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Preparation of lead-free base glaze Suitable for Pearlescent Pigments by Low-temperature Solid-phase Reaction with Alkali Waste

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Journal of Wuhan University of Technology(Materials Science) 2022年第6期37卷 1262-1270页

作者： RAO Li HUANG Kang FU Qiong WANG Junwei DAI Li ZHAO Na LI Xiangjun HE Yong ZHOU Yi CHEN Yanlin College of Materials and Chemical Engineering Hubei University of TechnologyWuhan 430068China Hubei Provincial Key Laboratory of Green Materials for Light Industry Hubei University of TechnologyWuhan 430068China New Materials and Green Manufacturing Talent Introduction and Innovation Demonstration base Hubei University of TechnologyWuhan 430068China Hubei Longzhong Laboratory Xiangyang 441000China

A lead-free base glaze suitable for pearlescent pigments was prepared by a low-temperature solid-phase reaction with alkali *** were performed to evaluate the effects of the sintering conditions and alkali waste composition on the prepared base glaze and pearlescent *** experimental results show that partially replacing SiO_(2) with B_(2)O_(3) effectively reduced the sintering temperature and time to form a glass network,but the network structure becomes disconnected as the B_(2)O_(3) content *** amorphous base glaze was obtained when soda ash was replaced with a small amount of alkali waste,but increasing the addition of NaCl further was adverse to base glaze formation by resulting in crystallization of the base glaze and a decrease in the bridging oxygen *** pearlescent pigment was thermally stable in the glaze at 750℃,while higher temperatures caused the crystalline phase of NaAlSiO_(4) to appear and adhere to the surface of pigment granules,which degraded the pearlescent effect of the glaze.

关键词： pearlescent pigment lead-free base glaze alkali waste low-temperature solid-phase reaction mica titanium

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