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Effect of liner and porcelain application on zirconia surface structure and composition

International Journal of Oral Science 2016年第3期8卷 164-171页

作者： Tariq F Alghazzawi Gregg M Janowski Department of Prosthetic Dental Sciences College of DentistryTaibah University Department of Materials Science and Engineering School of EngineeringThe University of Alabama at Birmingham

The purpose of this study was to determine if there is an effect of liner and porcelain application （layering and pressing techniques） on the surface of yttria-stabilized tetragonal zirconia polycrystals （Y-TZP）, which were exposed to permutations of liner, layered porcelain, and pressed porcelain. Scanning electron microscope （SEM）/energy dispersive spectroscope （EDS） was used to identify changes in composition and microstructure after removing liner and porcelain with hydrofluoric acid. Simulated aging was also conducted to determine the effect of liner and porcelain on low-temperature degradation. The control group had a typical equiaxed grain structure, referred to as unaffected. When covered with liner or porcelain, some areas changed in structure and composition and were termed affected. The frequency of affected sbructure decreased when liner was covered with either layered porcelain or pressed porcelain. There were statistical differences （P〈0.05） in the composition between affected and unaffected for zirconium （layered porcelain with liner： affected = 60% （0.8%）（m/m）, unaffected = 69% （4%）, layered porcelain without liner： affected = 59% （3%）, unaffected = 65% （3%）） and oxygen （layered porcelain with liner： affected = 35% （2%）, unaffected = 26% （4%）, layered porcelain without liner： affected = 35% （3%）, unaffected = 30% （2%））. However, there were statistical differences （P〈0.05） in the composition for zirconium and oxygen of the aged layered porcelain without liner only. The liner should not be used before porcelain application, especially when using the layering technique for zirconia restorations. Furthermore, pressing should be considered the technique of choice over layering.

关键词： aging coefficient of thermal expansion energy dispersive spectroscopy layering of porcelain pressing of porcelain scanning electron microscope zirconia

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Highly efficient and stable electrooxidation of methanol and ethanol on 3D Pt catalyst by thermal decomposition of In2O3 nanoshells

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Journal of energy Chemistry 2017年第1期26卷 193-199页

作者： Yuhang Xie Hulin Zhang Guang Yao Saeed Ahmed Khan Xiaojing Cui Min Gao Yuan Lin State Key Laboratory of Electronic Thin Film and Integrated Devices University of Electronic Science and Technology of ChinaChengdu 610054SichuanChina Center for Information in Medicine University of Electronic Science and Technology of ChinaChengdu 610054SichuanChina The First Sub-Institute Nuclear Power Institute of ChinaChengdu 610041SichuanChina

In this paper In2O3nanoshells have been synthesized via a facile hydrothermal approach. The nanoshells can be completely cracked into pony-size nanocubes by annealing, which are then used as a support of Pt catalyst for methanol and ethanol electrocatalytic oxidation. The prepared In2O3and supported Pt catalysts (Pt/In2O3) were characterized by X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), field effect scanning electron microscopy (FESEM), and transmission electron microscopy (TEM). Cyclic voltammetry (CV), linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS) were carried out, indicating the excellent catalytic performance for alcohol electrooxidation can be achieved on Pt/In2O3nanocatalysts due to the multiple active sites, high conductivity and a mass of microchannels and micropores for reactant diffusions arising from 3D frame structures compared with that on the Pt/C catalysts. ? 2016 Science Press

关键词： Alcohols Catalyst activity Catalysts Chronoamperometry Cyclic voltammetry Decomposition Electrocatalysis Electrochemical impedance spectroscopy Electron microscopy Electrooxidation energy dispersive spectroscopy Ethanol High resolution transmission electron microscopy Methanol Nanoshells Nanostructured materials Nanostructures Platinum Scanning electron microscopy Transmission electron microscopy X ray diffraction X ray photoelectron spectroscopy X ray spectroscopy

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FePO4-coated Li[Li0.2Ni0.13Co0.13Mn0.54]O2 with improved cycling performance as cathode material for Li-ion batteries

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Rare Metals 2017年第11期36卷 899-904页

作者： Zhong Wang Hua-Quan Lu Yan-Ping Yin Xue-Yi Sun Xiang-Tao Bai Xue-Ling Shen Wei-Dong Zhuang Shi-Gang Lu R&D Center for Vehicle and energy Storage General Research Institute of Nonferrous Metals Beijing 100088 China China Automotive Battery Research Institue Co. Ltd Beijing 100088 China

Li[Li0.2Ni0.13Coo.13Mn0.54]O2 cathode materials were synthesized by carbonate-based co-precipitation method, and then, its surface was coated by thin layers of FePO4. The prepared samples were characterized by X-ray diffraction （XRD）, field emission scanning electron micro- scope （FESEM）, energy-dispersive spectroscopy （EDS）, and transmission electron microscopy （TEM）. The XRD and TEM results suggest that both the pristine and the coated materials have a hexagonal layered structure, and the FePO4 coating layer does not make any major change in the crystal structure. The FePO4-coated sample exhibits both improved initial discharge capacity and columbic efficiency compared to the pristine one. More significantly, the FePO4 coating layer has a much positive influence on the cycling perfor- mance. The FePO4-coated sample exhibits capacity reten- tion of 82 % after 100 cycles at 0.5℃ between 2.0 and 4.8 V, while only 28 % for the pristine one at the same charge-discharge condition. The electrochemical impe- dance spectroscopy （EIS） results indicate that this improved cycling performance could be ascribed to the presence of FePO4 on the surface of Li[Li0.2Ni0.13Co0.13Mno.54102 par- ticle, which helps to protect the cathode from chemical attacks by HF and thus suppresses the large increase in charge transfer resistance.

