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Effect of doping aluminum and yttrium on high-temperature oxidation behavior of Ni-11Fe-10Cu alloy

Journal of Rare Earths 2016年第11期34卷 1139-1147页

作者：程新华范磊刘莉杜开发汪的华 School of Resource and Environmental Sciences Wuhan University Institute of Metal Research Chinese Academy of Sciences

Aiming to develop materials for construction of the set-up and electrode of high-temperature molten salt reactors, the effect of Al and Y on the high-temperature oxidation behavior of Ni-11Fe-10Cu at 750 and 950 °C in air were investigated. The oxidation kinetics of Ni-11Fe-10Cu alloy followed parabolic law at 750 °C without spallation and linear law at 950 °C with severe spallation, while that of Ni-11Fe-10Cu-6Al-3Y alloy followed parabolic law at 750 and 950 °C without spallation. The parabolic rate constant （kp） of Ni-11Fe-10Cu was smaller than that of Ni-11Fe-10Cu-6Al-3Y at 750 °C. The oxide scale formed on Ni-11Fe-10Cu at 750 °C was composed of a CuO outer layer, a NiFe2O4 middle layer and a NiO inner layer. The oxide scale formed on Ni-11Fe-10Cu-6Al-3Y at 750 °C was also composed of the similar triplex layers in addition to an internal oxidation zone containing Al, Ni and Cu oxide and the microstructure of the scale changed with increasing temperature. Although the doping Al and Y could improve the adherence of oxide scale, it could aggravate the extent of internal oxidation. Based on the combination of X-ray diffraction （XRD）, scanning electron mi-croscopy/energy dispersive spectroscopy （SEM/EDX） analysis, the microstructure and growth mechanism of the multi-layer oxide scale was studied and the effect of doping Al and Y on the oxidation behavior of Ni-11Fe-10Cu alloy was also discussed.

关键词： Ni-Fe-Cu alloy doping rare earths high-temperature oxidation behavior multi-layer oxide scale

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Revealing effect of Al content on oxidation of novel Co-Cr-Nb-W carbide-strengthened superalloy

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Rare Metals 2024年第9期43卷 4521-4534页

作者： Chen Ling Shang-Ping Li Jie Hou He-Li Luo Central Iron&Steel Research Institute Beijing 100081China Beijing GAONA Materials&Technology Co. Ltd.Beijing 100081China

The high-temperature oxidation behavior of novel Co-Cr-Nb-W carbide-strengthened wear-resistance alloys with different Al contents(1wt%,2wt%and 3wt%)at 950,1000 and 1050℃was thoroughly investigated by scanning electron microscopy,X-ray diffraction,X-ray photoelectron spectroscopy and field emission electron probe *** porous property of NbC in-situ oxidation products(Nb_(2)O_(5),Co Nb_(2)O_(6)and Co_(4)Nb_(2)O_(9))induces a multi-layered oxide scale with micropores and ***-Cr-Nb-W alloy with 1 wt%Al undergoes catastrophic oxidation and spalling above 1000℃.The outward transportation of Cr and Co is effectively restrained by a continuous Al_(2)O_(3)scale formed around NbC in-situ oxidation region when Al content reaches 3 wt%.The β-Co Al in Co-Cr-Nb-W alloy with 3 wt%Al has an oxidation priority over eutectic carbides and the alloy matrix which are both enriched with Cr,thereby preventing the formation of Cr-depletion area and improving the self-healing ability of the oxide film.A slight change in Al content has a remarkable influence on the cooperative effect of Al and Cr and multiplies the antioxidant capacity of Co-Cr-Nb-W alloy above 1000℃.

关键词： high-temperature oxidation behavior oxidation kinetics Superalloy Wear-resistant alloy Microstructure

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