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New role of α phase in the fracture behavior and fracture toughness of a β-type bio-titanium alloy

International Journal of Minerals,Metallurgy and Materials 2023年第9期30卷 1756-1763页

作者： Ran Wang Xiu Song Lei Wang Yang Liu Mitsuo Niinomi Deliang Zhang Jun Cheng Key Laboratory for Anisotropy and Texture of Materials(Ministry of Education)School of Materials Science and Engineering Northeastern UniversityShenyang 110819China Institute for Materials Research Tohoku University2-1-1 KatahiraAoba-kuSendai 980-8577Japan Meijo University 1-501 ShiogamaguchiTempaku-kuNagoya 468-8502Japan Nagoya University Furo-choChikusa-kuNagoya 464-8601Japan Shaanxi Key Laboratory of Biomedical Metal Materials Northwest Institute for Nonferrous Metal ResearchXi’an 710016China

The role of α precipitates formed during aging in the fracture toughness and fracture behavior of β-type bio-titanium alloy ti–29nb–13ta–4.6zr(TNTZ) was studied. Results showed that the fracture toughness of the TNTZ alloy aged at 723 K decreases to the minimum of 72.07–73.19 kJ·m^(-2)when the aging time is extended to 4–8 h and then gradually increases and reaches 144.89 kJ·m^(-2)after 72 h. The decrease in fracture toughness within the aging time of 4–8 h is caused by the large stress concentration at the tip of acicular α precipitates with a high aspect ratio and the preferential crack propagation along the inhomogeneous acicular α precipitates distributed in “V-shape” and “nearly perpendicular shape”. When the aging time is extended to 8–72 h, the precrack tip is uniformly blunted, and the crack is effectively deflected by α precipitates with multi long axis directions, more high homogeneity, low aspect ratio, and large number density. Analysis of the effect of αprecipitates on the fracture behavior suggested that the number of long axis directions of α precipitates is the key controlling factor for the fracture behavior and fracture toughness of the TNTZ alloy aged for different times.

关键词： fracture toughness ti-29nb-13ta-4.6zr alloy agedαphase crack tip blunting

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