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adhesion and corrosion resistance of polycaprolactone coating on NiTi alloy surface after alkali heat pretreatment

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Biosurface and Biotribology 2022年第4期8卷 307-314页

作者： Zhihui Zhang Yanan Yang Yunting Guo Pengwei Sha Zezhou Xu Zhenglei Yu Jiashun Si Zhengao Zhang Jia Guo Yifan Chen Key Laboratory of Bionic Engineering Ministry of EducationJilin UniversityChangchunChina Weihai Institute for Bionic Jilin UniversityWeihaiChina State Key Laboratory of Automotive Simulation and Control Jilin UniversityChangchunChina Beijing Reserarch Institute of Automation for Machinery Industry Co. LtdBeijingChina Key Laboratory of Automobile Materials Ministry of EducationCollege of Materials Science and EngineeringJilin UniversityChangchunChina

Selective laser melting of nickel-titanium alloy(SLM-NiTi)can precisely control the size of the sample molding structure and has attracted extensive attention due to its special superelasticity and shape memory effect.However,the biological inertness and poor corrosion resistance of SLM-NiTi alloy limit their wide application as biomedical implant materials.In this study,polycaprolactone(PCL)coating was prepared on SLM-NiTi alloy by dipping and pulling method,and the effects of alkali heat pretreatment on the morphology,adhesion,corrosion resistance,long-term stability and biomineralisation of the PCL coatings were investigated.The results showed that PCL coating can substan-tially improve the performance of SLM-NiTi alloy,and the PCL coating after alkali heat pretreatment has higher adhesion(increased from 1,747 to 2,498 mN)and lower corrosion current density(reduced by about an order of magnitude compared to PCL coating alone).In addition,the necessary stability,biomineralisation and biocompatibility ability of coatings were also further improved.Therefore,the alkali heat pretreated PCL-coated SLM-NiTi alloy has good application prospects in implants due to its superior properties.

关键词： adhesion alkali heat pretreatment corrosion resistance PCL coating SLM-NiTi alloy

A Bioinspired Adhesive Sucker with Both Suction and adhesion Mechanisms for Three-Dimensional Surfaces

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Journal of Bionic Engineering 2022年第6期19卷 1671-1683页

作者： Jing Li Zhenzhen Song Chuandong Ma Tonghang Sui Peng Yi Jianlin Liu College of Mechanical and Electrical Engineering China University of Petroleum(East China)Qingdao266580China College of Pipeline and Civil Engineering China University of Petroleum(East China)Qingdao266580China

There are significant advantages to investigate underwater attachments,which would be valuable in providing inspirations and design strategies for multi-functional surfaces and underwater robots.Here,an abalone-inspired sucker integrating an elastic body and a membrane structure is proposed and fabricated filled with rigid quartz particles to adjust the backing stiffness of the contact like abalone.The membrane is used to conform and contact surfaces well,the center area of which can be pulled in exposed to a negative pressure differential,to create a suction cavity.The pulling experiments indicate that the sucker can adhere to three-dimensional surfaces with both suction and adhesion mechanisms in both dry and liquid environments.The switching between soft/hard contact states leads to the change of adhesive strength over 30 times.Furthermore,we provide theoretical analysis on how the sucker work well in both dry and liquid environments.Finally,the developed sucker can easily lift up smooth planar objects and 3D objects,and can grip objects both smaller and larger than the size of the sucker,which have a difficulty for conventional suckers or friction-based grippers.The potential application of the sucker in flexible transfer robot is demonstrated on various surfaces and environments,paving the way for further bio-inspired adhesive designs for both dry and wet scenarios.

