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hot corrosion resistance of TB8 Titanium Alloy after ECAP and Heat Treatment

Journal of Wuhan University of Technology(Materials Science) 2023年第6期38卷 1440-1448页

作者： LI Shuaidi XU Xiaojing BAI Xiang CAO Bin Institute of Advanced Manufacturing and Modern Equipment Technology Jiangsu UniversityZhenjiang 212013China

The metastableβtitanium alloy TB8(Ti-12.76Mo-2.13Nb-2.73A1-0.16Si)was used as the original material,and the secondary processing method combining equal channel angular pressing(ECAP)and heat treatment was adopted.With the help of optical microscope(OM),scanning electron microscope(SEM)and X-ray diffractometer(XRD),the corrosion behavior of TB8 titanium alloy after different secondary processing(800℃/850℃solid solution-520℃aging,ECAP-800℃/850℃solid solution-520℃aging,and800℃/850℃solid solution-ECAP-520℃aging)was studied.The experimental results show that the hot corrosion products of the six samples are similar,mainly Na_(2)Si_(2)O_(5),MoS_(2),TiCl_(2),Ti(SO_(4))_(2),and TiS.Due to the grains of the TB8 titanium alloy treated by 850℃solid solution-ECAP-520℃aging are obviously refined,the surface structure is the most smooth and dense,forming a continuous Al2O3protective film,and the surface defects are the least after corrosion.Its corrosion layer thickness is the lowest(102.3μm),only 36.5%-81.4%of that of other secondary processing titanium alloys.In addition,the corrosion kinetics curves of the six materials all follow parabolic laws,and the minimum corrosion weight gain of the samples after 850℃solutionECAP-520℃aging treatment is 0.7507 mg·mm^(-2),showing better hot corrosion resistance.

关键词： TB8 ECAP heat treatment hot corrosion resistance

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corrosion Behaviors of Nitride Coatings on Titanium Alloy in NaCl-Induced hot corrosion

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Acta Metallurgica Sinica(English Letters) 2021年第10期34卷 1434-1446页

作者： Mingming Zhang Yipeng Feng Yahui Wang Yunsong Niu Li Xin Yongfeng Li Jianxiu Su Shenglong Zhu Fuhui Wang School of Mechanical and Electrical Engineering Henan Institute of Science and TechnologyXinxiang 453003China corrosion and Protection Division Shenyang National Laboratory for Materials ScienceInstitute of Metal ResearchShenyang 110016China corrosion and Protection Division Shenyang National Laboratory for Materials ScienceNortheastern UniversityShenyang 110819China

TiN and TiAlN coatings were deposited by arc ion plating on titanium alloys to study their hot corrosion resistance when they were exposed to NaCl at 600℃.The microstructure and corrosion behaviors of nitride coatings were studied using scanning electron microscope,X-ray diffraction,electro-probe microanalyzer and X-ray photoelectron spectroscopy.The results showed that nitride coatings with the different compositions and the ones with the same composition but different thicknesses presented different hot corrosion resistance.TiN and thin TiAlN coatings showed poor corrosion resistance.Serious internal oxidation attacked the alloy substrate.Their corrosion products were mainly consisted of non-protective TiO2 and sodium salt.By contrast,the thick TiAlN coating presented outstanding corrosion resistance.Besides sodium salt,the corrosion products were composed of protective Al_(2)O_(3).The increasing thickness of TiAlN significantly enhanced the hot corrosion resistance.The corrosion mechanisms of alloy,TiN and TiAlN coatings were discussed in detail.

关键词： Titanium alloy Nitride Coating hot corrosion resistance

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