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Fabrication of well-dispersive yttrium-stabilized cubic zirconia nanoparticles via vapor phase hydrolysis

Progress in Natural Science:Materials International 2012年第1期22卷 15-20页

作者： Fuzhi Shi a,Yaogang Li b,Hongzhi Wang a,Qinghong Zhang b a State Key Laboratory for Modification of Chemical Fibers and Polymer Materials,Donghua University,Shanghai 201620,China b Engineering Research Centre of Advanced Glasses Manufacturing Technology,Donghua University,Shanghai 201620,China State Key Laboratory for Modification of Chemical Fibers and Polymer Materials Donghua University Shanghai 201620 China Engineering Research Centre of Advanced Glasses Manufacturing Technology Donghua University Shanghai 201620 China

The well-dispersive yttrium-stabilized cubic zirconia nanoparticles were fabricated via vapor phase hydrolysis process,and the as-synthesized cubic zirconia nanoparticles were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM),highresolution electron microscopy(HRTEM) and N 2 adsorption-desorption isotherm *** results of XRD indicated that the pure cubic zirconia nanocrystals were obtained with 8 mol% yttrium atoms *** SEM and TEM observation showed the yttrium-stabilized cubic zirconia nanoparticles(8 mol% yttrium) were dispersive well,with an average crystallite size of 5 *** zirconia coatings were fabricated via the layer by layer(LbL) assembly using poly(allylamine hydrochloride) as polyelectrolyte and cubic zirconia nanoparticles as building blocks in order to illustrate its good *** quartz substrate coated on both sides with 10 layers of yttrium-stabilized cubic zirconia nanoparticles exhibited transmittance as high as 92.3%,which was decreased only one percent compared with bare quartz ***,the stable super-hydrophilic wetting property of the coating was obtained after a critical number of layers(10 layers) deposited onto the surface of quartz substrate,due to its porous structures.

关键词： Cubic zirconia Yttrium-stabilized vapor phase hydrolysis Layer by layer

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