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electrospun advanced nanomaterials for in situ transmission electron microscopy:Progress and perspectives

InfoMat 2023年第12期5卷 1-27页

作者： Jingyue Zhao Zulin Li Shiwen Lv Manxi Wang Chuanping Li Xuan Li Hongyang Chen Manxian Li Xiaochuan Chen Feifeng Wang Weiwei Fan Junxiong Wu Ziqiang Wang Xiaoyan Li Yuming Chen Engineering Research Center of Polymer Green Recycling of Ministry of Education Fujian Key Laboratory of Pollution Control&Resource ReuseCollege of Environmental and Resource Sciences and College of Carbon Neutral Modern IndustryFujian Normal UniversityFuzhouFujianthe People's Republic of China Department of Materials Science and Engineering and Department of Nuclear Science and Engineering Massachusetts Institute of TechnologyCambridgeMassachusettsUSA Institute of Materials Research Shenzhen International Graduate SchoolTsinghua UniversityShenzhenthe People's Republic of China State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of MatterChinese Academy of SciencesFuzhouFujianthe People's Republic of China

electrospun nanofibers(NFs)have shown excellent properties including high porosity,abundant active sites,controllable diameter,uniform and designable structure,high mechanical strength,and superior resistance to external destruction,which are ideal nanoreactors for in situ *** various techniques,in situ transmission electron microscopy(TEM)has enabled operando observation at the atomic level due to its high temporal and spatial resolution combined with excellent sensitivity,which is of great importance for rational materials design and performance *** this review,the basic knowledge of in situ TEM techniques and the advantages of electrospun nanoreactors for in situ TEM characterization are first *** recent development in electrospun nanoreactors for studying the physical properties,structural evolution,phase transition,and formation mechanisms of materials using in situ TEM is then *** electrochemical behaviors of carbon nanofibers(CNFs),metal/metal oxide NFs,and solidelectrolyte interphase for different rechargeable batteries are ***,challenges faced by electrospun nanoreactors for in situ TEM characterization are discussed and potential solutions are proposed to advance this field.

关键词： batteries electrospun advanced nanofibers in situ transmission electron microscopy nanoreactors

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