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Degradable magnesium-hydroxyapatite interpenetrating phase composites processed by current assisted metal infiltration in additive-manufactured porous preforms

引用

Journal of Magnesium and Alloys 2022年第12期10卷 3641-3656页

作者： Mariano Casas-Luna Edgar B.Montufar Norbert Hort Sebastian Díaz-de-la-Torre JoséClaudio Méndez-García Lucie Vištejnová Adam Brínek AlešDanhel Karel Dvorak Jozef Kaiser Ladislav Celko Central European Institute of Technology Brno University of TechnologyPurkynova 123Brno 61200Czech Republic Institute of Metallic Biomaterials Helmholtz-Zentrum HereonMax-Planck-Straße 1Geesthacht 21502Germany Institute of Product and Process Innovation Leuphana University LüneburgUniversitätsallee 1Lüneburg 21335Germany Centro de Investigación e Innovación Tecnológica Instituto Politécnico NacionalCerrada de Cecati s/nMexico City 02250Mexico Biomedical Center Faculty of Medicine in PilsenCharles UniversityAlej Svobody 1655/76Plzen 32300Czech Republic Institute of Biophysics of the Czech Academy of Sciences Královopolská135Brno 61265Czech Republic Faculty of Civil Engineering Brno University of TechnologyPurkynova 139Brno 61200Czech Republic

This work explores ceramic additive manufacturing in combination with liquid metal infiltration for the production of degradable interpenetrating phase magnesium/hydroxyapatite(Mg/HA) composites. Material extrusion additive manufacturing was used to produce stoichiometric,and calcium deficient HA preforms with a well-controlled open pore network, allowing the customization of the topological relationship of the composite. Pure Mg and two different Mg alloys were used to infiltrate the preforms by means of an advanced liquid infiltration method inspired by spark plasma sintering, using a novel die design to avoid the structural collapse of the preform. Complete infiltration was achieved in 8 min, including the time for the Mg melting. The short processing time enabled to restrict the decomposition of HA due to the reducing capacity of liquid Mg. The pure Mg-base composites showed compressive yield strength above pure Mg in cast state. Mg alloy-based composites did not show higher strength than the bare alloys due to grain coarsening, but showed similar mechanical properties than other Mg/HA composites that have significantly higher fraction of metallic phase. The composites showed faster degradation rate under simulated body conditions than the bare metallic component due to the formation of galvanic pairs at microstructural level. Mg dissolved preferentially over HA leaving behind a scaffold after a prolonged degradation period. In turn, the fast production of soluble degradation products caused cell metabolic changes after 24 h of culture with not-diluted material extracts. The topological optimization and reduction of the degradation rate are the topics for future research.

关键词： Interpenetrating phase composite Biodegradable metal Topological relationship Direct ink writing Metal infiltration computed aided design

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RESEARCH ON THE 3-AXES ROUGH MILLING OF MULTI-SURFACES

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Chinese Journal of Aeronautics 1997年第4期10卷 70-75页

作者： Liu Zhuang, Zhang Deqiang, Zhou Laishui, Zhou Rurong (Research Center of CAD/CAM Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing, 210026, China)

In particular, a fair amount of the machining time may be spent in rough cutting process when a large portion of the raw material has to be removed. Therefore, an algorithm for generating the toolpath for rough cutting is suggested in the paper. The algorithm is based on an extended tracing method for plane/surface intersection is proposed for smooth surface. A 2.5D milling or parallel offset machining is to be used to significantly improve producitvity and lead to lower production costs for the sculptured multi surfaces part rough machining..

关键词： computed aided design computer aided manufacturing numerical control machining rough machining toolpath generation

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