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Non-spherical aluminum nanoparticles fabricated using picosecond laser ablation

International Journal of Minerals,Metallurgy and Materials 2020年第7期27卷 980-986页

作者： A.Brahma Swamulu S.Venugopal Rao G.Krishna Podagatlapalli Department of Physics Rajiv Gandhi University of Knowledge TechnologiesNuzvidAndhra Pradesh 521202India Advanced Centre of Research in High Energy Materials(ACRHEM) University of HyderabadHyderabad 500046TelanganaIndia Department of Electronics&Physics Gandhi Institute of Technology and Management Institute of ScienceGandhi Institute of Technology and Management deemed to be UniversityVisakhapatnam 530045Andhra PradeshIndia

We report the picosecond laser ablation of aluminum targets immersed in a polar organic liquid(chloroform,CHCl3)with^2 ps laser pulses at an input energy of^350μ*** synthesized aluminum nanoparticles exhibited a surface plasmon resonance peak at^340 *** electron microscopy images of Al nanoparticles demonstrated the spherical morphology with an average size of(27±3.6)*** formation of smaller spherical Al nanoparticles and the diminished growth could be from the formation of electric double layers on the Al *** addition to spherical aluminum nanoparticles,triangular/pentagonal/hexagonal nanoparticles were also observed in the colloidal *** emission scanning electron microscopy images of ablated Al targets demonstrated laser induced periodic surface structures(LIPSSs),which were the high spatial frequency LIPSSs(HSF-LIPSSs)since their grating period was^280 ***,coarse structures with a period of^700 nm were observed.

关键词： ablation picosecond silver polar periodic surfaces electric double layers

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Evaluation of Intrinsic Ionization and Complexation Constants of TiO2 and Mg-Fe Hydrotalcite-like Compounds

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Chinese Journal of Chemistry 2006年第10期24卷 1336-1341页

作者：侯万国 REN Carolyn Key Laboratory for Colloid and Interface Chemistry of Education Ministry Shandong University Jinan Shandong 250100 China Environment Research Institute Shandong University Jinan Shandong 250100 China Department of Mechanical Engineering University of Waterloo 200 University Avenue West Waterloo Ontario N2L3G1 Canada

The intrinsic surface reaction constants, pKa1^int, pKa2^int, p^＊KC^int and p^＊KA^int , were evaluated by a modifieddouble extrapolation （MDE） for TiO2 without structural charge and Mg-Fe hydrotalcite-like compounds （HTlc） with structural charge, respectively. The results of intrinsic surface reaction constants for TiO2 were compared with those obtained by class double extrapolation （CDE） in literature. Furthermore, the values of intrinsic surface reaction constants obtained by MDE were used to simulate the charging behaviors of the materials. The following conclusions were obtained. For TiO2 without structural charge, the pKa1^int and pKa2^int evaluated by MDE are equal to those by CDE, however the p^＊KC^int and p^＊KA^int evaluated by MDE are much different from those by CDE. In principle, the results of the p^＊KC^int and p^＊KA^int evaluated by MDE are more accurate than those by CDE. The values of intrinsic surface reaction constants obtained by MDE can excellently simulate the charging curves for TiO2 with the triple layer model （TLM）. For HTlc with positive structural charge, the results of ^＊KC^int=0 and ^＊KA^int →∞ were obtained by MDE, which means the inert electrolyte chemical binding does not exist; the point of zero net charge （PZNC） of c-independence also exist as the same as solid without structural charge, and the PHPZNC obtained by the acid-base titration can excellently be simulated and the surface charging tendency can be simulated to a great extent using the pKa1^int and pKa2^int evaluated by MDE and the diffuse layer model （DLM）.

关键词： surface complexation electric double layers acid-base chemistry amphoteric surface

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