关键词： adhesion Sucker Abalone Suction Jamming Bioinspired

High-adhesion anionic copolymer as solid-state electrolyte for dendrite-free Zn-ion battery

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Nano Research 2022年第8期15卷 7190-7198页

作者： Jiaxu Li Junfeng Ren Caixia Li Pengxian Li Tingting Wu Shiwei Liu Lei Wang State Key Laboratory Base of Eco-chemical Engineering Taishan Scholar Advantage and Characteristic Discipline Team of Eco-chemical Process and TechnologyQingdao University of Science and TechnologyQingdao 266042China College of Chemical Engineering Qingdao University of Science and TechnologyQingdao 266042China College of Environment and Safety Engineering Qingdao University of Science and TechnologyQingdao 266042China

To conquer severe dendrites formation and side reactions of zinc metal anodes,which are serious obstacles for the practical applications of aqueous zinc ion battery(ZIB),herein,we develop a sodium allysulfonate(SAS)and acrylamide(AM)copolymer by radical polymerization process(crosslinking of C=C)as solid-state electrolyte.The interface kinetics is improved remarkably due to the high adhesion and excellent ion transferability of AM-SAS(AS)copolymers.Especially the sulfonic acid group in the hydrogel electrolyte can enhance the internal ionic conductivity effectively benefiting from its high affinity to Zn^(2+).Also,polymer chains realize re-regulation to Zn^(2+)flow in atomic-scale,thus leading to controllable deposition of Zn onto the dendrite-free Zn anodes.Consequently,the AS-1.5 electrolyte achieves ultra-stable Zn deposition/stripping behaviors with the lifespan over 1,000 h via the suppression of side-reactions and paralleled Zn deposition.High performances of Zn/Mn-doped V_(2)O_(5)(MnVO)(over 500 cycles)and Zn/diquinoxalino[2,3-a:2',3'-c]phenazine(HATN)(over 2,500 cycles)full cells demonstrate that the AS hydrogel electrolyte is a common approach for ZIBs under various conditions.This molecular regulation engineering opens a novel route for hydrogel electrolyte fabrication,where sulfonic groups perform as media of Zn^(2+)transfer.Therefore,high bulk ionic conductivity as well as excellent interface ion diffusion ability is obtained.

关键词： copolymer adhesion ionic conductivity dendrite-free interface kinetics

Contact Electrification and adhesion Between Carbon Nanotube and Graphene on Metal Surfaces: Insights from First-principles Study

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Journal of Bionic Engineering 2022年第1期19卷 103-112页

作者： Jing Tao Linfeng Wang Jin Li Zhendong Dai Jiangsu Provincial Key Laboratory of Bionic Functional Materials College of Mechanical and Electrical EngineeringNanjing University of Aeronautics and AstronauticsNanjing210016China College of Aerospace Engineering Nanjing University of Aeronautics and AstronauticsNanjing210016China

The effect of contact electrification on adhesion has been debated in recent years for gecko and bio-inspired dry adhesion material.To understand the fundamentals of this issue for Carbon Nanotube(CNT)dry adhesives,contact electrification and its relationship with adhesion are systematically studied using the first-principles calculation.Charge transfers from CNT or its special form,graphene,to the metal surface during the contact,and the transferred charge linearly correlates with the work function difference.Meanwhile,the adhesion energy is linearly related to the transferred charge for both CNT and graphene.More charge transfers from the flat graphene to metal surfaces than the curved CNT,leading to higher adhesion between graphene and metal surfaces.The curved structure of the CNT causes an irregular change of charge at the interface and hinders the charge transfer.Moreover,the curved structure induces electronic localization,which also decreases the interfacial charge transfer.The structure affects contact electrification,and hence adhesion is further demonstrated by the CNT with different deformation when contacting different surfaces.This study advances our understanding of contact electrification and its relationship with adhesion at the interface for bio-inspired carbon adhesive materials and sheds light on the control of them for engineering applications.

