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rejuvenation heat treatment of the Second-Generation Single-Crystal Superalloy DD6

Acta Metallurgica Sinica(English Letters) 2015年第10期28卷 1278-1285页

作者： Zhen-Xue Shi Shi-Zhong Liu Jia-Rong Li Science and Technology on Advanced High Temperature Structural Materials Laboratory Beijing Institute of Aeronautical Materials

The second-generation single-crystal superalloy DD6 with [001] orientation was prepared by screw selecting method in the directionally solidified furnace. The long-term aging of the alloy after full heat treatment was performed at1100 °C for 400 h. Then the rejuvenation heat treatment 1300 °C/4 h/AC ？ 1120 °C/4 h/AC ？ 870 °C/24 h/AC was carried out. The stress rupture properties were investigated at 760 °C/800 MPa, 850 °C/550 MPa, 980 °C/250 MPa and1100 °C/140 MPa after different heat treatments. The microstructures of the alloy at different conditions were studied by SEM. The results show that c0 phase of the alloy became very irregular and larger after long-term aging at 1100 °C for 400 h. A very small amount of needle-shaped TCP phase precipitated in the dendrite core. The coarsened c0 phase and TCP phase dissolved entirely after rejuvenation heat treatment. The microstructure was restored and almost same with the original microstructure. The stress rupture life of the alloy decreased in different degrees at various test conditions after long-term aging. The stress rupture life of the alloy after rejuvenation heat treatment all restores to the original specimen more than 80%at different conditions. The microstructure degradation of the alloy during long-term aging includes coarsening of the c0 phase,P-type raft and precipitation of TCP phase, which results in the degeneration of stress rupture property. The rejuvenation heat treatment succeeds in restoring the original microstructure and stress rupture properties of the alloy.

关键词： Single-crystal superalioy DD6 rejuvenation heat treatment Stress rupture properties

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Effects of rejuvenation heat treatment on microstructure and creep property of a Ni-based single crystal superalloy

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Journal of Materials Science & Technology 2021年第1期60卷 206-215页

作者： K.J.Tan X.G.Wang J.J.Liang J.Meng Y.Z.Zhou X.F.Sun Superalloys Division Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Department of Materials Science and Engineering University of Science and Technology of ChinaHefei 230026China

Both surface and internal microstructures of a second-generation Ni-based single crystal(SX) superalloy were studied after creep and rejuvenation heat treatment(RHT).It is indicated that the microstructures,such as the dislocation network,the γ phase and the γ' phase,can be recovered to those after the standard heat treatment(SHT).It is found that RHT affected zone(RAZ) formed at the surface is composed of theγ'-free layer,the transition layer and the recrystallization(RX),which are less than 20 μm in depth *** depth of the RAZ doesn't affect the properties of the *** morphology of γ' phase at the RAZ is related to the composition of the *** average creep life after RHT is close to the average life after *** is concluded that RHT could effectively repair SX parts and increase the total life of the sample after a damage by creep.

关键词： Superalloys rejuvenation heat treatment Microstructure Creep property

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Effect of microstructures restoration on high temperature fatigue behavior of DZ125 superalloy

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Progress in Natural Science:Materials International 2021年第4期31卷 633-640页

作者： Shifu Wang Allah Ditta Yi Xu Zheng Zhang School of Materials Science and Engineering Beihang University

Combination of hot isostatic pressing(HIP) and rejuvenation heat treatment(RHT) technology was used to restore creep-damaged DZ125 directional solidified superalloy, and the influence of microstructure restoration on high temperature fatigue behavior of the samples was explored. The results show that the HIP+RHT process could effectively heal internal cavities and recover the degraded γ' phase in creep-damaged DZ125 superalloy to cubic particles similar as in as-received sample. After restoration treatment, the stress concentration areas inside the sample eradicated with the healing of the internal cavities, and the fatigue source areas were limited only to near surface than initiating from inside as in the as-received and creep-damaged samples. As a result, the restored sample had higher crack initiation life and lower crack propagation rate compared to as-received and creep damaged samples. The TEM microstructure characterization near fatigue fracture showed that the restoration of the degraded γ0 phase eliminated tangled dislocation in creep damaged sample and produced evenly distributed dislocations in the γ channel with short curved line-like morphology, like the as-received sample, which effectively hindered the dislocations movement during subsequent deformation, and strengthen the fatigue resistant of alloy. Therefore, it can be concluded that the HIP-RHT process, through the combined effect of internal cavities healing and the restoration of the degraded microstructures, renders higher high temperature fatigue life than creep-damaged and even higher than as-received DZ125 superalloy.

关键词： Hot isostatic pressing rejuvenation heat treatment High temperature fatigue behavior Healing of internal cavities Restoring of degraded microstructures

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