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Annealing-induced Grain Refinement in a Nanostructured ferritic steel

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Journal of Materials Science & Technology 2012年第1期28卷 41-45页

作者： Limin Wang Zhenbo Wang Sheng Guo Ke Lu Sheng Guo and Ke Lu Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of Sciences72 Wenhua RoadShenyang 110016China

A nanostructured surface layer with a mean ferrite grain size of -8 nm was produced on a Fe-gCr steel by means of surface mechanical attrition treatment. Upon annealing, ferrite grains coarsen with increasing temperature and their sizes increase to -40 nm at 973 K. Further increasing annealing temperature leads to an obvious reduction of ferrite grain sizes, to -14 nm at 1173 K. The annealing-induced grain refinement is analyzed in terms of phase transformations in the nanostructured steel.

关键词： Nanostructured Surface mechanical attrition treatment (SMAT) ferritic steel Grain refinement Austenitization

Effect of Mo content on the thermal stability of Ti-Mo-bearing ferritic steel

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International Journal of Minerals,Metallurgy and Materials 2021年第3期28卷 412-421页

作者： Yao Huang Wei-ning Liu Ai-min Zhao Jun-ke Han Zhi-gang Wang Hong-xiang Yin China Electric Power Research Institute Beijing 100192China Institute of Engineering Technology University of Science and Technology BeijingBeijing 100083China State Grid Corporation Beijing 100031China Faculty of Materials Metallurgy and Chemistry Jiangxi University of Science and TechnologyGanzhou 341000China Metal and Chemistry Research Institute China Academy of Railway Sciences Corporation LimitedBeijing 100081China

The effects of tempering holding time at 700℃on the morphology,mechanical properties,and behavior of nanoparticles in Ti-Mo ferritic steel with different Mo contents were analyzed using scanning electron microscopy and transmission electron *** equilibrium solid solution amounts of Mo,Ti,and C in ferritic steel at various temperatures were calculated,and changes in the sizes of nanoparticles over time at different Mo contents were *** experimental results and theoretical calculations were in good agreement with each other and showed that the size of nanoparticles in middle Mo content nano-ferrite(MNF)steel changed the least during *** Mo contents inhibited the maturation and growth of nanoparticles,but no obvious inhibitory effect was observed when the Mo content exceeded 0.37wt%.The tensile strength and yield strength continuously decreased with the tempering *** of the strengthening and toughening mechanisms showed that the different mechanical properties among the three different Mo content experiment steels were mainly determined by grain refinement strengthening(the difference range was 30-40 MPa)and precipitation strengthening(the difference range was 78-127 MPa).MNF steel displayed an ideal chemical ratio and the highest thermodynamic stability,whereas low Mo content nano-ferrite(LNF)steel and high Mo content nano-ferrite(HNF)steel displayed relatively similar thermodynamic stabilities.

关键词： ferritic steel nanoparticles interphase precipitation thermal stability ostwald ripening rate

Deuterium Retention and Physical Sputtering of Low Activation ferritic steel

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Plasma Science and Technology 2005年第2期7卷 2737-2740页

作者： T.Hino K.Yamaguchi Y.Yamauchi Y.Hirohata K.Tsuzuki Y.Kusama Department of Nuclear Engineering Hokkaido University Sapporo060-8628 JapanDepartment of Nuclear Engineering Hokkaido UniversitySapporo060-8628 JapanDepartment of Nuclear Engineering Hokkaido UniversitySapporo060-8628 JapanDepartment of Nuclear Engineering Hokkaido UniversitySapporo060-8628 JapanJapan Atomic Energy Research Institute NakaIbaraki-ken311-0193 JapanJapan Atomic Energy Research Institute NakaIbaraki-ken311-0193 Japan

Low activation materials have to be developed toward fusion demonstrationreactors. ferritic steel, vanadium alloy and SiC/SiC composite are candidate materials of the firstwall, vacuum vessel and blanket components, respectively. Although changes of mechanical-thermalproperties owing to neutron irradiation have been investigated so far, there is little data for theplasma material interactions, such as fuel hydrogen retention and erosion. In the present study,deuterium retention and physical sputtering of low activation ferritic steel, F82H, wereinvestigated by using deuterium ion irradiation apparatus. After a ferritic steel sample wasirradiated by 1.7 keV D^+ ions, the weight loss was measured to obtain the physical sputteringyield. The sputtering yield was 0.04, comparable to that of stainless steel. In order to obtain theretained amount of deuterium, technique of thermal desorption spectroscopy (TDS) was employed to theirradiated sample. The retained deuterium desorbed at temperature ranging from 450 K to 700 K, inthe forms of DHO, D_2, D_2O and hydrocarbons. Hence, the deuterium retained can be reduced by bakingwith a relatively low temperature. The fluence dependence of retained amount of deuterium wasmeasured by changing the ion fluence. In the ferritic steel without mechanical polish, the retainedamount was large even when the fluence was low. In such a case, a large amount of deuterium wastrapped in the surface oxide layer containing O and C. When the fluence was large, the thickness ofsurface oxide layer was reduced by the ion sputtering, and then the retained amount in the oxidelayer decreased. In the case of a high fluence, the retained amount of deuterium became comparableto that of ferritic steel with mechanical polish or SS 316 L, and one order of magnitude smallerthan that of graphite. When the ferritic steel is used, it is required to remove the surface oxidelayer for reduction of fuel hydrogen retention. ferritic steel sample was exposed to the envi