关键词： Contact electrification adhesion Bio-inspired adhesive CNT First-principles calculation Interfacial interaction

The Effect of Printing Parameters and Wood Surface Preparation on the adhesion of Directly 3D-Printed PLA on Wood

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Journal of Renewable Materials 2022年第7期10卷 1787-1796页

作者： Daša KrapežTomec Angela Balzano JureŽigon MilanŠernek Mirko Kariž Department of Wood Science and Technology Biotechnical FacultyUniversity of LjubljanaLjubljana1000Slovenia

As additive manufacturing technologies advance,new opportunities are opening up for their application in the furniture industry.Wood remains one of the leading raw materials in the furniture industry;therefore,possible options for combining it with 3D printing have been researched.The bonding of 3D-printed polymer parts with wood or 3D printing with wood-plastic composites is already known,but in our research we attempted to directly 3D print polylactic acid(PLA)on wood surfaces.The effect of printing parameters,as well as the surface preparation of wood on the shear strength of the bond between wood and on-printed material was tested.Microscopic images of cross-sections of samples were analyzed.The results show that with a lower initial layer thickness(0.1 mm),a higher printing temperature(220℃),and with the use of polyvinyl acetate(PVAc)primer on the wood surface before 3D printing,a higher bond strength(5.4 MPa)was achieved,but the values for the bond strength remain low compared to the conventional bonding of wood to wood with PVAc adhesive(around 10 MPa).Microscopy studies revealed barely visible penetration of PLA into the lumens of the wood cells.However,the PVAc adhesive used as primer penetrated more into the cell lumens and served as interface layer between deposited melted PLA and the wood,thus creating stronger joints.

关键词： FDM direct 3D printing adhesion printing parameters wood PLA PVAc

Effect of spatial configuration on adhesion of 1,2-disubstituted cyclohexane derivatives

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中国化学快报:英文版 2023年第8期34卷 196-200页

作者： Qiao Zhang Yuhang Yin Jingfu Song Gai Zhao Shengyi Dong College of Chemistry and Chemical Engineering Hunan UniversityChangsha 410082China State Key Laboratory of Mechanics and Control of Mechanical Structures Nanjing University of Aeronautics and AstronauticsNanjing 210016China

Spatial configuration has a significant effect on chemical self-assembly.However,the importance of spatial configuration in supramolecular adhesive materials has been frequently ignored.In this study,the effects of the spatial configuration on cohesion and adhesion were investigated.Owing to the diversities of the chemical structures and assembly patterns,1,2-disubstituted cyclohexane derivatives were used in this combined experimental and theoretical investigation.The self-sorting assembly of enantiopure isomers improved cohesion but had a negative effect on adhesion.In contrast,racemic mixtures displayed stronger adhesion effects.Moreover,it was proven that the cis-configuration was more favorable for supramolecular adhesion than the trans-counterpart.In addition,the influence of the spatial configuration of 1,2-disubstituted cyclohexane derivatives could be effectively mitigated by hydrogen bond donors or acceptors.The addition of natural acids yielded three-dimensional polymeric networks,in which the spatial configuration was not the decisive factor for supramolecular adhesion.

关键词： Spatial configuration Supramolecular adhesive material Assembly Cohesion adhesion

Preparation and Properties of Spray Polyurea Elastomer for Aquaculture Foam Floating Balls

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Agricultural Biotechnology 2024年第2期13卷 38-42页

作者： Guifang HUANG Guanyuan WEI Shengjun WEI Lan DING Wenhong CAI Bolin PAN Fisheries Research Institute of Fujian Xiamen 361013China

[Objectives] This study was conducted to develop a polyurea elastomer which can be sprayed on the surface of expanded polystyrene (EPS) floating balls, so as to improve the surface strength and service life of the floating balls. [Methods] The effects of the types and amounts of isocyanate, chain extenders and polyether polyols on the gelation rate, adhesion and wear resistance of polyurea elastomer were investigated, and it was finally determined the preparation process of polyurea elastomer using liquid isophorone diisocyanate (IPDI) and amino-terminated polyether (D2000) as the main raw materials, dimethylthiotoluene diamine (E300) as the chain extender and silica as the wear resistance modifier through two-step solution polymerization of prepolymerization and chain extension. [Results] The physical properties and chemical resistance tests of spray polyurea elastomer showed that it had good physical properties and acid and alkali resistance, and could meet the requirements of spraying and protection of EPS floating ball surface in marine environment. [Conclusions] Polyurea elastomer coating can improve the aging resistance, wear resistance and acid and alkali resistance of EPS floating balls, and prevent them from being fragile and floating randomly to form marine floating garbage which results in "white pollution".

