sized silicon carbide(SiC:0wt%,1wt%,2wt%,4wt%,and 8wt%)reinforced copper(Cu)matrix nanocomposites were manufactured,pressed,and sintered at 775 and 875℃in an argon atmosphere.X-ray diffraction(XRD)and scanning electron microscopy were performed to characterize the microstructural *** density,thermal expansion,mechanical,and electrical properties were *** analyses showed that with increasing SiC content,the microstrain and dislocation density increased,while the crystal size *** coefficient of thermal expansion(CTE)of the nanocomposites was less than that of the Cu *** improvement in the CTE with increasing sintering temperature may be because of densification of the ***,the mechanical properties of these nanocomposites showed noticeable enhancements with the addition of SiC and sintering temperatures,where the microhardness and apparent strengthening efficiency of nanocomposites containing 8wt%SiC and sintered at 875℃were 958.7 MPa and 1.07 vol%^(−1),*** electrical conductivity of the sample slightly decreased with additional SiC and increased with sintering *** prepared Cu/SiC nanocomposites possessed good electrical conductivity,high thermal stability,and excellent mechanical properties.

关键词： copper matrix nanocomposites silicon carbide coefficient of thermal expansion elastic moduli electrical conductivity mechanical alloying

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Microstructure and mechanical properties of Ti-Cu amorphous coating synthesized on pure Cu substrate by mechanical alloying method

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Rare Metals 2020年第10期39卷 1222-1228页

作者： Cheng Chen Xiao-mei Feng Yi-fu Shen School of mechanical and Power Engineering Nanjing Tech UniversityNanjing 211800China College of Materials Science and Technology Nanjing University of Aeronautics and AstronauticsNanjing 210016China

mechanical alloying method was applied to fabricate coating with amorphous structure on pure Cu *** microstructure,the phase composition and the mechanical properties including microhardness and wear resistance of the coating were,respectively,characterized and *** results show that the coating is rough but *** has favorable adhesion to the *** coating is made up of an inner composite layer and an outer amorphous *** microhardness and the wear resistance of the pure Cu substrate are improved because of the bilayer *** formation mechanism of the coating was *** as-synthesized coating is considered to be effective to strengthen the surface of pure Cu substrate.

关键词： Coating Amorphous mechanical alloying Surface reinforcement

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Influence of B source materials on the synthesis of TiB_2-Al_2O_3 nanocomposite powders by mechanical alloying

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International Journal of Minerals,Metallurgy and Materials 2013年第12期20卷 1214-1220页

作者： Majid Abdellahi Javad Heidari Rahman Sabouhi Materials Engineering Department Islamic Azad University

An Al2O3-TiB2 nanocomposite was successfully synthesized by ball milling of Al, TiO2 and two B source materials of B2O3 （system （1）） and H3BO3 （system （2））. Phase identification of the milled samples was examined by Xray diffraction. The morphology and microstructure of the milled powders were monitored by scanning electron microscopy and transmission electron microscopy. It was found that the formation of this composite was completed after 15 and 30 h of milling time in systems （1） and （2）, respectively. More milling energy was required for the formation of this composite in system （2） due to the lubricant properties of HaBO3 and also its decomposition to HBO2 and B2O3 during milling. On the basis of X-ray diffraction patterns and thermodynamic calculations, this composite was formed by highly exothermic mechanically induced self-sustaining reactions （MSR） in both systems. The MSR mode took place around 9 h and 25 h of milling in systems （1） and （2）, respectively. At the end of milling （15 h for system （1） and 30 h for system （2）） the grain size of about 35-50 nm was obtained in both systems.

关键词： nanocomposites powders alumina titanium diboride mechanical alloying

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Fabrication of Bulk (Fe,Cr)_3Al/Al_2O_3 Intermetallic Matrix Nanocomposite Through mechanical alloying and Sintering

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Acta Metallurgica Sinica(English Letters) 2016年第10期29卷 911-919页

作者： Sayyed Erfan Aghili Mohammad Hossein Enayati Fathallah Karimzadeh Department of Materials Engineering Isfahan University of Technology

In the present study, （Fe,Cr）3Al/20 vol% A1203 nanocomposite was prepared through mechanochemical reactions during ball milling and successfully bulked using a combination of cold isostatic press and sintering at 1400℃ for 1 h. Two processing approaches were utilized to produce （Fe,Cr）3A1/A1203 nanocomposite： The first was milling of Fe, Cr, AI and Fe203, while the second one was milling of Fe, Cr, Al and Cr203, both in stoichiometric condition, to synthesize （Fe,Cr）3Al/20 vol% Al2O3. Structural changes of powder particles during mechanical alloying were studied by X-ray diffraction. The microstructure and the morphology of powder particles and bulk samples were also studied by scanning electron microscopy and transmission electron microscopy. Microstructural analysis showed that mechanochemical reactions took place during milling, and nanometric Al2O3 was uniformly distributed in the matrix. The results also showed that the second approach required a considerably higher milling time to produce （Fe,Cr）3Al/Al2O3 nanocomposite, as compared to the first one. For this reason, bulk samples were produced from the synthesized nanocomposite in the first approach. The microstructure of the sintered samples consisted of a network structure of （Fe,Cr）3Al and Al2O3 phases with superior mechanical properties.

关键词： Iron aluminide mechanical alloying Nanocomposite Mechanochemical treatment

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Microstructure, thermal properties, and corrosion behaviors of FeSiBAlNi alloy fabricated by mechanical alloying and spark plasma sintering

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International Journal of Minerals,Metallurgy and Materials 2016年第1期23卷 77-82页

作者： Hong-lei Wang Tai-xiu Gao Jia-zheng Niu Pei-jian Shi Jing Xu Yan Wang School of Materials Science and Engineering University of Jinan Shandong Provincial Key Laboratory of Preparation and Measurement of Building Materials University of Jinan

An equiatomic FeSiBAlNi amorphous high-entropy alloy （HEA） was fabricated by mechanical alloying （MA）. A fully amorphous phase was obtained in the FeSiBAlNi HEA after 240 h of MA. The bulk FeSiBAlNi samples were sintered by spark plasma sintering （SPS） at 520 and 1080℃ under a pressure of 80 MPa. The sample sintered at 520℃ exhibited an amorphous composite structure comprising solid-solution phases （body-centered cubic （bcc） and face-centered cubic （fee） phases）. When the as-milled amorphous HEA was consoli- dated at 1080℃, another fcc phase appeared and the amorphous phase disappeared. The sample sintered by SPS at 1080℃ exhibited a slightly higher melting temperature compared with those of the as-milled alloy and the bulk sample sintered at 520℃. The corrosion behav- iors of the as-sintered samples were investigated by potentiodynamic polarization measurements and immersion tests in seawater solution. The results showed that the HEA obtained by SPS at 1080℃ exhibited better corrosion resistance than that obtained by SPS at 520℃.

关键词： high entropy alloys spark plasma sintering mechanical alloying microstructure corrosion resistance

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