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Single crystal growth and characterization of 166-type magnetic kagome metals

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Chinese Physics B 2024年第9期33卷 145-150页

作者： Huangyu Wu Jinjin Liu Yongkai Li Peng Zhu Liu Yang Fuhong Chen Deng Hu Zhiwei Wang Centre for Quantum Physics Key Laboratory of Advanced Optoelectronic Quantum Architecture and Measurement(MOE)School of PhysicsBeijing Institute of TechnologyBeijing 100081China Beijing Key Laboratory of Nanophotonics and Ultrafine Optoelectronic Systems Beijing Institute of TechnologyBeijing 100081China Beijing Institute of Technology Zhuhai 519000China Material Science Center Yangtze Delta Region Academy of Beijing Institute of TechnologyJiaxing 314011China

Kagome magnets were predicted to be a good platform to investigate correlated topology band structure,Chern quantum phase,and geometrical frustration due to their unique lattice *** we reported single crystal growth of 166-type kagome magnetic materials,including HfMn_(6)Sn_(6),ZrMn_(6)Sn_(6),GdMn_(6)Sn_(6)and GdV_(6)Sn_(6),by using the flux method with Sn as the *** them,HfMn_(6)Sn_(6)and ZrMn_(6)Sn_(6)single crystals were grown for the first time.X-ray diffraction measurements reveal that all four samples crystallize in HfFe6Ge6-type hexagonal structure with space group P6/*** samples show metallic behavior from temperature dependence of resistivity measurements,and the dominant carrier is hole,except for GdV6Sn6 which is electron *** samples have magnetic order with different transition temperatures,HfMn_(6)Sn_(6),ZrMn_(6)Sn_(6)and GdV_(6)Sn_(6)are antiferromagnetic with TN of 541 K,466 K and 4 K respectively,while GdMn_(6)Sn_(6)is ferrimagnetic with the critical temperature of about 470 *** study will enrich the research platform of magnetic kagome materials and help explore the novel quantum phenomena in these interesting *** dataset of specific crystal structure parameters for HfMn_(6)Sn_(6)are available in Science Data Bank,with the link.

关键词： kagome metal single crystal growth crystal structure physical property

Preparation and Metallurgical Analysis of High Activity Burnt Lime for Steelmaking

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Journal of Iron and Steel Research International 2016年第9期23卷 884-890页

作者： Hua-qiang HAO Yu-zhu ZHANG Su-ju HAO Chao-fa ZHANG Wu-feng JIANG Peng-hui CUI College of Metallurgy Northeastern University Department of Long Product Tangshan Iron and Steel CompanyHebei Iron and Steel Group College of Metallurgy & Energy Key Laboratory of the Ministry of Education for Modern Metallurgy TechnologyNorth China University of Science and Technology

Burnt lime is an important material in steelmaking and its activity degree is a key factor for liquid steel quality. The burnt lime was made by the calcination of limestone in a high pressure electric furnace. The burnt lime mineralogical phases and micro-morphologies were characterized by X-ray diffraction （XRD） and field emission scan- ning electron microscopy （FE-SEM）. The burnt lime activity degree was determined by acid-base titration, the burnt lime pore distribution was measured by mercury intrusion porosimetry （MIP）, and the thermal effect of a mixture of burnt lime and slag was measured by differential scanning calorimetry （DSC）. The results showed that the CaO grain size and pore size of burnt lime made under high pressure were larger than those of burnt lime made under atmos- pheric pressure. The CaO grain size and pore size increased and the laminate phenomenon also occurred clearly under high pressure. The activity degree of burnt lime made under high pressure was greater than that made under atmos- pheric pressure. The maximum activity degree was 437 mL for burnt lime made under a pressure of 0.4 MPa. For the same ratio of CaO to SiOz, the melting temperature, hemisphere temperature and fluidity temperature of slag decreased with increasing burnt lime activity degree. The higher the activity degree the burnt lime had, the better the slag forming occurred. It was advantageous for -2CaO · SiO2 and 3CaO · SiO2 forming at lower temperatures if the burnt lime activity degree was increased.

