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Improving the radiopacity of Fe-Mn biodegradable metals by magnetron-sputtered W-Fe-Mn-C coatings:Application for thinner stents

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Bioactive Materials 2022年第6期7卷 64-70页

作者： Samira Ravanbakhsh Carlo Paternoster Gianni Barucca Paolo Mengucci Sofia Gambaro Theophraste Lescot Pascale Chevallier a Marc-Andre Fortin Diego Mantovani Laboratory for Biomaterials and Bioengineering Canada Research Chair I in Biomaterials and Bioengineering for the Innovation in SurgeryDepartment of Min-Met-Materials EngineeringResearch Center of CHU de QuebecDivision of Regenerative MedicineLaval UniversityQuebec CityQuebec G1V 0A6Canada Laboratory for Biomaterials in Imaging(BIM) Axe Medecine RegeneratriceCentre Hospitalier Universitaire(CHU)de Quebec-Universite Laval2705boul.Laurier(T1-61a)QuebecG1V 4G2Canada Department of Materials Environmental Sciences and Urban PlanningUniversita Politecnica delle Marchevia Brecce Bianche 1260131AnconaItaly National Research Council Institute of Condensed Matter Chemistry and EnergyCNR-ICMATEVia de Marini 616149GenovaItaly Departement de Genie des Mines de la Metallurgie et des MateriauxCentre de Recherche sur les Materiaux Avances(CERMA)Universite LavalQuebecG1V 0A6Canada Axe Medecine Regeneratrice Centre Hospitalier Universitaire(CHU)de Quebec-Universite Laval2705boul.Laurier(T1-61a)QuebecG1V 4G2Canada

In this exploratory work,micrometric radiopaque W-Fe-Mn-C coatings were produced by magnetron sputtering plasma deposition,for the first time,with the aim to make very thin Fe-Mn stents trackable by *** power of Fe-13Mn-1.2C target was kept constant at 400 W while that of W target varied from 100 to 400 W producing three different coatings referred to as P100,P200,*** effect of the increased W power on coatings thickness,roughness,structure,corrosion behavior and radiopacity was *** coatings showed a power-dependent thickness and W concentration,different roughness values while a similar and uniform columnar *** amorphous phase was detected for both P100 and P200 coatings while γ-Fe,bcc-W and W_(3)C phases found for ***,P200 and P400 showed a significantly higher corrosion rate(CR)compared to *** presence of W,W_(3)C as well as the Fe amount variation determined two different micro-galvanic corrosion mechanisms significantly changing the CR of coatings,0.26±0.02,59.68±1.21 and 59.06±1.16μm/year for P100,P200 and P400,*** P200 with its most uniform morphology,lowest roughness(RMS=3.9±0.4 nm)and good radiopacity(~6%)appeared the most suitable radiopaque biodegradable coating investigated in this study.

关键词： Fe-Mn-Based alloys Degradable coatings W-Fe-Mn-C coatings Magnetron sputtering Radiopacity stent fluoroscopy

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