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Remarkably enhanced dielectric stability and energy storage properties in BNT–BST relaxor ceramics by A-site defect engineering for pulsed power applications

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Journal of Advanced ceramics 2022年第2期11卷 283-294页

作者： Zhipeng LI Dong-Xu LI Zong-Yang SHEN Xiaojun ZENG Fusheng SONG Wenqin LUO Xingcai WANG Zhumei WANG Yueming LI energy storage and Conversion Ceramic Materials Engineering Laboratory of Jiangxi Province China National Light Industry Key Laboratory of Functional Ceramic MaterialsSchool of Materials Science and EngineeringJingdezhen Ceramic UniversityJingdezhen 333403China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing School of Materials Science and EngineeringWuhan University of TechnologyWuhan 430070China Chengdu Hongke Electronic Technology Co. Ltd.Chengdu 610000China

Lead-free bulk ceramics for advanced pulsed power capacitors show relatively low recoverable energy storage density(Wrec)especially at low electric field condition.To address this challenge,we propose an A-site defect engineering to optimize the electric polarization behavior by disrupting the orderly arrangement of A-site ions,in which Ba_(0.105)Na_(0.325)Sr_(0.245−1.5x)□_(0.5x)Bi_(0.325)+xTiO_(3)(BNS_(0.245−1.5x)□_(0.5x)B_(0.325+x)T,x=0,0.02,0.04,0.06,and 0.08)lead-free ceramics are selected as the representative.The BNS_(0.245−1.5x)□_(0.5x)B_(0.325+x)T ceramics are prepared by using pressureless solid-state sintering and achieve large W_(rec)(1.8 J/cm^(3))at a low electric field(@110 kV/cm)when x=0.06.The value of 1.8 J/cm3 is super high as compared to all other W_(rec) in lead-free bulk ceramics under a relatively low electric field(ceramics.The excellent performances can be attributed to the A-site defect engineering,which can reduce remnant polarization(P_(r))and improve the thermal evolution of polar nanoregions(PNRs).This work confirms that the BNS_(0.245−1.5x)□_(0.5x)B_(0.325+x)T(x=0.06)ceramics are desirable for advanced pulsed power capacitors,and will push the development of a series of Bi0.5Na0.5TiO3(BNT)-based ceramics with high W_(rec) and high-temperature stability.

关键词： relaxor ferroelectrics energy storage ceramics ceramic capacitor Bi_(0.5)Na_(0.5)TiO_(3)(BNT) defect engine

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Progress and perspectives in dielectric energy storage ceramics

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Journal of Advanced ceramics 2021年第4期10卷 675-703页

作者： Dongxu LI Xiaojun ZENG Zhipeng LI Zong-Yang SHEN Hua HAO Wenqin LUO Xingcai WANG Fusheng SONG Zhumei WANG Yueming LI energy storage and Conversion Ceramic Materials Engineering Laboratory of Jiangxi Province China National Light Industry Key Laboratory of Functional Ceramic MaterialsSchool of Materials Science and EngineeringJingdezhen Ceramic UniversityJingdezhen 333403China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing School of Materials Science and EngineeringWuhan University of TechnologyWuhan 430070China Chengdu Hongke Electronic Technology Co. Ltd.Chengdu 610000China

Dielectric ceramic capacitors,with the advantages of high power density,fast chargedischarge capability,excellent fatigue endurance,and good high temperature stability,have been acknowledged to be promising candidates for solid-state pulse power systems.This review investigates the energy storage performances of linear dielectric,relaxor ferroelectric,and antiferroelectric from the viewpoint of chemical modification,macro/microstructural design,and electrical property optimization.Research progress of ceramic bulks and films for Pb-based and/or Pb-free systems is summarized.Finally,we propose the perspectives on the development of energy storage ceramics for pulse power capacitors in the future.

关键词： energy storage ceramics dielectric relaxor ferroelectric antiferroelectric pulse power capacitor

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P-E hysteresis loop going slim in Ba0.3Sr0.7TiO3-modified Bi0.5Na0.5TiO3 ceramics for energy storage applications

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Journal of Advanced ceramics 2020年第2期9卷 183-192页

作者： Dongxu LI Zong-Yang SHEN Zhipeng LI Wenqin LUO Xingcai WANG Zhumei WANG Fusheng SONG Yueming LI energy storage and Conversion Ceramic Materials Engineering Laboratory of Jiangxi Province China National Light Industry Key Laboratory of Functional Ceramic MaterialsSchool of Materials Science and EngineeringJingdezhen Ceramic InstituteJingdezhen333000China Chengdu Hongke Electronic Technology Co. Ltd.Chengdu610000China

