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Reduction effect of final-pass heavy reduction rolling on the texture development,tensile property and Stretch formability of ZWK100 alloy plates

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Journal of Materials Science & Technology 2022年第16期111卷 211-223页

作者： B.Q.Shi L.Y.Zhao X.L.Shang B.H.Nie D.C.Chen C.Q.Li Y.Q.Cheng School of Materials Science and Hydrogen Energy Foshan UniversityFoshan 528000China School of Materials and Energy Guangdong University of TechnologyGuangzhouGuangdong 510006China GD Midea Air-Conditioning Equipment Co. Ltd.Foshan 528311China Guangdong Key Laboratory of Hydrogen Energy Technology Foshan 528000China YunFu(Foshan)R&D Center of Hydrogen Energy Standardization Yunfu 527326China

Obviously planar anisotropy due to‘TD split’orthotropic texture(TD indicates Transverse direction)always exist in the Rare-earth(RE)or Ca containing Mg alloy sheets,which is likely caused by the lowreduction rolling(and annealing)as revealed in our previous research.In this work,the as-cast billets of a ZWK100 alloy were subjected to final-pass heavy reduction rolling(FHRR)at 500°C with different reductions(30%-70%)after rough rolling,aiming to investigate the reduction effect on the microstructure and texture formation.The results show that FHRR with higher reductions above 50%is in favor of shear banding formation but has little effect on the as-deformed texture components,and the excellent formability with single-pass reduction up to 70%is mainly ascribed to the activation of prismatic slip.FHRR with reduction above 50%and annealing can generate uniform grain structures of~10μm and symmetrical‘oblique-line split’texture in(0001)pole figures,with basal poles tilting by about 50°from ND(Normal direction)towards some oblique-line of TD and RD(Rolling direction)as well as uniform distribution of counter lines as an annular shape,resulting in excellent elongation to failure of~50%and ultra-low planar anisotropyΔr_of~0.1 and high Stretch formability(Erichsen value:8.1).The formation‘oblique-line split’texture in(0001)pole figures is mainly correlated with the preferred growth tendency of grains with■//RD,which was suggested to relate to the high mobility of some special boundaries such as 40°-45°■.The influences of starting textures on the mechanical properties,planar anisotropy and related deformation modes,as well as their correlations with the Stretch formability were comparatively investigated with the‘TD split’orthotropic texture as a counterpoint.

关键词： Magnesium alloys Texture Plane anisotropy Stretch formability Rolled sheets

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Effect of bending and tension deformation on the texture evolution and Stretch formability of Mg-Zn-RE-Zr alloy

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International Journal of Minerals,Metallurgy and Materials 2022年第7期29卷 1334-1342页

作者： Yuya Ishiguro Xinsheng Huang Yuhki Tsukada Toshiyuki Koyama Yasumasa Chino Department of Materials Design Innovation Engineering Nagoya UniversityFuro-choChikusa-kuNagoya464-8603Japan Multi-Material Research Institute National Institute of Advanced Industrial Science and Technology2266-98AnagahoraSimo-shidami Moriyama-kuNagoya463-8560Japan

Bending and tension deformations were performed on Mg-1.3 wt%Zn-0.2 wt%RE-0.3 wt%Zr(ZEK100)alloy sheets that initially had a transverse direction(TD)-split texture.The effects of bending and tension deformations on the texture formation and room-temperature formability of specimens were investigated.The specimen subjected to 3-pass bending and tension deformations exhibited an excellent Erichsen value of 9.6 mm.However,the Erichsen value deterioration was observed in the specimen subjected to 7-pass deformations.The rolling direction-split texture developed on the surface with an increasing pass number of deformations.Conversely,the clear TD-split texture remained at the central part.As a result,a quadrupole texture was macroscopically developed with an increasing pass number of deformations.The reduction in anisotropy by the formation of the quadrupole texture is suggested to be the main reason for the improvement in Stretch formability.By contrast,the generation of coarse grains near the surface is suggested to be the direct cause for the deterioration of the Stretch formability of the specimen subjected to 7-pass deformations.

关键词： magnesium alloy texture Stretch formability bending and tension deformation mechanical properties

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Texture and Stretch formability of rolled Mg–Zn–RE(Y, Ce, and Gd) alloys at room temperature

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Rare Metals 2013年第5期32卷 441-447页

作者： Zheng-Xu Cai Hai-Tao Jiang Di Tang Zhao Ma Qiang Kang National Engineering Research Center of Advanced Rolling University of Science and Technology Beijing

To develop a new magnesium alloy with excellent formability at room temperature, the effect of Y, Ce, and Gd addition on texture and Stretch formability of Mg-1.5Zn alloys was carried out. The result shows that Y, Ce, and Gd addition in Mg-1.5Zn alloys can effectively weaken and modify the basal plane texture, characterized by TD-split texture in which the position of basal is titled from normal direction （ND） toward transverse direction （TD）. When Mg-1.5Zn alloy with Gd addition appears low texture intensity and TD-split texture, where the position of basal poles is tilted by about 4-35° from ND toward to TD, the largest Erichsen value of 7.0 and the elongation rate reaches 29.1% in TD direction. However, Y and Ce addition in Mg-1.5Zn alloys promote a large number of second phase particles, which cancel the contribution of the unique basal texture to Stretch formability and ductility.

