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Advances in microwave assisted synthesis of ordered mesoporous materials

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中国有色金属学会会刊：英文版 2009年第S3期19卷 656-664页

作者：曹渊魏红娟夏之宁 College of Chemistry and Chemical Engineering Chongqing University College of Bioengineering Chongqing University

Mesoporous materials with uniform pores and high specific areas are used in many fields including catalysts, separation and adsorbents, etc. In order to find faster and more economical synthesis routes, the use of microwave heating was deeply studied. Compared to the hydrothermal method, microwave energy can heat the samples to crystallization temperature rapidly and uniformly result in homogeneous nucleation and shorten crystallization time. The basic principles of microwave assisted synthesis and advantages of microwave heating, and the obtained progress concerning ordered mesoporous materials through microwave synthesis were summarized.

关键词： microwave assisted synthesis ordered mesoporous materials (OMMs) ordered mesoporous silicas (OMSs) periodic mesoporous organosilicas (PMOs)

Rapid Microwave assisted Synthesis and Antiproliferative Evaluation of Novel Steroidal Thiazole Derivatives

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Chemical Research in Chinese Universities 2017年第2期33卷 206-212页

作者： HUANG Yanmin ZHAO Dandan LIU Chang GAN Chunfang ZHAN Junyan LIN Qifu SHI Haixin CUI Jianguo College of Chemistry and Material Science Guangxi Teachers Education University Nanning 530001 P. R. China Guangxi Colleges and University Key Laboratory of Beibu Gulf Oil and Natural Gas Resource Effectfve Utffizat~'on Qizhou University Qizhou 535011 P. R. China

Three series of novel steroidal thiazole derivatives were synthesized by microwave assisted one-potreaction from pregnenolone, testosterone and estrone, respectively. Their structures were characterized by IR, NMRand HRMS, and the antiproliferative activities of all the synthesized compounds against human cervical carcinoma（HeLa）, human liver carcinoma（HepG2）, human lung carcinoma（A549）, nasopharyngeal carcinoma（CNE2） andnormal kidney epithelial cells（HEK293T） were screened. Among the compounds, 1-estron-17＇-ylidene-2-[4＇-（p-bromophenyl）-2＇-thiazol]hydrazone（12） displayed distinct antiproliferative activity against all the tested cancercell lines and was almost inactive to normal kidney epithelial cells.

关键词： Microwave assisted synthesis Pregnenolone Testosterone Estrone Steroidal thiazole derivative

Microstructure and Tribological Behavior of Cr-Cu-N Coatings Deposited by Ion Beam assisted Magnetron Sputtering

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稀有金属材料与工程 2012年第S1期41卷 355-358页

作者： Tian Linhai Zhang Yang Yang Yaojun Zhu Xiaodong Tang Bin Taiyuan Univ Technol Res Inst Surface Engn Taiyuan 030024 Peoples R China Xi An Jiao Tong Univ State Key Lab Mech Behav Mat Xian 710049 Peoples R China

Cr-Cu-N coatings with copper content from 0 at%to 6.8 at%were deposited on silicon and M2 steel by ion beam assisted magnetron sputtering.The microstructure and composition of the coatings were characterized using SEM,GDOES,XRD and XPS.The mechanical properties of the coatings were tested on a standard hardness tester.The tribological behavior of the coatings in dry wear condition was studied by means of ball-on-disc wear test.The experimental results show that addition of copper can restrict the columnar crystal growing to a certain degree.XRD and XPS analysis indicate that coatings are mainly composed of Cr and CrN phase.Cu is mainly existed in a free state in the coatings.Copper adding has no obvious effects on the hardness of the coatings.However,the coatings fracture toughness can be improved by doped copper.The coefficient of friction of the coatings against bearing steel is in the range of 0.25-0.6 changing with the copper content.The coating with 2.6 at%copper shows the lowest coefficient of friction about 0.25 and wear rate which is about one tenth of that of the coating with 6.8 at%copper.The higher coefficient of friction and wear rate of the coating with 6.8at%copper may be attributed to its lower bonding strength.

关键词： Cr-Cu-N coatings ion beam assisted magnetron sputtering microstructure tribological behavior

A Review of Ion Beam assisted Deposition of Thermal Barrier Coatings

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稀有金属材料与工程 2011年第S4期40卷 215-217页

作者： Liu Liang1,2,Gao Wei2,Zhang Huafang2,Lei Xingen2,Cui Xiangzhong2,Zheng Yufeng1 1Centre for Biomedical Materials and Engineering,Harbin Engineering University,Harbin 150001,China2Science and Technology on Power Beam Processes Laboratory,AVIC Beijing Aeronautical Manufacturing Technology Research Institute,Beijing 100024,China Harbin Engn Univ Ctr Biomed Mat & Engn Harbin 150001 Peoples R China AVIC Beijing Aeronaut Mfg Technol Res Inst Sci & Technol Power Beam Proc Lab Beijing 100024 Peoples R China

Ion beam assisted deposition (IBAD) technology has been employed more and more in the fabrication of films and/or coatings,especially in the composite system.In the present work,after the introduction about IBAD,the latest development of IBAD in thermal barrier coatings (TBCs) is briefly summarized and the future trend is also concluded.

