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The relation between ductility at high temperature and solid solution in Mg alloys

Journal of Magnesium and Alloys 2022年第1期10卷 241-256页

作者： D.F.Shi C.M.Cepeda-Jiménez M.T.Pérez-Prado IM DEA Materials Institute C/Eric Ka ridel228906 GetafeMadridSpain Department of Materials Science Polytechnic University of Madrid/Universidad Politecnica de MadridE.T.S.de Ingenieros de Caminos28040MadridSpain Department of Physical Metallurgy CENIMCSICAv.Gregorio del Amo 828040 MadridSpain

This work investigates the effect of solid solution on ductility and on the activation of individual deformation mechanisms at moderate temperatures and at quasi-static strain rates in Mg-Zn and Mg-Al alloys. With that aim, four solid solution Mg-Zn and Mg-Al binary alloy ingots containing 1 and 2 wt.% solute atoms were subjected to hot rolling and subsequent annealing to generate polycrystals with similar average grain size and basal-type texture for each composition. The activity of the different slip systems after tensile testing at 150°C and at 250°C was evaluated in pure Mg and in the alloys by EBSD-assisted slip trace analysis. In addition, segregation of Zn and Al atoms at grain boundaries during the thermo-mechanical processing was characterized by HAADF-STEM and EDX. It was found that while the addition of Al and Zn atoms to pure Mg does not lead to major changes in the mechanical strength at the investigated temperatures, it does enhance ductility significantly, especially at 250℃. Our results show that this increase in ductility cannot be attributed to a higher activation of non-basal systems in the alloys, as reported earlier, as the incidence of non-basal systems is indeed considerably higher in pure Mg. This work suggests, on the contrary, that the ductility increase may be attributed to the presence of a more homogenous basal activity in the alloys due to a lower degree of orientation clustering, to grain boundary solute segregation, and to a higher slip diffusivity at grain interiors.

关键词： Magnesium Solute segregation Slip trace analysis ductility Deformation mechanisms

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Alloying design and microstructural control strategies towards developing Mg alloys with enhanced ductility

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Journal of Magnesium and Alloys 2022年第5期10卷 1191-1206页

作者： Zhong-Zheng Jin Min Zha Si-Qing Wang Shi-Chao Wang Cheng Wang Hai-Long Jia Hui-Yuan Wang Key Laboratory of Automobile Materials of Ministry of Education&School of Materials Science and Engineering Nanling CampusJilin UniversityNo.5988 Renmin StreetChangchun 130025China International Center of Future Science Jilin UniversityChangchun 130012China State Key Laboratory of Superhard Materials Jilin UniversityChangchun 130012China

Nowadays,magnesium(Mg)alloys are promising lightweight structural materials,especially in transportation and aerospace fields,due to their inherent low density and high specific strength.Most of the high-strength Mg alloys exhibit poor formability and ductility at room temperature,which limit their wide applications.However,by proper alloying design and/or delicate microstructural control,some newly developed Mg alloys,including rare-earth(RE)and RE-free ones,show enhanced ductility without significant loss of strength.To identify the critical reasons,recent researches on ductile Mg alloys have been reviewed from the aspects of alloying design strategies and microstructural control via advanced processing technologies.Moreover,some outlooks on enhanced ductility of Mg alloys are suggested,e.***.enhancing the beneficial effect of solute atoms,introducing second phase particles,tailoring bimodal-grained structures,introducing pre-twinning structures,etc.The current research progresses in alloying design and/or novel microstructural control have shed some lights on designing and producing Mg alloys with enhanced ductility.

关键词： Mg alloys Alloying Microstructure ductility Strength

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Steel rings as seismic fuses for enhancing ductility of cross braced frames

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Earthquake Engineering and Engineering Vibration 2022年第4期21卷 1103-1117页

作者： Farhad Behnamfar Saeid Arman Hassan Zibasokhan Department of Civil Engineering Isfahan University of TechnologyIsfahan ***Iran Department of Civil Engineering Kermanshah University of TechnologyKermanshah ***Iran

A new remedy is proposed in this study to increase the ductility of cross-braced frames to a level comparable with ductile moment frames.The suggested system consists of one or two concentric steel rings installed in the cross-braced bay vertically.The steel rings are designed such that they fail in bending sooner than failure of the braces in compression.Then the rings act as seismic fuses with multiple bending plastic hinges.Using nonlinear static analysis,it is shown that the proposed system can be designed to behave like cross-braced frames with regard to stiffness and strength,and like special moment frames with regard to ductility.Seismic design factors for the proposed system are recommended based on nonlinear pushover and cyclic analysis studies.

