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Saturation Estimation with Complex Electrical Conductivity for hydrate-Bearing Clayey Sediments:An Experimental Study

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Journal of Ocean University of China 2024年第1期23卷 173-189页

作者： XING Lanchang ZHANG Shuli ZHANG Huanhuan WU Chenyutong WANG Bin LAO Liyun WEI Wei HAN Weifeng WEI Zhoutuo GE Xinmin DENG Shaogui College of Control Science and Engineering China University of Petroleum(East China)Qingdao 266580China School of Water Energy and EnvironmentCranfield UniversityCranfield MK430ALUnited Kingdom Department of Alternative Energy PetroChina Research Institute of Petroleum Exploration&DevelopmentLangfang 065007China School of Geosciences China University of Petroleum(East China)Qingdao 266580China Laboratory for Marine Mineral Resources Qingdao National Laboratory for Marine Science and TechnologyQingdao 266071China

Clays have considerable influence on the electrical properties of hydrate-bearing sediments.It is desirable to understand the electrical properties of hydrate-bearing clayey sediments and to build hydrate saturation(S_(h))models for reservoir evaluation and monitoring.The electrical properties of tetrahydrofuran-hydrate-bearing sediments with montmorillonite are characterized by complex conductivity at frequencies from 0.01 Hz to 1 kHz.The effects of clay and Sh on the complex conductivity were analyzed.A decrease and increase in electrical conductance result from the clay-swelling-induced blockage and ion migration in the electrical double layer(EDL),respectively.The quadrature conductivity increases with the clay content up to 10%because of the increased surface site density of counterions in EDL.Both the in-phase conductivity and quadrature conductivity decrease consistently with increasing Sh from 0.50 to 0.90.Three sets of models for Sh evaluation were developed.The model based on the Simandoux equation outperforms Archie’s formula,with a root-mean-square error(E_(RMS))of 1.8%and 3.9%,respectively,highlighting the clay effects on the in-phase conductivity.The fre-quency effect correlations based on in-phase and quadrature conductivities exhibit inferior performance(E_(RMS)=11.6%and 13.2%,re-spectively)due to the challenge of choosing an appropriate pair of frequencies and intrinsic uncertainties from two measurements.The second-order Cole-Cole formula can be used to fit the complex-conductivity spectra.One pair of inverted Cole-Cole parameters,i.e.,characteristic time and chargeability,is employed to predict S_(h) with an E_(RMS) of 5.05%and 9.05%,respectively.

关键词： gas hydrate complex electrical conductivity hydrate-bearing clayey sediment hydrate saturation Simandoux equation frequency dispersion Cole-Cole formula

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Rate-limiting factors in hydrate decomposition through depressurization across various scales:A mini-review

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Chinese Journal of Chemical Engineering 2024年第3期67卷 206-219页

作者： Xian Sun Peng Xiao Qinfeng Shi Lingban Wang Zhenbin Xu Yuhao Bu Xiaohui Wang Yifei Sun Changyu Sun Guangjin Chen State Key Laboratory of Heavy Oil Processing China University of Petroleum(Beijing)Beijing 102249China Jining University Jining 273115China

Natural gas hydrate is an energy resource for methane that has a carbon quantity twice more than all traditional fossil fuels combined.However,their practical application in the field has been limited due to the challenges of long-term preparation,high costs and associated risks.Experimental studies,on the other hand,offer a safe and cost-effective means of exploring the mechanisms of hydrate dissociation and optimizing exploitation conditions.gas hydrate decomposition is a complicated process along with intrinsic kinetics,mass transfer and heat transfer,which are the influencing factors for hydrate decomposition rate.The identification of the rate-limiting factor for hydrate dissociation during depressurization varies with the scale of the reservoir,making it challenging to extrapolate findings from laboratory experiments to the actual exploitation.This review aims to summarize current knowledge of investigations on hydrate decomposition on the subject of the research scale(core scale,middle scale,large scale and field tests)and to analyze determining factors for decomposition rate,considering the various research scales and their associated influencing factors.

