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Journal of Iron and Steel Research(International) 2022年第4期29卷 698-706页

作者： Sheng-rong Wang Jian-wei Yang Jian-ping Cao Shan Jiang Fei-fan Xu Shougang Research Institute of Technology of Shougang Group Co. Ltd.Beijing 100043China Beijing Key Laboratory of Green Recyclable Process for Iron&Steel Production Technology Beijing 100043China

The addition of Ni element into steel to prolong the service life of coated steel was investigated in marine atmospheric environment by laboratory simulated accelerated experiment.The scanning electron microscope and electron probe microanalysis combined with electrochemical impedance spectroscopy were used to characterize coated steel properties and examined the anti-corrosion performance.The results showed that 3 wt.%Ni-advanced steel(3Ni steel)substrate obviously delayed the failure time of coating compared to carbon steel,therefore prolonging the service life of coating on the steel.X-ray diffraction patterns for the corrosion products under the scratched coating on 3Ni steel exhibited that FeNi_(2)O_(4) and Fe_(2)O_(3) occurred in the corrosion product of 3Ni steel.It was also found that Ni element enriched in the product layer through analyzing the appearance and composition of corrosion products by electron probe micro-analysis.Chloride ions were blocked out of product by the enrichment of Ni element in rust layer.

关键词： 3wt.% Ni-advanced low-alloy steel Coating failure Service life Corrosion product Marine atmosphere

Effects of Zr addition on microstructure and toughness of simulated CGHAZ in high-strength low-alloy steels

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Journal of Iron and Steel Research(International) 2019年第10期26卷 1117-1125页

作者： Jin-wei Lei Kai-ming Wu Yu Li Ting-ping Hou Xing Xie RDKMisra The State Key Laboratory of Refractories and Metallurgy Hubei Province Key Laboratory of Systems Science on Metallurgical ProcessingInternational Research Institute for Steel TechnologyWuhan University of Science and TechnologyWuhan 430081HubeiChina Wuhan Second Ship Design and Research Institute Wuhan 430064HubeiChina Department of Metallurgical and Materials Engineering University of Texas at El PasoEl PasoTX 79968USA

The effect of Zr addition(0.005,0.013,and 0.054 wt.%)on the microstructure and toughness of simulated coarse-grained heat-affected zone in high-strength low-alloy steels was revealed using a Gleeble 2000 thermal simulator.It was observed that elongated MnS inclusions were formed in the lowest Zr-containing steel,while only pure equiaxed ZrO2 existed in the 0.054Zr steel(Zr content of 0.054 wt.%).Complex oxide-sulfide inclusions(ZrO2+MnS)with size of(1.40±0.25)μtm were formed in 0.013Zr steel(Zr content of 0.013 wt.%).The complex inclusions refined the prior austenite grain,and the nucleation of acicular ferrite was promoted compared to those of 0.005Zr steel(Zr content of 0.005 wt.%)and 0.054Zr steel.Consequently,the 0.013Zr steel possessed superior low-temperature impact toughness in relation to 0.005Zr and 0.054Zr steels.Thus,moderate Zr addition can be considered as an effective method to refine the structure and improve the mechanical properties of the coarse-grained heat-affected zone.

关键词： High-strength low-alloy steel Welding Heat-affected zone Heat input Zirconium addition

Hot Deformation and Corrosion Resistance of High-Strength low-alloy Steel

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Acta Metallurgica Sinica(English Letters) 2019年第4期32卷 495-505页

作者： Wilasinee Kingkam Cheng-Zhi Zhao Hong Li He-Xin Zhang Zhi-Ming Li College of Materials Science and Chemical Engineering Harbin Engineering University Key Laboratory of Superlight Materials and Surface Technology Ministry of EducationHarbin Engineering University College of Power and Energy Engineering Harbin Engineering University

The hot deformation characteristics and the corrosion behavior of a high-strength low-alloy(HSLA) steel were investigated at deformation temperatures ranging from 800 to 1100 ℃ and strain rates ranging from 0.1 to 10 s-1 using an MMS-200 thermal simulation testing machine. Based on the flow curves from the experiment, the effects of temperature and strain rate on the dynamic recrystallization behavior were analyzed. The flow stress decreased with increasing deformation temperature and decreasing strain rate. With the assistance of the process parameters, constitutive equations were used to obtain the activation energy and hot working equation. The hot deformation activation energy of HSLA steel in this work was 351.87 kJ/mol. The work hardening rate was used to determine the critical stress(strain) or the peak stress(strain). The dependence of these characteristic values on the Zener-Hollomon parameter was found. A dynamic recrystallization kinetics model of the tested HSLA steel was constructed, and the validity of the model was confirmed by the experimental results. Observation of the microstructures indicated that the grain size increased with increasing deformation temperature,which led to a lowered corrosion resistance of the specimens.