关键词： cross brace special moment frame steel ring seismic fuse ductility

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Solute clusters-promoted strength-ductility synergy in Al-Sc alloy

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Journal of Materials Science & Technology 2022年第1期96卷 325-331页

作者： Chong Yang Pengming Cheng Baoan Chen Jinyu Zhang Gang Liu Jun Sun State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong UniversityXi’an 710049China State Key Laboratory of Advanced Power Transmission Technology Global Energy Interconnection Research Institute Co.Ltd.Beijing 102209China

Sc solute clusters with a high number density were produced in an Al-0.3 wt.%Sc alloy when aged at250℃,while fine Al_(3)Sc precipitates were predominantly formed in the same alloy aged at 300℃.The alloy strengthened by Sc solute clusters displayed higher yield strength and simultaneously greater ductility than its counterpart strengthened by Al_(3)Sc precipitates.This clearly demonstrates a superior strengthductility synergy promoted by the Sc solute clusters in Al-Sc alloys.The effects of Al_(3)Sc precipitates and Sc solute clusters on ductility were discussed in comparison by using a micromechanics fracture model.Since the Sc clusters were stabilized at 250℃,the Al-Sc alloys strengthened by Sc solute clusters should find extensive application fields within a wide temperature range,due to their high temperature resistance.

关键词： Al-Sc alloy Solute clusters Strength ductility Micromechanics model

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A superior strength-ductility synergy of Al_(0.1)CrFeCoNi high-entropy alloy with fully recrystallized ultrafine grains and annealing twins

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Journal of Materials Science & Technology 2022年第36期131卷 185-194页

作者： Jiahao Li Kejie Lu Xiaojun Zhao Xinkai Ma Fuguo Li Hongbo Pan Jieming Chen Key Laboratory of Advanced Technologies of Materials Ministry of EducationSchool of Materials Science and EngineeringSouthwest Jiaotong UniversityChengdu 610031China Shenzhen Institute of Southwest Jiaotong University Shenzhen 518000China State Key Laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China Anhui Province Key Laboratory of Metallurgical Engineering&Resources Recycling(Anhui University of Technology) 243002 MaanshanChina Luoyang Ship Material Research Institute Luoyang 471023China

Grain refinement usually makes the materials stronger,while ductility has a dramatic loss.Here,a superior tensile strength–ductility synergy in a fully recrystallized ultrafine-grained(UFG)Al_(0.1)CrFeCoNi with abundant annealing twins was achieved by cold rolling at room temperature and short-time annealing.The microstructure characterization using electron backscattered scattering diffraction demonstrates that abundant geometrically necessary dislocations(GNDs)gather around the grain boundaries and twin boundaries after tensile deformation.Although coarse-grained(CG)samples undergo a larger plastic deformation than UFG samples,the GND density decreases with grain size ranging from UFG to CG.Transmission electron microscopy results reveal that the annealing twin boundary,which effectively hinders the dislocation slip and stores dislocation in grain interior,and the activation of multiple deformation twins are responsible for the superior strength–ductility synergy and work hardening ability.In addition,the yield strength of fully recrystallized Al_(0.1)CrFeCoNi follows a Hall–Petch relationship(σ_y=24+676d^(–1/2)),where d takes into account both grain boundaries and annealing twin boundaries.The strengthening effects of grain boundaries and annealing twin boundaries were also evaluated separately.

关键词： High-entropy alloy Ultrafine grains Annealing twins Strength ductility

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Controlling Carbide Evolution to Improve the ductility in High Specific Young’s Modulus Steels

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Acta Metallurgica Sinica(English Letters) 2022年第10期35卷 1703-1711页

作者： Peng Chen Xin Xu Chao Lin Fuming Yang Jiachen Pang Xiaowu Li Hongliang Yi Department of Materials Physics and Chemistry School of Materials Science and EngineeringNortheastern UniversityShenyang110819China The State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang110819China Angang Steel Company Limited Technology Centre Anshan114009China Key Laboratory for Anisotropy and Texture of Materials Northeastern UniversityShenyang110819China