关键词： gas hydrate Rate-limiting factors Research scale Depressurization Decomposition

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Deformation Characteristics of hydrate-Bearing Sediments

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Journal of Ocean University of China 2024年第1期23卷 149-156页

作者： DONG Lin LI Yanlong ZHANG Yajuan HU Gaowei LIAO Hualin CHEN Qiang WU Nengyou Key Laboratory of gas hydrate Ministry of Natural ResourcesQingdao Institute of Marine GeologyQingdao 266237China Laboratory for Marine Mineral Resources Laoshan LaboratoryQingdao 266237China College of Oceanography Hohai UniversityNanjing 210098China College of Petroleum Engineering China University of Petroleum(East China)Qingdao 266555China

The safe and efficient development of natural gas hydrate requires a deep understanding of the deformation behaviors of reservoirs.In this study,a series of triaxial shearing tests are carried out to investigate the deformation properties of hydrate-bearing sediments.Variations of volumetric and lateral strains versus hydrate saturation are analyzed comprehensively.Results indicate that the sediments with high hydrate saturation show dilative behaviors,which lead to strain-softening characteristics during shearing.The volumetric strain curves have a tendency to transform gradually from dilatation to compression with the increase in effective confining pressure.An easy prediction model is proposed to describe the relationship between volumetric and axial strains.The model coefficientβis the key dominating factor for the shape of volumetric strain curves and can be determined by the hydrate saturation and stress state.Moreover,a modified model is established for the calculation of lateral strain.The corresponding determination method is provided for the easy estimation of model coefficients for medium sand sediments containing hydrate.This study provides a theoretical and experimental reference for deformation estimation in natural gas hydrate development.

关键词： gas hydrate deformation characteristics volumetric strain lateral strain prediction model

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gas hydrate accumulation associated with fluid escape structure in the western margin of South China Sea

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Journal of Oceanology and Limnology 2023年第3期41卷 947-958页

作者： Taotao YANG Lin LI Yintao LU Kaiqi YU Zhili YANG Xuefeng WANG Wei LI PetroChina Hangzhou Research Institute of Geology Hangzhou 310023China CAS Key Laboratory of Ocean and Marginal Sea Geology South China Sea Institute of OceanologyChinese Academy of SciencesGuangzhou 510301China

gas hydrates have been found in the western continental margin of South China Sea,which are revealed by widespread bottom simulating reflectors(BSRs)imaged from a three-dimensional(3D)seismic volume near the Guangle carbonate platform in the western South China Sea.Fluid-escape structures(faults and gas chimneys)are originated below BSR were distinguished.A comprehensive model in three-level structure was proposed to depict the gas hydrate accumulation in the study area.In Level 1,regional major faults and gas chimneys provide the first pathways of upward migration of gas near basement.In Level 2,pervasive polygonal faults in carbonate layer promote the migration of gas.In Level 3,gases sourced from near-basement accumulate within shallow sediment layers and form gas hydrate above the unit with faults once appropriate temperature and pressure occur.The gas hydrates in the study area are mainly in microbial origin,and their accumulation occurs only when fluid-escape structures align in all the three levels.The proposed model of the gas hydrate accumulation in western SCS margin provides new insights for further studies in this poorly studied area.

关键词： gas hydrate fluid-escape structures gas sources bottom simulating reflector(BSR) South

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Auto-Detection Method Using Convolution Neural Network for Bottom-Simulating Reflectors

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Journal of Ocean University of China 2024年第3期23卷 683-694页

作者： XU Haowei XING Junhui YANG Boxue LIU Chuang Key Laboratory of Submarine Geosciences and Prospecting Techniques MOE and College of Marine GeosciencesOcean University of ChinaQingdao 266100China Laboratory for Marine Mineral Resources Qingdao National Laboratory for Marine Science and TechnologyQingdao 266071China

In studies on gas hydrate,bottom-simulating reflectors(BSR)are used to determine the potential hydrate-bearing sedimentary layers.Usually,BSR detection is performed manually by experienced interpreters.Therefore,a method for implementing an auto-matic BSR detection process should be established.In this study,we develop a novel architecture for BSR characterization using the convolutional neural network(CNN)technique.We propose the use of Stokes’transform(ST)to obtain a time-frequency spectrum for the input of CNN.ST fully uses the frequency content of the seismic data,and a part of the 3D seismic data collected from the Blake Ridge is utilized to train the CNN.Synthetic seismic records with variable signal-to-noise ratios(SNR),as well as Blake Ridge seismic data,were used to validate the detection effect of the CNN.Results show that the CNN trained by this method exhibits excellent performance in noise-resistant testing and achieves an accuracy of more than 89% in field seismic data detection.