关键词： Dynamic recrystallization Potentiodynamic polarization Hot deformation Flow stress High-strength low-alloy steel

Microstructure and nanoindentation hardness of shot-peened ultrafine-grained low-alloy steel

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Journal of Iron and Steel Research(International) 2019年第5期26卷 472-482页

作者： Xiao-wei Feng Juan Xie Wen-ying Xue Yong-feng Shen Hong-bo Wang Zhen-yu Liu Institute of Systems Engineering of China Academy of Engineering Physics Mianyang 621999 Sichuan China Key Laboratory for Anisotropy and Texture of Materials (MOE) School of Materials Science and Engineering Northeastern University Shenyang 110819 Liaoning China The State Key Lab of Rolling and Automation Northeastern University Shenyang 110819 Liaoning China

The effect of shot peening (SP) on microstructure and hardness of ultrafine-grained (UFG) low-alloy steel was investigated. With increasing shot-peening time from 0.5 to 1.5 h, grain size of UFG low-alloy steel decreases from 400 to 280 nm at surface whilst that of the layer with a depth of 160μm decreases from (230 ± 15) to (75 ± 5) nm. Interestingly, nanoindentation shows that hardness increases linearly with increasing the SP duration, reaching a value as high as (7.10 ± 0.1) GPa at the depth of 160 μm after the SP duration of 1.5 h. The thickness of the SP treated layer is measured as^300 μm. The Hall-Petch (H-P) relationship was established for the hardening layer. Correspondingly, abrasion resistance should be ~51% higher than that of as-prepared UFG low-alloy steel. As shown in SP processing, grain refinement is the key factor responsible for the strengthening of the studied steel.

关键词： low-alloy steel Shot peening Grain refinement Nanoindentation Hardness

Effect of Heat Treatment Parameters on the Mechanical and Microstructure Properties of low-alloy Steel

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Journal of Surface Engineered Materials and Advanced Technology 2015年第4期5卷 214-227页

作者： Mohamed H. Frihat Mechanical Engineering Department Al-Hsoun University College Al-Balqa Applied University Irbid Jordan

This study examines the effect of heat treatment at three different temperatures of 800°C, 950°C and 1100°C on the microstructure and mechanical properties of low-alloy steel with an addition of manganese, chrome and lead. To determine an impact of the applied heat treatment operations, testing of mechanical properties and microstructural examinations of the steel with 0.23%, 0.24%, 0.29% and 0.31% C were conducted. This work shows that the mechanical strengths of the alloy steel are improved with increasing the heat treatment temperature. In addition, the microstructure trends toward recrystallized ferrite grains as the heat treatment temperature increases.

关键词： low-alloy Steel Heat Treatment Microstructure Mechanical Properties

High-resolution Transmission Electron Microscopy Characterization of the Structure of Cu Precipitate in a Thermal-aged Multicomponent Steel

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Chinese Journal of Mechanical Engineering 2019年第5期32卷 117-124页

作者： Lizhan Han Qingdong Liu Jianfeng Gu Institute of Materials Modification and Modelling School of Materials Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China Collaborative Innovation Center for Advanced Ship and Deep-Sea Exploration Shanghai Jiao Tong UniversityShanghai 200240China

High-dispersed nanoscale Cu precipitates often contribute to extremely high strength due to precipitation hardening,and whereas usually lead to degraded toughness for especially ferritic steels.Hence,it is important to understand the formation behaviors of the Cu precipitates.High-resolution transmission electron microscopy(TEM)is utilized to investigate the structure of Cu precipitates thermally formed in a high-strength low-alloy(HSLA)steel.The Cu precipitates were generally formed from solid solution and at the crystallographic defects such as martensite lath boundaries and dislocations.The Cu precipitates in the same aging condition have various structure of BCC,9 R and FCC,and the structural evolution does not greatly correlate with the actual sizes.The presence of different structures in an individual Cu precipitate is observed,which reflects the structural transformation occurring locally to relax the strain energy.The multiply additions in the steel possibly make the Cu precipitation more complex compared to the binary or the ternary Fe-Cu alloys with Ni or Mn additions.This research gives constructive suggestions on alloying design of Cu-bearing alloy steels.