A high specific Young’s modulus steel could be achieved by introducing a large fraction of kappa-carbides(κ-carbide),and its ductility was improved by efficiency divorced eutectoid transformation(DET)treatment.For this steel,carbon and aluminum contents affect not only the carbide fraction,but also the type and morphology of carbides,and consequently the mechanical properties.In this work,the alloy was designed by considering both the carbide morphology and Young’s modulus,and the carbides in the high specific Young’s modulus steels were adjusted by controlling carbon content in a suitable range for achieving a good combination of strength and ductility.The detailed microstructure evolution process during DET reaction was studied,and it was found that a higher austenitizing temperature and the cooling rate lower than 300℃ h^(−1) are suitable.The blocky carbides could be avoided by designing the carbon content in a limited content range.The microstructure-property relationship of the experimental steels was also discussed for giving an impetus to the future development of high specific Young’s modulus steels.

关键词： κ-carbide High aluminum High carbon Divorced eutectoid transformation ductility

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Mining of lattice distortion, strength, and intrinsic ductility of refractory high entropy alloys

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npj Computational Materials 2023年第1期9卷 1814-1825页

作者： Christopher Tandoc Yong-Jie Hu Liang Qi Peter K.Liaw Department of Materials Science and Engineering Drexel UniversityPhiladelphiaPA 19104USA Department of Materials Science and Engineering University of MichiganAnn ArborMI 48109USA Department of Materials Science and Engineering University of TennesseeKnoxvilleTN 37996USA

Severe lattice distortion is a prominent feature of high-entropy alloys(HEAs)considered a reason for many of those alloys’properties.Nevertheless,accurate characterizations of lattice distortion are still scarce to only cover a tiny fraction of HEA’s giant composition space due to the expensive experimental or computational costs.Here we present a physics-informed statistical model to efficiently produce high-throughput lattice distortion predictions for refractory non-dilute/high-entropy alloys(RHEAs)in a 10-element composition space.The model offers improved accuracy over conventional methods for fast estimates of lattice distortion by making predictions based on physical properties of interatomic bonding rather than atomic size mismatch of pure elements.The modeling of lattice distortion also implements a predictive model for yield strengths of RHEAs validated by various sets of experimental data.Combining our previous model on intrinsic ductility,a data mining design framework is demonstrated for efficient exploration of strong and ductile single-phase RHEAs.

关键词： alloys ductility strength

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Enhancing strength and ductility of AlSi10Mg fabricated by selective laser melting by TiB_(2)nanoparticles

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Journal of Materials Science & Technology 2022年第14期109卷 254-266页

作者： Y.K.Xiao H.Chen Z.Y.Bian T.T.Sun H.Ding Q.Yang Y.Wu Q.Lian Z.Chen H.W.Wang State Key Laboratory of Metal Matrix Composites Shanghai Jiao Tong UniversityShanghai 200240China School of Materials Science&Engineering Shanghai Jiao Tong UniversityShanghai 200240China

In the metallic components fabricated by the emerging selective laser melting(SLM)technology,most strategies used for strengthening the materials sacrifice the ductility,leading to the so-called strengthductility trade-off.In the present study,we report that the strength and ductility of materials can be enhanced simultaneously by introducing nanoparticles,which can break the trade-off of the metallic materials.In the case of in-situ nano-TiB_(2)decorated AlSi10Mg composites,the introduced nanoparticles lead to columnar-to-equiaxed transition,grain refinement and texture elimination.With increasing content of nanoparticles,the strength increases continually.Significantly,the ductility first increases and then decreases.Our results show that the ductility is controlled by the competition between the crack-induced catastrophic fracture and ductile fracture associated with dislocation activities.The first increase of ductility is mainly attributed to the suppression of crack-induced catastrophic fracture when TiB_(2)nanoparticles present.With the further increase of TiB_(2)nanoparticles,the subsequent decrease of ductility is mainly controlled by dislocation activities.Thus,the materials will exhibit the optimum strength and ductility combination in a certain range of TiB_(2)nanoparticles.This study clarifies the physical mechanism controlling ductility for nano-TiB_(2)decorated Al Si10Mg composites,which provides the insights for the design of structural materials.