关键词： Cathodes Charge transfer Coated materials Coatings Crystal structure Electric batteries Electrochemical impedance spectroscopy Electrodes energy dispersive spectroscopy Field emission cathodes High resolution transmission electron microscopy Lithium Lithium alloys Lithium compounds Manganese Nickel Precipitation (chemical) Scanning electron microscopy Secondary batteries Transmission electron microscopy X ray diffraction

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Investigation on LaF_3/porous silicon system for photonic application

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Chinese Optics Letters 2010年第3期8卷 306-308页

作者： Halima Khatun Sinthia Shabnam Mou Abdul Al Mortuza Abu Bakar Md.Ismail Department of Applied Physics and Electronic EngineeringRajshahi University School of Electrical and Electronic EngineeringIndependent University

We present the investigation on LaF3/porous silicon （PS） system that has properties of both the materials to be applied in photonics. Epilayers of LaF3 are grown on PS under different anodization conditions using electron-beam evaporation （EBE）. The characteristics of the LaF3/PS system are analyzed by X-ray diffraction （XRD）, scanning electron microscope （SEM）, energy dispersive X-ray spectroscopy （EDX）, and photoluminescence （PL）. XRD confirms the polycrystalline nature of the LaFz film. Nearly stoichiometric growth of LaF3 on PS is established by EDX. Such a thin LaF3 layer grown on PS leads to a good enhancement of PL yield of PS. But with the increasing thickness of LaF3 layer, PL intensity of PS is found to decrease along with a small blue-shift.

关键词： energy dispersive spectroscopy Scanning electron microscopy X ray spectroscopy

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Study on the laser treatment of electroless Ni-P-SiC composite coatings

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Chinese Optics Letters 2006年第10期4卷 589-591页

作者：邵红红蒋小燕王兰花银群 School of Material Science and Technology Jiangsu UniversityZhenjiang 212013

Effect of the laser treatment on electroless Ni-P-SiC composite coatings was investigated. The microscopic structure, surface morphology, ingredient, and performance of the Ni-P-SiC composite coatings were synthetically analyzed by the use of X-ray diffraction apparatus, scanning electron microscope, energy distribution spectrometer, micro-hardness tester, wear tester and so on. It was found that the composite coatings did make crystalloblastic transformation after laser heating. Structural analysis confirmed that some new types of phase Ni2Si or Ni3Si compound would emerge in the Ni-P-SiC coatings after laser treatment. The micro-hardness measurement results showed that when the laser power was 450 W with scanning speed of 0.5 m/min, the hardness of the coating was superior to the coating obtained by the conventional furnace heating, and wear resistance of the composite coating after laser treating could also improve.

关键词： Composite materials energy dispersive spectroscopy Heating Laser applications Microhardness Morphology Scanning electron microscopy Structural analysis Wear resistance X ray diffraction analysis

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Integration of GaN thin films with silicon substrates by fusion bonding and laser lift-off

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Chinese Optics Letters 2006年第7期4卷 416-418页

作者：王婷郭霞方圆刘斌沈光地 Optoelectronic Technology Laboratory Institute of Electronic Information & Control Engineering Beijing University of Technology

GaN thin films grown on sapphire substrates by metalorganic chemical vapor deposition （MOCVD） are successfully bonded and transferred onto Si receptor substrates using fusion bonding and laser lift-off （LLO） technique. GaN/Al2O3 structures are joined to Si substrates by pressure bonding Ti/Au coated GaN surface onto Ti/Au coated Si receptor substrates at the temperature of 400℃. KrF excimer laser with 400-mJ/cm^2 energy density, 248-nm wavelength, and 30-ns pulse width is used to irradiate the wafer through the transparent sapphire substrates and separate GaN films from sapphire. Cross-section scanning electron microscopy （SEM） combined with energy dispersive X-ray spectrometer （EDS） measurements show that Au/Si solid solution is formed during bonding process. Atomic force microscopy （AFM） and photoluminescence （PL） measurements show that the qualities of GaN films on Si substrates degrade little after substrates transfer.

关键词： Atomic force microscopy Bonding energy dispersive spectroscopy Excimer lasers Fusion reactions Gallium nitride Metallorganic chemical vapor deposition Photoluminescence Sapphire Scanning electron microscopy Silicon Solid solutions Substrates Surfaces X ray spectrometers

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