关键词： BSR CNN Stocks’transform gas hydrate Blake Ridge

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Influence of gas hydrate on the Acoustic Properties of Sediment: A Comprehensive Review with a Focus on Experimental Measurements

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Acta Geologica Sinica(English Edition) 2022年第2期96卷 713-726页

作者： ZHANG Qi LIU Xin HE Tao LU Hailong Key Laboratory of Orogenic Belts and Crustal Evolution(Ministry of Education) School of Earth and Space SciencesPeking UniversityBeijing 100871China Beijing International Center for gas hydrate Peking UniversityBeijing 100871China Institute for Marine Science and Technology Shenzhen Graduate SchoolPeking UniversityShenzhen 518055China

In recent years, natural gas hydrate has attracted increasing attention worldwide as a potential alternative energy source due to its attributes of wide distribution, large reserves, and low carbon. Since the acoustic characteristics of hydratebearing reservoirs clearly differ from those of adjacent formations, an acoustic approach, using seismic and acoustic logging, is one of the most direct, effective and widely used methods among the identification and characterization techniques for hydrate reservoir exploration. This review of research on the influence of hydrate(content and distribution) on the acoustic properties(velocity and attenuation) of sediments in the past two decades includes experimental studies based on different hydrate formation methods and measurements, as well as rock physics models. The main problems in current research are also pointed out and future prospects discussed.

关键词： gas hydrate acoustic properties rock physics model experimental measurements

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Research Progress on the Electrical Properties of gas hydrate-bearing Sediments

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Acta Geologica Sinica(English Edition) 2023年第3期97卷 816-827页

作者： TAN Kui ZHANG Qi HE Tao Key Laboratory of Orogenic Belts and Crustal Evolution(Ministry of Education) School of Earth and Space SciencesPeking UniversityBeijing 100871China Beijing International Center for gas hydrate Peking UniversityBeijing 100871China

Electrical properties are important physical parameters of natural gas hydrate,and,specifically,resistivity has been widely used in the quantitative estimation of hydrate saturation.There are three main methods to study the electrical properties of gas hydrate-bearing sediments:experimental laboratory measurements,numerical simulation,and resistivity logging.Experimental measurements can be divided into three categories:normal electrical measurement,complex resistivity measurement,and electrical resistivity tomography.Experimental measurements show that the resistivity of hydrate-bearing sediment is affected by many factors,and its distribution as well as the hydrate saturation is not uniform;there is a distinct non-Archie phenomenon.The numerical method can simulate the resistivity of sediments by changing the hydrate occurrence state,saturation,distribution,etc.However,it needs to be combined with X-ray CT,nuclear magnetic resonance,and other imaging techniques to characterize the porous characteristics of the hydrate-bearing sediments.Resistivity well logging can easily identify hydrate layers based on their significantly higher resistivity than the background,but the field data of the hydrate layer also has a serious non-Archie phenomenon.Therefore,more experimental measurements and numerical simulation studies are needed to correct the parameters of Archie’s formula.

关键词： resource exploration gas hydrate resistivity hydrate saturation numerical simulation well logging Archie's formula

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Geochemical Characteristics and gas-to-gas Correlation of Two Leakage-type gas hydrate Accumulations in the Western Qiongdongnan Basin, South China Sea

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Acta Geologica Sinica(English Edition) 2022年第2期96卷 680-690页

作者： LAI Hongfei QIU Haijun LIANG Jinqiang KUANG Zenggui FANG Yunxin REN Jinfeng LU Jing’an Southern Marine Science and Engineering Guangdong Laboratory(Guangzhou) Guangzhou 511458China MNR Key Laboratory of Marine Mineral Resources Guangzhou Marine Geological SurveyMinistry of Natural ResourcesGuangzhou 510075China

In recent years,a series of highly saturated leakage-type gas hydrates have been discovered in the western Qiongdongnan Basin(QDNB),South China Sea.Based on the molecular compositional and isotopic characteristics of the gas samples relevant to the gas hydrates collected from the two leakage-type gas hydrate accumulations in the GMGS5 and GMGS6 drilling zones,a detailed geochemical gas-to-gas correlation was conducted in this study,in order to further understand the geochemical characteristics and possible hydrocarbon sources of these gas hydrates.The natural gas relevant to the gas hydrates in the GMGS5 block is characterized by wet gas(67.96%gas samples from the GMGS6 block exhibit the characteristics of dry gas(99.25%0.9)and lack molecular and carbon isotope fractionation.Approximately 40%‒60%of the methane within the gas hydrate is of microbial origin,while the C^(2+)gas components are typical coal-type gas that are derived from thermogenic source rocks or deeply-buried natural gas fields.In addition,typical in situ primary microbial methane(−80.6‰gas to the gas hydrates.The gas-to-gas correlation results show that the hydrate gases within the two leakage-type gas hydrate accumulations in the GMGS5 and GMGS6 blocks are geochemically different,suggesting that they may have been derived from different source kitchens.Our results further indicate that the deeply-buried thermogenic gas significantly contributed to the shallowly-buried gas hydrates in the western QDNB and multiple effective thermogenic source kitchens provided the hydrocarbon gas in the gas hydrate accumulations.