关键词： Selective laser melting Aluminium matrix composites ductility Mechanical behavior Dislocations Cracks

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Shear banding-inducedslip enables unprecedented strength-ductility combination of laminated metallic composites

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Journal of Materials Science & Technology 2022年第15期110卷 260-268页

作者： Shuang Jiang Ru Lin Peng Kristián Máthis Hai-Le Yan Gergely Farkas Zoltán Hegedues Ulrich Lienert Johan Moverare Xiang Zhao Liang Zuo Nan Jia Yan-Dong Wang Key Laboratory for Anisotropy and Texture of Materials(Ministry of Education) School of Material Science and EngineeringNortheastern UniversityShenyang 110819China Division of Engineering Materials Department of Management and EngineeringLinköping UniversityLinköping 58183Sweden Department of Physics of Materials Faculty of Mathematics and PhysicsCharles UniversityKe Karlovu 5Prague 12116Czech Republic Nuclear Physics Institute of the Czech Academy of Sciences Rež130Husinec-ˇRež25068Czech Republic Deutsches Elektronen-Synchrotron(DESY) Notkestr.85Hamburg 22607Germany Beijing Advanced Innovation Center for Materials Genome Engineering State Key Laboratory for Advanced Metals and MaterialsUniversity of Science and Technology BeijingBeijing 100083China

Shear bands in metallic materials have been reported to be catastrophic because they normally lead to non-uniform plastic deformation. ductility of laminated metallic composites deteriorates with increasing processing strain, particularly for those having hexagonal-close-packed(hcp) constituents due to inadequate slip systems and consequently prominent shear banding. Here, we propose a design strategy that counterintuitively tolerates the bands with localized strains, i.e. the shear banded laminar(SBL) structure, which promotes dislocation activation in hcp metals and renders unprecedented strengthductility combination in hcp-metal-based composites fabricated by accumulative roll bonding(ARB). The SBL structure is characterized with one soft hcp metal constrained by adjacent hard metal in which dislocations have been accumulated near the bimetal interfaces. High-energy X-ray diffraction astonishingly reveals that more than 90% of dislocations are non-basal in Ti layers of the SBL Ti/Nb composite processed by eight ARB cycles. Moreover, dislocations occupy a high fraction of ~30%, promoting further cross slip. The unique stress field tailored by both shear banding and heterophase interface-mediated deformation accommodation triggers important slip. This SBL design is of significance for developing hcp-based laminates and other heterostructured materials with high performances.

关键词： Shear band Laminated metallic composites ductility High-energy X-ray diffraction Dislocation slip

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Achieving high strength and ductility in high-entropy alloys via spinodal decomposition-induced compositional heterogeneity

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Journal of Materials Science & Technology 2023年第10期141卷 149-154页

作者： Yujie Chen Yan Fang Ruixin Wang Yu Tang Shuxin Bai Qian Yu Department of Materials Science and Engineering Center of Electron Microscopy and State Key Laboratory of Silicon MaterialsZhejiang UniversityHangzhou 310027China College of Aerospace Science and Engineering National University of Defense TechnologyChangsha 410073China

The compositional heterogeneity in high-entropy alloys(HEAs)has been reported to be an inherent en-tity,which significantly alters the mechanical properties of materials by tuning the variation of lattice resistance for dislocation motion.However,since the body-centered cubic(BCC)structure is not close-packed,the change of lattice resistance is less sensitive to the normal concentration wave compared to that in face-centered cubic(FCC)structured materials.In this work,we selected a refractory bcc HEAs TiZrNbTa for the matrix and added a small amount of Al to facilitate the special spinodal decomposition structure.In particular,(TiZrNbTa)98.5 Al 1.5 displayed a typical basket-weave fabric morphology of spinodal decomposition structure with a characteristic periodicity of∼8 nm and had an optimal combination of strength and ductility(the yield strength of 1123±9 MPa and ductility of∼20.7%±0.6%).It was de-termined that by doing in situ TEM mechanical testing,the plastic deformation was dominated by the formation and operation of dislocation loops which provided both edge and screw components of dislo-cations.The synergetic effect of the remarkable chemical heterogeneity created by the spinodal decompo-sition and the spreading lattice distortion in high entropy alloys is quite effective in tuning the mobility of different types of dislocations and facilitates dislocation interactions,enabling the combination of high strength and ductility.

关键词： Bcc high-entropy alloys Spinodal decomposition Compositional heterogeneity Dislocation loops High strength ductility

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