关键词： burnt lime high pressure calcination activity degree physical property slag performance

Effects of Different Calcining Temperatures on the Properties of Ceramsite Prepared by High-carbon Gasification Slag

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Journal of Wuhan University of Technology(Materials Science) 2023年第2期38卷 292-298页

作者： WU Feng LI Hui LI Taizhi MA Xudong College of Materials Science and Engineering Xi’an University of Architecture and TechnologyXi’an710055China State Key Laboratory of Green Building in Western China Xi’an University of Architecture and TechnologyXi’an710055China Shaanxi Ecological Cement&Concrete Engineering Technology Research Center Xi’an710055China

The structure and characteristics of high-performance lightweight aggregates produced by high-carbon gasification slag were investigated by X-ray diffraction,scanning electron microscopy,thermogravimetry/differential thermogravimetr,differential scanning calorimetry-Fourier transform infrared,and mercury intrusion porosimetry,*** experimental results show that the ceramsite undergoes two weightless stages in the calcining *** the increase in the calcining temperature,a large number of pores are formed inside the ceramsite,its structure becomes denser,but the calcining temperature band of the ceramsite becomes *** crystalline phase of the ceramsite changes at different calcining temperatures and the mineral phase changes from the earlieralbite,quartz,oligoclase,hematite,etc,to a silica-aluminum-rich glass *** 1130℃ is a more suitable calcining temperature,and the cylinder compressive strength of ceramics is 11.59 MPa,the packing density,apparent density,porosity,and water absorption are 939.11 kg/m^(3),1643.75 kg/m^(3),28.11%,and 10.35%,respectively,which can meet the standards for high-strength lightweight aggregates.

关键词： high-carbon gasification slag ceramsite concrete physical property

Theoretical calculation of high-pressure CO_(2)jet in cases of composite rock-breaking based on span-wagner equation of state

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Journal of Hydrodynamics 2022年第5期34卷 948-964页

作者： Xian-peng Yang Can Cai Xiao-hua Chen Pei Zhang Xin Zeng Chi Peng Yingfang Zhou Oil and Gas Equipment Technology Sharing and Service Platform of Sichuan Province School of Mechanical EngineeringSouthwest Petroleum UniversityChengdu610500China School of Engineering University of AberdeenAberdeenUK Laboratory of High-pressure Jet Theory and Application Technology Southwest Petroleum UniversityChengdu610599China Key Laboratory of Groundwater Resources and Environment Ministry of EducationJilin UniversityChangchun130021China Southwest Pipeline Co. Ltd.National Pipe Network GroupChengdu610064China

Although several theoretical calculation methods for high-pressure jet are available,there is currently no theoretical model for the high-pressure CO_(2)jet based on the high-precision equation of state(EOS).To investigate the flow field of the high-pressure CO_(2)jet in cases of the composite rock-breaking under the high-pressure CO_(2)Jet and PDC cutter,a semi-analytical approach of the high-pressure CO_(2)jet is developed based on the Span-Wagner EOS and CO_(2)jet *** semi-analytical calculations and the physical property calculations under the action of the high-pressure CO_(2)jet are conducted with consideration of the jet pressure,the jet distance,the nozzle diameter and the jet *** results indicate that the distribution of the physical properties calculated by the semi-analytical approaches is similar to that obtained by experimental monitoring and numerical simulation,which indicates that the calculation method of the high-pressure CO_(2)jet presented in this paper is effective and *** properties of the CO_(2)jet obtained by the theoretical calculation see a significant difference between the initial region and the jet impact *** the temperature of 300 K,the increase of the initial pressure can effectively increase the impact force and the cooling ability of the *** proportion of the jet core lengths in the jet on the axis increases with the increase of the ratio of the nozzle diameter to the jet length,accompanied with the increase of the impact force of the *** increase of the jet angle can effectively increase the impacting force of the jet,but hampers the fluid *** study combines the theoretical calculation of the jet with the calculation of the physical properties of the high-pressure CO_(2),for comprehensively understanding the CO_(2)jet field in the composite rock-breaking under the action of the high-pressure CO_(2)jet and PDC *** theoretical calculation of the CO_(2)jet based on the high-precisio