关键词： EPS floating ball Spray polyurea elastomer Gelation rate Wear resistant adhesion Chemical resistance

Insight into Atomic-Scale adhesion at the C-Cu Interface During theInitial Stage of Nanoindentation

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Nanomanufacturing and Metrology 2022年第3期5卷 250-258页

作者： Jian Gao Xichun Luo Wenlong Chang Zhengjian Wang Yongda Yan Yanquan Geng Centrefor Precision Manufacturing DMEMUniversity of StrathclydeGlasgowUK Center for Precision Engineering Harbin Institute of TechnologyHarbinPeople's Republic of China

adhesion is a common phenomenon in nanomachining which affects processing accuracy and repeatability.As material removal approaches the atomic or close-to-atomic scale,quantum mechanics becomes the dominant principle behind the atomic-level interaction.However,atomic-scale effects cannot be properly described by empirical potential function-based molecular dynamics simulations.This study uses a first-principles method to reveal the atomic-scale adhesion between a diamond tip and a copper slab during initial-stage nanoindentation.Using a simplified tip and slab model,adhesion energy,electronic distribution,and density of states are analyzed based on quantum chemistry calculation.Results show that atomic adhesion is primarily due to the covalent bonding interaction between C and Cu atoms,which can induce structural changes to the diamond tip and copper slab.The effects of tip position and angles on adhesion are further studied through a series of simulations.The results show that adhesion between the tip and slab is sensitive to the lattice structure and a variant in angstroms is enough to cause different adhesion and structural changes.The actual determinants of adhesion can only be the atomic and electronic structures at the tip-slab interface.Bond rotation and breakage are observed during simulation and their effects on adhesion are further discussed.To conclude,the first-principles method is important for the analysis of an atomic-scale interaction system,even if only as an aid to describing adhesion at atomic and electronic scales.

关键词： Nanoindentation adhesion Diamond Copper First-principles Density functional theory

adhesion and immunomodulatory effects of Bifidobacterium lactis HN019 on intestinal epithelial cells INT-407

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World Journal of Gastroenterology 2010年第18期16卷 2283-2290页

作者： Liu, Chang Zhang, Zhuo-Yang Dong, Ke Guo, Xiao-Kui Shanghai Jiao Tong Univ Sch Med Inst Med Sci Dept Med Microbiol & Parasitol Shanghai 200025 Peoples R China

AIM:To elucidate the adherence and immunomodulatory properties of a probiotic strain Bifidobacterium lactis(B.lactis) HN019.METHODS:adhesion assays of B.lactis HN019 and Salmonella typhimurium(S.typhimurium) ATCC 14028 to INT-407 cells were carried out by detecting copies of species-specific genes with real-time polymerase chain reaction.Morphological study was further conducted by transmission electron microscopy.Interleukin-1β(IL-1β),interleukin-8,and tumor necrosis factor-α(TNF-α) gene expression were assessed while enzyme linked immunosorbent assay was used to detect IL-8 protein secretion.RESULTS:The attachment of S.typhimurium ATCC 14028 to INT407 intestinal epithelial cells was inhibited significantly by B.lactis HN019.B.lactis HN019 could be internalized into the INT-407 cells and attenuated IL-8 mRNA level at both baseline and S.typhimuriuminduced pro-inflammatory responses.IL-8 secretion was reduced while IL-1β and TNF-α mRNA expression level remained unchanged at baseline after treated with B.lactis HN019.CONCLUSION:B.lactis HN019 does not up-regulate the intestinal epithelium expressed pro-inflammatory cytokine,it showed the potential to protect enterocytes from an acute inflammatory response induced by enteropathogen.

关键词： Probiotics Intestinal epithelium Enteropathogen Immunomodulation adhesion