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The Adsorption Properties of TEMPO Oxidized Cellulose against the Mixture of Methylene Blue and Rhemazol Yellow FG

Journal of Renewable Materials 2024年第8期12卷 1369-1382页

作者： I.Putu Mahendra Kartika Dinita Program Studi Kimia Fakultas SainsInsitut Teknologi SumateraJalan Terusan RyacuduWay HuwiJati AgungLampung Selatan35365Indonesia

TEMPO/NaOCl/NaBr treatment significantly increased the number of negative charges on the cellulose *** concentrations of NaOCl,5 and 30 mmol/g of cellulose,were used in this *** number of carboxyl groups in the two cellulosic samples oxidized using TEMPO/NaOCl/NaBr was 0.5160 and 1.8461 mmol/g of cellulose,*** oxidized cellulose samples treated with 5 and 30 mmol/g NaOCl exhibited higher crystallinity,at 81.15%and 80.14%,respectively,compared to untreated cellulose,which had a crystallinity of 75.95%.The pH effect indicated that the highest adsorption capacity for methylene blue was achieved under alkaline conditions(pH 9),while the highest adsorption capacity for rhemazol yellow FG was achieved under acidic *** kinetic model of TEMPO-oxidized cellulose for methylene blue and rhemazol yellow FG conformed to the pseudo-second-order *** initial concentration parameter revealed that the isotherm model for the adsorption of methylene blue and rhemazol yellow FG by TEMPO-oxidized cellulose conformed to the Langmuir *** dye removal efficiencies for methylene blue and rhemazol yellow FG using TEMPOoxidized cellulose(30 mmol/g)were approximately 80.17%and 59.52%,*** results demonstrate that TEMPO/NaOCl/NaBr-oxidized samples can effectively separate cationic and anionic dye ***,the use of TEMPO-oxidized cellulose showed good regeneration capability,maintaining more than 95%of its adsorption capacity after 8 cycles.

关键词： Cellulose TEMPO oxidation cationic and anionic dyes dye separation

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Preparation of Fe-Mg MOFs and Its Application in Removal of RhB and MO

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Journal of Geoscience and Environment Protection 2022年第4期10卷 167-180页

作者： Onyeka Samuel Ojinna Yueli Wen Bin Wang Chengda Li Wei Huang Ikeh Justin Tobechukwu College of Environmental Science and Engineering Taiyuan University of Technology Taiyuan China State Key Laboratory of Clean and Efficient Coal Utilization Taiyuan University of Technology Taiyuan China Coal Conversion Technology & Engineering Co. Ltd. Taiyuan University of Technology Taiyuan China Geological Resources and Geological Engineering Taiyuan University of Technology Taiyuan China

The world wide application of dyes in papermaking, fabric, lithography, leather and other industrial production, has attracted more attention, due to water pollution caused by these organic dyes. Metal-organic frameworks (MOFs) which are a physical adsorption method of wastewater treatment are a kind of special three-dimensional crystal-like constituents built by multipurpose ligands and metallic ion classes, showing an advantage in removal of pollutants from solutions because of its unique properties are convenient for operation, high removal efficiency, and low cost. In this study, we investigated Fe-Mg based metal organic framework, Fe-Mg MOFs which was directly synthesized by the hydrothermal method. The obtained materials were analyzed with XRD, FT-IR, TG-DTG, SEM etc. and used for the treatment of printing and dyeing wastewater. The results showed that it has good adsorption performance for cation dye rhodamine B (RhB) and anion dye methyl orange (MO) in a wide pH range. The Fe-Mg MOF even after the 4th run, the Fe-Mg MOF catalyst still maintained nearly the initial catalytic activities. The kinetic studies revealed the adsorption process of the both contaminants obeys a pseudo-second order model. In addition, the equilibrium adsorption data of RhB and MO are in good agreement with Langmuir models. The maximum adsorption capacities are 694.44 and 236.97 mg/g at 308 K respectively. This work synthesizes a promising dual-functional adsorbent that can remove cationic and anionic dyes, which provide potential applications for actual wastewater treatment.

关键词： Metal-Organic Frameworks (MOFs) Adsorption cationic and anionic dyes Wastewater Treatment

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