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Metal-organic frameworks:Synthetic methods for industrial production

Nano Research 2023年第5期16卷 7906-7925页

作者： Dou Ma Xin Huang Yu Zhang Lu Wang Bo Wang Frontiers Science Center for High Energy Material Beijing Key Laboratory of Photoelectronic/Electrophotonic Conversion MaterialsKey Laboratory of Cluster ScienceSchool of Chemistry and Chemical EngineeringBeijing Institute of TechnologyBeijing 100081China Advanced Technology Research Institute(Jinan) Beijing Institute of TechnologyJi’nan 250000China Beijing Institute of Technology Library Beijing Institute of TechnologyBeijing 100081China

Metal-organic frameworks(MOFs),which are constructed by metal ions or clusters with organic ligands,have shown great potential in gas storage and separation,luminescence,catalysis,drug delivery,sensing,so on.More than 20,000 MOFs have been reported by adjusting the composition and reaction conditions,most of them were synthesized by hydrothermal or solvothermal methods.The conventional solvothermal methods are favorable for the slow crystallization of MOFs to obtain single crystals or highly crystalline powders,which are suitable for the structure analysis.However,their harsh synthesis conditions,long reaction time,difficulty in continuous synthesis limit their scale-up in industrial production and application.Meanwhile,shaping or processing is also required to bring MOF crystals and powders into the market.Therefore,this review demonstrates the crystallization mechanisms of MOFs to understand how the synthetic parameters affect the final products.Additionally,a variety of promising synthetic routes which can be used for large scale synthesis were reviewed in details.Lastly,the prospects of MOF shaping and processing are provided to promote their industrial application.

关键词： metal-organic frameworks synthetic methods crystallization mechanisms scale-up

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