关键词： ion beam assisted deposition ion source thermal barrier coatings thermal conductivity

Harmony search optimization applied to reservoir engineering assisted history matching

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Petroleum Exploration and Development 2020年第1期47卷 154-160页

作者： SHAMS Mohamed EL-BANBI Ahmed SAYYOUH Helmy Dana Gas Plot 188City Center5th SettlementNew Cairo11835 Egypt Petroleum Engineering Department AUC/Cairo UniversityNew Cairo/Giza11835/12613 Egypt Petroleum Engineering Department Cairo UniversityGiza12613 Egypt

Based on the analysis of characteristics and advantages of HSO(harmony search optimization) algorithm, HSO was used in reservoir engineering assisted history matching of Kareem reservoir in Amal field in the Gulf of Suez, Egypt. HSO algorithm has the following advantages:(1) The good balance between exploration and exploitation techniques during searching for optimal solutions makes the HSO algorithm robust and efficient.(2) The diversity of generated solutions is more effectively controlled by two components, making it suitable for highly non-linear problems in reservoir engineering history matching.(3) The integration between the three components(harmony memory values, pitch adjusting and randomization) of the HSO helps in finding unbiased solutions.(4) The implementation process of the HSO algorithm is much easier. The HSO algorithm and two other commonly used algorithms(genetic and particle swarm optimization algorithms) were used in three reservoir engineering history match questions of different complex degrees, which are two material balance history matches of different scales and one reservoir history matching. The results were compared, which proves the superiority and validity of HSO. The results of Kareem reservoir history matching show that using the HSO algorithm as the optimization method in the assisted history matching workflow improves the simulation quality and saves solution time significantly.

关键词： reservoir engineering assisted history matching optimization algorithm harmony search optimization algorithm

Microwave assisted hydrothermal synthesis of tin niobates nanosheets with high cycle stability as lithium-ion battery anodes

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Chinese Chemical Letters 2019年第3期30卷 771-774页

作者： Xingang Kong Jiarui Zhang Jianfeng Huang Jiayin Li Yi Qin Ting Zhao Qi Feng School of Materials Science and Engineering Shaanxi University of Science and technology Department of Advanced Materials Science Faculty of Engineering Kagawa University

In this study, SnNb_2O_6 and Sn_2Nb_2O_7 nanosheets are synthetized via microwave assisted hydrothermal method, and innovatively employed as anode materials for lithium-ion battery. The SnNb_2O_6 electrode exhibits high reversible capacity and excellent cycling stability(498 mAh/g at 0.1 A/g after 100 cycles),which is superior to that of Sn_2Nb_2O_7 electrode(173 mAh/g at 0.1 A/g after 100 cycles). Even increasing the current density to 2.0 A/g, the SnNb_2O_6 electrode still delivers a reversible capacity up to 306 mAh/g.The rate performance of the SnNb_2O_6 electrode is also better than that of Sn_2 Nb_2O_7 electrode at different current densities from 0.1 A/g to 2.0 A/g. The enhanced electrochemical performance of SnNb_2O_6 nanosheets can be attributed to the unique layered structure, which is conducive to the diffusion of the lithium ions and the migration of electrons during discharge/charge.

关键词： Tin niobates nanosheets Microwave assisted hydrothermal Anode materials Lithium ion batteries Layered structure

Ultrasound-assisted extraction of antioxidant polyphenolic compounds from Nephelium lappaceum L.(Mexican variety) husk

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Asian Pacific Journal of Tropical Medicine 2018年第12期11卷 676-681页

作者： Adriana Méndez-Flores Ayerim Hérnandez-Almanza Aidé Sáenz-Galindo Jesús Morlett-Chávez Cristóbal N Aguilar Juan Ascacio-Valdés Bioprocesses and Bioproducts Research Group Food Research Department School of Chemistry Autonomous University of Coahuila Organic Chemistry Department School of Chemistry Autonomous University of Coahuila Molecular Biology Laboratory School of Chemistry Autonomous University of Coahuila