关键词： ferritic steel fuel hydrogen retention sputtering yield first wall fusionreactor

Bi-modal microstructure in a powder metallurgical ferritic steel

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Transactions of Nonferrous Metals Society of China 2012年第2期22卷 330-334页

作者：刘锋刘咏吴宏方京华赵大鹏张刘杰刘东华中南大学粉末冶金国家重点实验室长沙410083

ferritic steel with a nominal composition of Fe-14Cr-3W-0.42Ti-0.32Y was prepared by mixing gas-atomized prealloyed powder and mechanically alloyed powder. The microstructure is much different fxom other ferritic steels with the same composition and prepared via only mechanically alloyed powder. A bi-modal structure, which consists of pure ferritic grains and martensitic grains, was obtained after hot forging and air cooling. A phase transformation of αbcc→γfcc→α＇bcc was also discovered in microstructural observation. The bi-modal microstructure shows a good combination of high strength and high ductility.

关键词： ferritic steel powder metallurgy phase transformation bi-modal microstructure mechanical property

Test research on sticking mechanism during hot rolling of SUS 430 ferritic stainless steel

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International Journal of Minerals,Metallurgy and Materials 2010年第5期17卷 573-578页

作者： Jun-xian Liu Yong-jun Zhang Jing-tao Han School of Materials Science and Engineering University of Science and Technology Beijing Beijing 100083 China

The sticking phenomenon during hot rolling of SUS 430 ferritic stainless steel was investigated by means of a two-disc type high-temperature wear tester. The test results indicate that sticking particles on the surfaces of high chromium steel （HiCr） and high-speed steel （HSS） rolls undergo nucleation, growth, and saturation stages. Grooves on the roll surface generated by grinding provide nucleation sites for sticking particles. The number of sticking particles on the HiCr roll surface is greater than that on the HSS roll surface. The average surface roughnesses （Ra） of HiCr and HSS rolls change from 0.502 and 0.493 μm at the initial stage to 0.837 and 0.530 μm at the saturation stage, respectively. The test further proves that the sticking behavior is strongly dependent on roll materials, and the HSS roll is more benefi- cial to prevent particles sticking compared with the HiCr roll under the same hot-rolling conditions.

关键词： ferritic steel stainless steel hot rolling sticking rolls

Comparison between Charpy Transition Temperature TCVN and Reference Temperature T0 for 10Ni3CrMoV ferritic steel

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Comparison between Charpy Transition Temperature TCVN and Re...

Precipitation behavior and martensite lath coarsening during tempering of T/P92 ferritic heat-resistant steel

第五届国际低合金高强度钢会议暨第三届国际超细晶粒钢会议

作者： Gao Yifei Shen Junchang Liu Tao Wu Boqun (Central Iron & steel Research Institute Beijing China)

Charpy transition temperature TCVN and reference temperature To for 10Ni3CrMoV ferritic steel were determined using two different experimental techniques such as Charpy impact test technique and refer

关键词： ferritic steel TCVN reference temperature To master curve thermal treatment

来源： cnki会议评论

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International Journal of Minerals,Metallurgy and Materials 2014年第5期21卷 438-447页

作者： Lin-qing Xu Dan-tian Zhang Yong-chang Liu Bao-qun Ning Zhi-xia Qiao Ze-sheng Yan Hui-jun Li State Key Lab of Hydaulic Engineering Simulation and Safety School of Material Science and EngineeringTianjin University School of Materials Science and Engineering Tianjin University of Technology School of Mechanical Engineering Tianjin University of Commerce