关键词： gas hydrate gas genetic type hydrocarbon gas source geochemical characteristics

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Controls on the gas hydrate Occurrence in Lower Slope to Basin-Floor,Northeastern Bay of Bengal

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Journal of Ocean University of China 2022年第4期21卷 813-826页

作者： LU Yintao LUAN Xiwu SHI Boqing FAN Guozhang RAN Weimin XU Ning WANG Haiqiang SHAO Dali DING Liangbo WANG Xingxing Petrochina Hangzhou Research Institute of Geology Hangzhou 310023China School of Earth Science and Engineering Shandong University of Science and TechnologyQingdao 266590China China National Oil and gas Exploration and Development Company Beijing 100031China Qingdao Institute of Marine Geology China Geological SurveyQingdao 266071China College of Marine Science and Technology China University of GeosciencesWuhan 430074China

High resolution seismic data and newly acquired logging data reveal the presence of gas hydrates in the deep-water area in the northeastern Bay of Bengal.Bottom Simulating Reflectors(BSRs)appear at 430 ms beneath the seafloor,with the features of typical gas hydrates reported elsewhere except for some discontinuity.The BSR distribution is closely related to the position of anticline structures and turbidite channels.Anticlines provide conduits for the upward migration of gases from deeper intervals,while the turbidite sands within channels act as reservoirs for gas hydrate accumulation.High sedimentation rates in the Bengal Fan were ge-nerally favorable to produce a great amount of methane gas,providing favorable preconditions for the formation of gas hydrates.The discovery of gases in adjacent area indicates the contribution of the biogenic gas to the formation of gas hydrates.Meanwhile,seismic sections provide the evidence for the potential thermogenic gas kitchen in deep intervals.The anticline structures and the associated vertical fractures may constitute vertical fluid flowing conduits,which hydraulically connect the two deeper thermogenic petroleum systems(i.e.,rifting and Eocene-Oligocene source rocks)with the turbidite reservoirs and thus facilitate the fluid migration from the sources to the reservoirs,generating favorable conditions for gas-hydrate accumulation in such foreland setting.

关键词： Bay of Bengal gas hydrate anticline turbidite sands

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Growth behavior and resource potential evaluation of gas hydrate in core fractures in Qilian Mountain permafrost area, Qinghai-Tibet Plateau

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China Geology 2023年第2期6卷 208-215页

作者： Qing-guo Meng Chang-ling Liu Zhen-quan Lu Xi-luo Hao Cheng-feng Li Qing-tao Bu Yun-kai Ji Jia-xian Wang Key Laboratory of gas hydrate Qingdao Institute of Marine GeologyChina Geological SurveyMinistry of Natural ResourcesQingdao 266237China Laboratory for Marine Mineral Resources Laoshan LaboratoryQingdao 266237China Oil and gas Survey China Geological SurveyMinistry of Natural ResourcesBeijing 100083China Faculty of Engineering China University of GeosciencesWuhan 430074China

The Qilian Mountain permafrost area located in the northern of Qinghai-Tibet Plateau is a favorable place for natural gas hydrate formation and enrichment,due to its well-developed fractures and abundant gas sources.Understanding the formation and distribution of multi-component gas hydrates in fractures is crucial in accurately evaluating the hydrate reservoir resources in this area.The hydrate formation experiments were carried out using the core samples drilled from hydrate-bearing sediments in Qilian Mountain permafrost area and the multi-component gas with similar composition to natural gas hydrates in Qilian Mountain permafrost area.The formation and distribution characteristics of multi-component gas hydrates in core samples were observed in situ by X-ray Computed Tomography(X-CT)under high pressure and low temperature conditions.Results show that hydrates are mainly formed and distributed in the fractures with good connectivity.The ratios of volume of hydrates formed in fractures to the volume of fractures are about 96.8%and 60.67%in two different core samples.This indicates that the fracture surface may act as a favorable reaction site for hydrate formation in core samples.Based on the field geological data and the experimental results,it is preliminarily estimated that the inventory of methane stored in the fractured gas hydrate in Qilian Mountain permafrost area is about 8.67×1013 m3,with a resource abundance of 8.67×108 m3/km2.This study demonstrates the great resource potential of fractured gas hydrate and also provides a new way to further understand the prospect of natural gas hydrate and other oil and gas resources in Qilian Mountain permafrost area.

关键词： gas hydrate Growth behavior Core fracture Rock Quality Designation Resource potential evaluation Engineering Oil and gas exploration Qilian Mountain permafrost area Qinghai-Tibet Plateau

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