Objective: To reach the recovery and identification of antioxidant polyphenolic compounds from Nephelium lappaceum L.(Mexican variety) husk using ultrasound-assisted extraction and liquid chromatography/mass spectrometry as well as the in vitro antioxidant activity. Methods: Rambutan husk extracts were obtained by ultrasound-assisted extraction, mass/volume ratio, water/ethanol percentage and extraction time were evaluated. Once the best extraction condition of polyphenolic compounds was defined, a polyphenolic fraction was recovered using Ambetlite XAD-16. The total content of antioxidant polyphenolic compounds was determined by summation of the total hydrolysable polyphenol and total condensed polyphenol contents. Recovered compounds were identified by FTIR(ATR) spectroscopy and HPLC/ESI/MS. The antioxidant activity was carried out by ABTS, DPPH and lipid oxidation inhibition in vitro methods. Results: In Mexican variety rambutan husk, the total polyphenolic content was 487.67 mg/g, after ultrasound-assisted extraction. According to the HPLC/ESI/MS analysis 12 antioxidant polyphenolic compounds were identified, mostly ellagitannins such as geraniin, corilagin and ellagic acid. The antioxidant activity determined by ABTS, DPPH and lipid oxidation inhibition methods was demonstrated. The main functional groups of the identified compounds were determined by FTIR analysis. Conclusions: It was demonstrated that ultrasound-assisted extraction was effective and allowed the extraction and recovery of antioxidant polyphenolic compounds. Furthermore Mexican variety rambutan husk is an important source for recovering polyphenolic compounds with antioxidant activity, these compounds have potential application for the treatment/prevention of various diseases related to cancer and pathogenic microorganisms.

关键词： Mexican variety rambutan Ultra-sound assisted extraction Antioxidant polyphenolic compounds HPLC/ESI/MS

Recent developments in computer assisted rehabilitation environments

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Journal of Medical Colleges of PLA(China) 2014年第3期29卷 137-142页

作者： Rob van der Meer Meer Health Ri?nzistraat 41 2555 JT ‘s-Gravenhage Netherlands

Computer assisted Rehabilitation Environment(CAREN) is a system that integrates a training platform(motion base), a virtual environment, a sensor system(motion capture) and D-flow software. It is useful for both diagnostic and therapeutic use. The human gait pattern can be impaired due to disease, trauma or natural decline. Gait analysis is a useful tool to identify impaired gait patterns. Traditional gait analysis is a very time consuming process and therefore only used in exceptional cases. With new systems a quick and extensive analysis is possible and provides useful tools for therapeutic purposes. The range of systems will be described in this paper, highlighting both their diagnostic use and the therapeutic possibilities. Because wounded warriors often have an impaired gait due to amputations or other extremity trauma, these systems are very useful for military rehabilitative efforts. Additionally, the virtual reality environment creates a very challenging situation for the patient, enhancing their rehabilitation experience. For that reason several Armed Forces have these systems already in use. The most recent experiences will be discussed; including new developments both in the extension of the range of systems and the improvement and adaptation of the software. A new and promising development, the use of CAREN in a special application for patients with posttraumatic stress disorder(PTSD), will also be reviewed.

关键词： Computer assisted rehabilitation environment Virtu

Live birth rates of assisted reproductive technology treatment and spontaneous conception among subfertile couples in Singapore: A follow-up study

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Asian pacific Journal of Reproduction 2018年第5期7卷 206-213页

作者： Ho Lee Mee de Souza Nurun Nisa Lee Shaw Ni Yu Su Ling Centre for assisted Reproduction Department of Obstetrics and GynaecologySingapore General HospitalSingapore Centre for Quantitative Medicine Duke-NUS Medical School SingaporeSingapore Epidemiology Department Singapore Clinical Research InstituteSingapore

Objective: To explore the potential predictors of a live birth (LB) outcome among subfertile couples of Asian ethnicity undergoing the first fertility treatment cycle;to assess the cumulative live birth rates after successive cycles;and to determine the incidence rate of spontaneous conception (SC).Methods:Subfertile couples were grouped according to treatment modalities at the first fertility treatment cycle: intrauterine insemination (IUI),in vitro fertilization (IVF), intracytoplasmic sperm injection (ICSI) and no treatment, and were followed-up for duration up to seven years. Multivariable logistic regression analysis was used for statistical analyses. Results: Age of female subjects [35-38 years, odds ratio (OR): 0.39;≥39 years, OR: 0.14], uterine factor subfertility (OR: 5.24), and treatment modalities (ORs: IUI 0.25, IVF 2.33 and ICSI 1.91) significantly predicted a LB outcome (P<0.05). The cumulative live birth rates were 11.7% IUI, 41.5% IVF, 27.5% ICSI and 22.6% from frozen embryo transfer cycles. The cumulative SC rate was 24.6% in the non-treated group and 10.7% in the treated group. All LBs from IVF cycles were delivered by the second cycle and within four years, compared to SC delivery of within five years in the non-treated group and six years in the treated group. Conclusions:Age of female subject, uterine factor and modalities of treatment are significant predictors for LB outcome at the first cycle. Higher delivery rates could be achieved following fewer successive IVF cycles and within a shorter duration compared to SC.

关键词： assisted reproductive technology Semen parameters Sperm hyaluronan-binding assay Spontaneous conception Subfertile Asian couples