Tempering is an important process for T/P92 ferritic heat-resistant steel from the viewpoint of microstructure control, as it facili- tates the formation of final tempered martensite under serving conditions. In this study, we have gained deeper insights on the mechanism underlying the microstructural evolution during tempering treatment, including the precipitation of carbides and the coarsening of martensite laths, as systematically analyzed by optical microscopy, transmission electron microscopy, and high-resolution transmission electron mi- croscopy. The chemical composition of the precipitates was analyzed using energy dispersive X-ray spectroscopy. Results indicate the for- mation of M3C （cementite） precipitates under normalized conditions. However, they tend to dissolve within a short time of tempering, owing to their low thermal stability. This phenomenon was substantiated by X-ray diffraction analysis. Besides, we could observe the precipitation of fine carbonitrides （MX） along the dislocations. The mechanism of carbon diffusion controlled growth of M23C6 can be expressed by the Zener＇s equation. The movement of Y-junctions was determined to be the fundamental mechanism underlying the martensite lath coarsening process. Vickers hardness was estimated to determine their mechanical properties. Based on the comprehensive analysis of both the micro- structural evolution and hardness variation, the process of tempering can be separated into three steps.

关键词： ferritic steel heat resisting tempering precipitation martensite coarsening

Microstructural evolution of a silicon carbide-carbon coated nanostructured ferritic alloy composite during in-situ Kr ion irradiation at 300℃ 450℃

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Journal of Materials Science & Technology 2021年第12期71卷 75-83页

作者： Kaustubh Bawane Kathy Lu Xian-Ming Bai Jing Hu Meimei Li Peter M.Bald Edward Ryan Department of Materials Science and Engineering Virginia TechBlacksburgVAUSA IVEM-Tandem Facility Argonne National LaboratoryLemontILUSA

This work focuses on irradiation behaviors of a novel silicon carbide and carbon coated nanostructured ferritic alloy(SiC-C@NFA)composite for potential applications as a cladding and structural material for next generation nuclear *** SiC-C@NFA samples were irradiated with 1 MeV Kr ions up to 10 dpa at 300 and 4500 *** and defect evolution were studied in-situ at the IVEM-Tandem facility at Argonne National *** effects of ion irradiation on various phases such asα-ferrite matrix,(Fe,Cr)_(7)C_(3),and(Ti,W)C precipitates were ***α-ferrite matrix showed a continuous increase in dislocation density along with spatial ordering of dislocation loops(or loop strings)at>5 *** size of the dislocation loops at 450℃was larger than that at 300℃.The nucleation and growth of new(Ti,W)C precipitates inα-ferrite grains were enhanced with the ion dose at 450℃.This study provides new insight into the irradiation resistance of the SiC-C@NFA system.

关键词： In-situ ion irradiation ferritic steel (FeCr)_(7)C_(3) Metal matrix composite Fuel cladding

The origin of different morphology of internal oxide precipitates in ferritic and austenitic steels

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Journal of Materials Science & Technology 2023年第30期161卷 88-100页

作者： Zhao Shen Xiaoqin Zeng Shengchuan Wu Hongbing Yu Benjamin M.Jenkins Phani Karamched Michael P.Moody Jianqiang Zhang You Wang Sergio Lozano-Perez National Engineering Research Center of Light Alloy Net Forming and State Key Laboratory of Metal Matrix Composites School of Materials Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China State Key Laboratory of Traction Power Southwest Jiaotong UniversityChengdu 610031China Department of Engineering Science University of OxfordParks RoadOX13PJ OxfordUK Department of Materials University of OxfordParks RoadOX13PH OxfordUK School of Materials Science and Engineering University of New South WalesSydneyNSW 2052Australia School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China

The internal oxide precipitates were supposed to be spherical in Wagner’s original theory,while the fol-lowing research demonstrated that this assumption is an exception rather than the truth,which caused deviations in the application of this *** this study,the internal oxide precipitates have a needle-like and a near-spherical morphology in a Fe-9Cr ferritic and a Fe-17Cr-9Ni austenitic steels after expo-sure to 600℃ deaerated steam for 600 h,*** nano-to-atomic scale characterization shows that the morphology of the internal oxide precipitates is controlled by the structure of the interfaces be-tween the metal matrix and the internal oxide,while the interface structure is mainly affected by the crystallographic structure of the two phases and their orientation *** addition,the internal oxide precipitation-induced volume expansion and the outward Fe diffusion-induced volume shrink oc-cur simultaneously during the oxidation *** stress status in the internal oxidation zone(IOZ)is the competing result of the two factors,which could dynamically affect the high-temperature *** results obtained in this study suggest that there is potential to control the distribution,morphology,and interface structure of the internal oxide precipitates by selecting appropriate base metal and internal oxide-forming element,in order to obtain better high-temperature oxidation-resistant materials.

关键词： Austenitic steel ferritic steel Oxide precipitates Phase boundary Orientation relationship