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fluidization behavior and reducibility of iron ore fines during hydrogen-induced fluidized bed reduction

Particuology 2020年第5期18卷 36-46页

作者： Daniel Spreitzer Johannes Schenk Chair of Ferrous Metallurgy Montanuniversitaet LeobenFranz-Josef-Straβe 188700 LeobenAustria

A laboratory fluidized bed reactor was used to investigate the fluidization behavior and reducibility of various iron ore *** was chosen as a reducing agent across a temperature range of 873-1073 *** magnetite ore used exhibited strong sticking behavior after the initiation of metallic iron *** other tested ores fluidized sufficiently well when subjected to the same high reduction *** kinetic analysis was conducted using a previously developed model to include three rate-limiting step *** trend of apparent activation energy was correlated with the degree of ***,the influence of varying the specific gas rate was *** results show the variation in reducibility as a result of different interactions,which influence the rate-limiting mechanisms of nucleation and the undertaken chemical reactions,which vary as a function of temperature and degree of *** apparent activation energies,determined from the reduction of wtistite to metallic iron,were in the range of 15-60 kJ/mol,depending on the iron ore used and the degree of *** change in apparent activation energy deriving from the increased specific gas rate can be explained by an increasing nucleation effect,especially at lower reduction temperatures.

关键词： Fluidized bed Iron ore reduction Hydrogen fluidization behavior Kinetic analysis

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fluidization behavior and reduction kinetics of pre-oxidized magnetite-based iron ore in a hydrogen-induced fluidized bed

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International Journal of Minerals,Metallurgy and Materials 2022年第10期29卷 1873-1881页

作者： Heng Zheng Oday Daghagheleh Thomas Wolfinger Bernd Taferner Johannes Schenk Runsheng Xu Chair of Ferrous Metallurgy Montanuniversitaet LeobenFranz-Josef-Straβe 188700LeobenAustria K1-MET GmbH Stahlstraße 144020 LinzAustria The State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China

The influence of different pre-oxidation temperatures and pre-oxidation degrees on the reduction and fluidization behaviors of magnetite-based iron ore was investigated in a hydrogen-induced fluidized *** raw magnetite-based iron ore was pre-oxidized at 800 and1000℃ for a certain time to reach a partly oxidation and deeply oxidation *** structure and morphology of the reduced particles were analyzed via optical microscope and scanning electron microscopy(SEM).The reaction kinetic mechanism was determined based on the double-logarithm *** results indicate that the materials with higher oxidation temperature and wider particle size range show better fluidization *** lower oxidation temperature is more beneficial for the reduction rate,especially in the later reduction *** pre-oxidation degree shows no obvious influence on the fluidization and reduction *** on the kinetic analysis,the reduction progress can be divided into three *** reduction mechanism was discussed combing the surface morphology and phase structure.

关键词： magnetite-based iron ore prior oxidation fluidization behavior kinetic analysis hydrogen reduction

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The Influence of Feeding Method on fluidization behavior of Fixed Fluidized Bed

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China Petroleum Processing & Petrochemical Technology 2014年第1期16卷 13-18页

作者： Ren Shihong Mao Anguo Wei Xiaoli SINOPEC Research Institute of Petroleum Processing

An experimental installation of cold model simulation was set up to study the bed pressure drop in different regions of fixed fluidized bed reactor during top feeding and bottom feeding, respectively, at various gas velocities with the fluidization image of solid particles monitored at the same time. By comparing the changes in bed density and operating gas velocity in different regions of fixed fluidized bed reactor, the influence of top feeding and bottom feeding patterns on fluidization behavior could be investigated. The results showed that the bed density in top feeding reactor responded more stably to the change in gas velocity along with the advantage of working in a wider range of operating gas velocities. Based on this study, it is concluded that existing bottom feeding reactor configurations cannot meet the fluidization requirements; and optimization of bottom feeding reactor will be needed.

关键词： feeding method fixed fluidized bed fluidization behavior bed density operating gas velocity

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