关键词： Magnesium Texture Size effects Stretch formability Mechanical property Rare earth elements

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Microstructure,mechanical properties and Stretch formability of as-rolled Mg alloys with Zn and Er additions

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Rare Metals 2021年第8期40卷 2179-2187页

作者： Ke Liu Jing-Tao Liang Wen-Bo Du Shu-Bo Li Zhao-Hui Wang Zi-Jian Yu Jin-Xue Liu College of Materials Science and Engineering Beijing University of TechnologyBeijing100124China Zhengzhou Light Metal Research Institute Zhengzhou450041China

The magnesium alloy has a unique advantage in 3C fields due to its high specific strength and excellent electromagnetic shielding characteristic.However,it is difficult to deform homogeneously because of hexagonal close-packed structure.In the present work,the microstructure,mechanical properties and Stretch formability of magnesium alloy sheets with different alloying elements were investigated.It was indicated that a trace addition of Zn or/and Er made a key role in modifying texture,activating shear bands formation and precipitating nanoscale second phases,respectively,which resulted in an obvious improvement in both Stretch formability and mechanical properties.The results suggested that the Mg-0.5 Zn-0.5 Er alloy sheet exhibited higher tensile strength along the rolling direction,i.e.,yield strength of 180 MPa and ultimate tensile strength of 201 MPa,accompanying with superior Erichsen value of 7.0 mm at room temperature.The good performances of the sheet were ascribed to weakening basal texture intensity,formation of shear bands and precipitation of nanoscale W-phase(Mg_(3)Zn_(3)Er_(2)).

关键词： Mg-Zn-Er alloy Hot rolling Texture Shear band Stretch formability

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The effects of orientation control via tension-compression on microstructural evolution and mechanical behavior of AZ31 Mg alloy sheet

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Journal of Magnesium and Alloys 2022年第2期10卷 446-458页

作者： Qingshan Yang Bin Jiang Bo Song Zujian Yu Dewei He Yanfu Chai Jianyue Zhang Fusheng Pan School of Metallurgy and Material Engineering Chongqing University of Science and TechnologyChongqing 401331China National Engineering Research Center for Magnesium Alloys Chongqing UniversityChongqing 400044China School of Materials and Energy Southwest UniversityChongqing400715China MagIC–Magnesium Innovation Centre Helmholtz-Zentrum GeesthachtMax-Planck-Straße 1Geesthacht 21502Germany School of Engineering Technology Purdue UniversityWest LafayetteIN 47907-2021United States

The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were performed by pre-strain paths,i.e.,tension(6%)and compression(5%)perpendicular to the c-axis along extrusion direction(ED),to investigate the microstructural evolution and mechanical properties of AZ31 Mg alloy sheets.The distinction in the texture evolution and strain hardening behavior was illustrated in connection with the pre-strain paths for the activities of twinning and slip.The result shows that the activation of the deformation mode was closely bound up with the grain orientation and the additional applied load direction.The{10–12}twin-texture components with c-axis//ED were generated by precompression,which can provide an appropriate alternative to accommodate the thin sheet thickness strain and enhance the room temperature formability of Mg alloy sheet.

关键词： Mg alloy Orientation control Microstructural evolution Texture Stretch formability

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Influence of Continuous Bending Process on Texture Evolution and Mechanical Properties of AZ31 Magnesium Alloy

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Acta Metallurgica Sinica(English Letters) 2018年第3期31卷 225-233页

作者： Ting-Zhuang Han Guang-Sheng Huang Lun Huang Bin Jiang Guan-Gang Wang Ai-Tao Tang Fu-Sheng Pan State Key Laboratory of Mechanical Transmission College of Materials Science and Engineering Chongqing University National Engineering Research Center for Magnesium Alloys Chongqing University Chongqing Research Center for Advanced Materials Chongqing Academy of Science & Technology

Mg-3Al-lZn alloy sheets have been deformed by continuous bending（CB）to investigate the effects of pro-cessing parameters（bending angle and repetitive passes）on the texture and formability.The samples exhibited a bimodal microstructure with abnormal growth grains in the surface region and fine grains distributed in the center after CB process followed by annealing.The texture evolution measured by XRD indicated that the basal poles were rotated from ND toward RD,and the texture intensity decreased with the bending angle decreasing and repetitive passes increasing.Compared with the as-received sample,the yield strength of CBA-120-2 sample significantly decreased from 183 to 112 MPa,and a smaller r-value and a larger n-value were obtained.The formability of CB processed samples in annealing condition was significantly enhanced with the highest of Erichsen value of 5.4 mm,increased by about 135%.The improvement of formability was likely attributed to the weakened and RD-tilt basal texture and coarse grains in the surface part.

关键词： Magnesium alloy Continuous bending Microstructure Texture Stretch formability

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