关键词： Cu precipitate High-resolution transmission electron microscopy Thermal aging High-strength low-alloy steel

Effect of Nb on corrosion behavior of inner bottom plate of cargo oil tankers

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Journal of Iron and Steel Research(International) 2019年第6期26卷 611-620页

作者： Xiang-yu Xu Long Tian Yun Zhou Ming-yu Sun Xue-min Wang Cheng-jia Shang R.D.K. Misra Collaborative Innovation Center of Steel Technology University of Science and Technology Beijing Beijing 100083 China Tianjin Long March Launch Vehicle Manufacturing Co. Ltd. Tianjin 300462 China Institute of Research of Iron and Steel (IRIS) Sha-steel Zhangjiagang 215625 Jiangsu China Center for Structural and Functional Materials Research and Innovation Department of Metallurgical and Materials Engineering University of Texas at El Paso El Paso TX 7996& USA

The effect of Nb on the corrosion resistance of steels in simulating an oil-corrosion environment was investigated by means of microstructure observation, electrochemical test, dissolved Nb content measurement and Nb segregation observation. The results show that the microstructure of the experimental steels is mainly ferrite with a little pearlite. The dissolved Nb contents of the experimental steels are 0.0235 and 0.0458 wt.%, respectively, while the undissolved Nb content is nearly the same. In addition to enhancing mechanical properties of the steel, dissolved Nb improves the corrosion resistance by enriching Nb in the rust layer. Nb oxides in the rust layer cause a decrease in the corrosion rate due to a decrease in the anodic reaction kinetics. The segregation of Nb at the grain boundaries suppresses the corrosion. Moreover, Nb is enriched at the bottom of the corrosion pit and prevents any further corrosion.

关键词： low-alloy steel Acid corrosion Pitting corrosion Electrochemical impedance spectroscopy segregation

Kinetics and microstructural modeling of isothermal austenite-to-ferrite transformation in Fe-C-Mn-Si steels

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Journal of Materials Science & Technology 2019年第8期35卷 1753-1766页

作者： S.J.Song W.K.Che J.B.Zhang L.K.Huang S.Y.Duan F.Liu State Key Laboratory of Solidification Processing Northwestern Polytechnical University

During the multi-stage processing of advanced high-strength steels, the austenite-to-ferrite transformation, generally as a precursor of the formation of other non-equilibrium or metastable structures, has a severe effect on the subsequent phase transformations. Herein, a more flexible kinetic and microstructural predictive modeling for the key austenite-to-ferrite transformation of Fe-C-Mn-Si steels was developed,in combination with the classical nucleation theory, the general mixed-mode growth model based on Gibbs energy balance, the microstructural path method and the kinetic framework for grain boundary nucleation. Adopting a bounded, extended matrix space corresponding to a single ferrite grain, both softimpingement and hard-impingement can be naturally included in the current modeling. Accordingly, this model outputs the ferrite volume fraction, the austenite/ferrite interface area per unit volume, and the average grain size of ferrite, which will serve as the input parameters for modeling the subsequent bainite or martensite transformations. Applying the model, this work successfully predicts the experiment measurement of the isothermal austenite-to-ferrite transformation in Fe-0.17 C-0.91 Mn-1.03 Si(wt%) steel at different temperatures and explains why the final-state average grain size of ferrite has a maximum at the moderate annealing temperature. Effectiveness and advantages of the present model are discussed arising from kinetics and thermodynamics accompanied with nucleation, growth and impingement.

关键词： Isothermal austenite-ferrite transformation Kinetics Thermodynamics Microstructural modeling low-alloy steel

Oxidation behavior and lifetime prediction of three commercial alloys used in power plants at 550 ℃ in CO2 environment

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Journal of Iron and Steel Research(International) 2019年第8期26卷 898-908页

作者： Mohammad Hassan Shirani Bidabadi Yu Zheng Abdul Rehman Chi Zhang Hao Chen Peggy Hou Zhi-gang Yang Key Laboratory of Advanced Materials of Ministry of Education School of Materials Science and Engineering Collaborative Innovation Center of Advanced Nuclear Energy Technology Tsinghua University Beijing 100084 China Materials Sciences Division Lawrence Berkeley National Laboratory Berkeley CA 94720 USA

The oxidation behaviors of CrMoV, F91, and 310S alloys in CO2 at 550 °C for up to 1000 h were studied by weight change measurements, scanning electron microscopy, X-ray diffraction, Raman microscopy, optical microscopy, and glow dis-charge optical emission spectroscopy. 310S showed the best oxidation resistance followed by F91 and then CrMoV. Both CrMoV and F91 formed a duplex oxide layer, consisted of Fe2O3, Fe3O4, and Fe-Cr spinel, while 310S formed NiFe2O4 spinel and Cr2O3. Carburization was only observed in F91 and 310S alloys. The rates of metal loss were evaluated for long-term applications in power plants.

关键词： low-alloy steel 9Cr steel Stainless steel High-temperature corrosion Carburization