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Surfactant-assisted hydrothermal synthesis of MoS_(2) micro-pompon structure with enhanced photocatalytic performance under visible light

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Tungsten 2020年第2期2卷 203-213页

作者： Man‑Zhang Xu Qiang Li Yuan‑Yuan Lv Zhi‑Ming Yuan Yu‑Xi Guo Han‑Jun Jiang Jiu‑Wei Gao Jun Di Pin Song Li‑Xing Kang Lu Zheng Zhi‑Yong Zhang Wu Zhao Xue‑Wen Wang Zheng Liu Frontiers Science Center for Flexible Electronics Xi’an Institute of Flexible Electronics(IFE)and Xi’an Institute of Biomedical Materials&EngineeringNorthwestern Polytechnical UniversityXi’an 710072China School of Information Science and Technology Northwest UniversityXi’an 710127China School of Materials Science and Engineering Nanyang Technological UniversitySingapore 639798Singapore MIIT Key Laboratory of Flexible Electronics(KLoFE) Northwestern Polytechnical UniversityXi’an 710072China Centre for Micro‑/Nano‑Electronics(NOVITAS) School of Electrical and Electronic EngineeringNanyang Technological UniversitySingapore 639798Singapore CINTRA CNRS/NTU/THALES and UMI 3288Research Techno PlazaSingapore 637553Singapore

MoS_(2) nanomaterial with the micro-pompon structure was synthesized by a surfactant-assisted hydrothermal method.The morphologies and structures of as-prepared MoS_(2) micro-pompon were investigated by adding different types of surfactants such as cetyltrimethyl ammonium bromide(CTAB),sodium dodecylbenzene sulphonate(SDBS),and polyvinyl pyrrolidone(PVP).The results indicated that the morphology of MoS_(2) could be controlled and changed effectively by the cationic sur-factant of CTAB.A reasonable growth mechanism for hollow structured MoS_(2) micro-pompon by hydrothermal processes was proposed.Further,photocatalytic degradation properties of MoS_(2) micro-pompon under visible light were evaluated by degradation of common organic dyes,which include rhodamine B(RhB),congo red,methyl orange,and methylene blue.The results indicated that MoS_(2) micro-pompon owned the highly selective catalytic ability to RhB with degradation efficiency of 95%in 60 min and 68%in 30 min.With the additive of the surfactant,the MoS_(2)-CTAB sample exhibited an enhanced ability of photocatalytic activity where degradation efficiency was improved to 92%in 30 min.The method employed in this work could be expanded to fabricate other sulfides with the controllable morphology and structure to further regulate the photocatalytic performance.

关键词： Hydrothermal method MoS_(2)micro-pompon Surfactant-assistant visible light photocatalytic Rhodamine B

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Fabrication of NiCoP decorated TiO_(2)/polypyrrole nanocomposites for the effective photocatalytic degradation of tetracycline

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Chinese Chemical Letters 2022年第5期33卷 2741-2746页

作者： Yalu Wu Yinyin Xu Yan Zhang Jingbo Feng Yuanyuan Li Jiaying Lan Xiuwen Cheng Key Laboratory for Environmental Pollution Prediction and Control College of Earth and Environmental SciencesLanzhou UniversityLanzhou 730000China

Due to the massive discharge of antibiotics in water,it is an urgent matter to remove antibiotics from waste water.The photocatalysts with high stability and activity have attracted extensive attention from researchers.By an in-situ polymerization method,polypyrrole(PPy)was modified on the surface of TiO_(2)(named as TiO_(2)/PPy).By one-step reduction method,NiCoP was grafted on the surface of TiO_(2)/PPy(named as TiO_(2)/PPy/NiCoP)to synthesize the photocatalyst of TiO_(2)/PPy/NiCoP for degradation of tetra-cycline(TC)antibiotic.The characterization results revealed that NiCoP was deposited on the surface of TiO_(2)/PPy successfully.The photocatalytic experiment results illustrated that 83.2%of TC could be de-graded at natural pH with 20 mg of TiO_(2)/PPy/NiCoP in 50 mL of TC solution(10 mg/L)under visible light irradiation.The high catalytic activity is attributed to the attachment of NiCoP on the surface of TiO_(2)/PPy which can enlarge the light response range of TiO_(2)effectively.Scavenger studies revealed that the degra-dation of TC was dominated by•O_(2)−and h+.The photodegradation efficiency of TC with TiO_(2)/PPy/NiCoP still reached over 74%after 5 consecutive cycles,indicating the potential applications in practical wastew-ater.

关键词： TiO_(2) NiCoP Polypyrrole visible light photocatalytic Tetracycline

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