(Ba0.3Sr0.7)x(Bi0.5Na0.5)1-xTiO3(BSxBNT,x=0.3–V0.8)ceramics were prepared to investigate their structure,dielectric and ferroelectric properties.BSxBNT ceramics possess pure perovskite structure accompanied from a tetragonal symmetry to pseudo-cubic one with the increase of x value,being confirmed by X-ray diffraction(XRD)and Raman results.The Tm corresponding to a temperature in the vicinity of maximum dielectric constant gradually decreases from 110℃(x=0.3)to-45℃(x=0.8),across Tm=36℃(x=0.5)with a maximum dielectric constant(ɛr=5920@1 kHz)around room temperature.The saturated polarization Ps gradually while the remnant polarization Pr sharply decreases with the increase of x value,making the P-E hysteresis loop of BSxBNT ceramics goes slim.A maximum difference between Ps and Pr(Ps-Pr)is obtained for BSxBNT ceramics with x=0.5,at which a high recoverable energy density(Wrec=1.04 J/cm3)is achieved under an applied electric field of 100 kV/cm with an efficiency ofη=77%.Meanwhile,the varied temperature P-E loops,fatigue measurements,and electric breakdown characteristics for the sample with x=0.5 indicate that it is promising for pulsed power energy storage capacitor candidate materials.

关键词： energy storage ceramics Ba0.3Sr0.7TiO3(BST) Bi0.5Na0.5TiO3(BNT) relaxor ferroelectrics pulsed power capacitor

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Structure and dielectric properties of NBT-xBT-ST lead-free ceramics for energy storage

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Journal of Advanced Dielectrics 2018年第6期8卷 3-7页

作者： Wen-Qin Luo Zong-Yang Shen Yuan-Ying Yu Fu-Sheng Song Zhu-Mei Wang Yue-Ming Li energy storage and Conversion Ceramic Materials Engineering Laboratory of Jiangxi Province China National Light Industry Key Laboratory of Functional Ceramic Materials School of Materials Science and Engineering Jingdezhen Ceramic Institute Jingdezhen 333403P.R.China

(0:74-x)(Na_(0.5)Bi_(0.5))TiO_(3)-xBaTiO_(3)-0.26SrTiO_(3)(x=0~0.1)(abbreviated as NBT-xBT-ST)lead-free ceramics were fabricated by a solid-state reaction method.The effect of Ba doping amount x on the structure and energy storage properties of NBT-xBT-ST ceramics were investigated.All the NBT-xBT-ST ceramics showed single perovskite structure with a pseudocubic phase.Ba doping effectively suppressed grain growth,in favor of forming small and uniform grains.The ceramics with a composition of x=0.04,an optimized energy storage density(γ=0.47 J/cm^(3))and efficiency(η=48:67%),under an applied electric field of 50 kV/cm,should be a candidate for solid-state compact pulsed power capacitor materials.

关键词： Sodium bismuth titanate barium strontium titanate energy storage ceramics compact pulsed power

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BS_(0.5)BNT-based relaxor ferroelectric ceramic/glass-ceramic composites for energy storage

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Journal of Advanced ceramics 2023年第4期12卷 695-710页

作者： Xuhai Shi Kai Li Zong-Yang Shen Junqi Liu Chaoqun Chen Xiaojun Zeng Bo Zhang Fusheng Song Wenqin Luo Zhumei Wang Yueming Li China National Light Industry Key Laboratory of Functional Ceramic Materials Energy Storage and Conversion Ceramic Materials Engineering Laboratory of Jiangxi ProvinceAdvanced Ceramic Materials Research InstituteSchool of Materials Science and EngineeringJingdezhen Ceramic UniversityJingdezhen 333403China

Relaxor ferroelectric ceramics have very high dielectric constant(e)but relatively low electrical breakdown strength(Eb),while glass-ceramics exhibit higher E,due to the more uniformly dispersed amorphous phases and submicrocrystals/nanocrystals inside.How to effectively combine the advantages of both relaxor ferroelectric ceramics and glass-ceramics is of great significance for the development of new dielectric materials with high energy storage performance.In this work,we firstly prepared BaO-SrO-Bi_(2)O_(3)-Na_(2)0-TiO_(2)-Al_(2)O_(3)-SiO_(2)(abbreviated as GS)glass powders,and then fabricated(Ba_(0.3)Sr_(0.7))_(0.5)(Bi_(0.5)Na_(0.5))_(0.5)TiO_(3)+x wt%GS ceramic composites(abbreviated as BSo.sBNT-xGS,x=0,2,6,10,14,16,and 18).Submicrocrystals/nanocrystals with a similar composition to BSo.sBNT were crystalized from the glass,ensuring the formation of uniform core-shell structure in BSo.sBNT-xGS relaxor ferroelectric ceramic/glass-ceramic composites.When the addition amount of GS was 14 wt%,the composite possessed both high&r(>3200 at 1 kHz)and high E,(~170 kV/cm)at room temperature,and their recoverable energy storage density and efficiency were Wrec=2.1 J/cm’and n=65.2%,respectively.The BSo.sBNT-14GS composite also had several attractive properties such as good temperature,frequency,cycle stability,and fast charge-discharge speed.This work provides insights into the relaxor ceramic/glass-ceramic composites for pulsed power capacitors and sheds light on the utilization of the hybrid systems.

关键词： relaxor ferroelectrics energy storage ceramics glass-ceramics Bi_(0.5)Na_(0.5)TiO_(3)(BNT) Ba_(0.3)Sr_(0.7)TiO_(3)(BST)

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