关键词： CO_(2)jet hydraulic jet drill theoretical calculation equation of state(EOS) physical property

Effects of the band-filling and Fe/Mo disorder on physical properties of Ca_2FeMoO_6

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Chinese Physics B 2018年第12期27卷 444-449页

作者： Jin-Feng Wang Zhao-Tong Zhuang Shuai-Shuai Liu Qian-Qian Gao College of Physics and Materials Science National Demonstration Center for Experimental Physics EducationHenan Normal University and Henan Key Laboratory of Photovoltaic Materials

Both the band filling effect and Fe/Mo disorder have a close correlation with the physical properties of the double perovskite Ca2FeMoO6. Two series of Ca2FeMoO6and Nd0.3Ca1.7FeMoO6ceramics sintered at(1050℃, 1200℃, and 1300℃) were specially designed to comparatively investigate the band-filling effect and Fe/Mo disorder on the physical properties of Ca2FeMoO6. The x-ray diffraction indicates that Fe/Mo disorder is sensitive to the sintering temperature. The magnetization behavior is mainly controlled by the Fe/Mo disorder not by the band filling effect, manifested by a close correlation of saturated magnetization(Ms) with the Fe/Mo disorder. Interestingly, magnetoresistance(MR) property of the same composition is dominantly contributed by the grain boundary strength, which can be expressed by the macroscopic resistivity values. However, the band filling effect caused by the Nd-substitution can decrease the spin polarization, and thus suppress the MR performance fundamentally. Contrary to the MR response, the Curie temperature(TC) shows an obvious optimization due to the band filling effect, which increases the carrier density near the Fermi level responsible for the ferromagnetic coupling interaction strengthen. Maybe, our work can provoke further research interests into the correlation of the band-filling effects and Fe/Mo disorder with the physical properties of other Fe/Mo-based double perovskites.

关键词： band filling effect Fe/Mo disorder Ca_2FeMoO_6 physical property

physical and Electrochemical Properties of Acid 1-Methyl-3-Ethylimidazolium Chloride/AlCl_3/LiAlCl_4 Molten Salt

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International Journal of Minerals,Metallurgy and Materials 2000年第4期14卷 286-291页

作者： Ying Sing Fung, Ruqi Zhou ( Department of Chemistry, The University of Hong Kong, Hong Kong, China Department of Inorganic and Non-metal Materials, University of Science and Technology Beijing, Beijing 100083, China) Department of Chemistry University of Hong Kong Hong Kong Hong Kong Department of Inorganic and Non-metal Materials University of Science and Technology Beijing Beijing 100083 China

An acid molten salt was formed by means of mixing 1 -methyl- 3 -ethylimidazolium chloride with AlCl3 and LiAlCl4 at ambient temperature. The solubility of LiAlCl4 in the acid molten salt was measured. Variations of specific conductivity, density and kinetic viscosity of molten salt with mole ratio o f MeEtlmCl/A1lCl3/LiAlCl4 were observed. A solubility maximum of LiAlCl4 with 5 4% in molar fraction was shown at a mole ratio of AlCl43/MeEtlmCl = 1 .2. An increase in density and viscosity, and a decrease in specific conductivity were found with increasing the concentrations of LiAlCl4 and AlCl3. The dependence of specific conductivity of this acid molten salt upon temperature was found to display Vogel-Tammanm-Fucher behavior. However, Arrhenius behavior was observed at two special mole ratios of MeEtImCl/AlCl3/LiAlCl4 = 1:1.5:0.05 and 1. 1.5:0. 10. The conductivity equations of this molten salt at various compositions were constructed. The ion interaction in the acid molten salt was studied using 7Li and 27Al nuclear magnetic resonance spectroscopic methods. The effect of concentrations of LiAlCl4 and AlCl3 on the ion interaction was also discussed.

关键词： Li-7 NMR Al-27 NMR room temperature molten salt aluminum chloride lithium tetrachloroaluminate physical property electrochemical property Materials

Structure and properties of nanocrystalline rare earth bulks prepared by spark plasma sintering

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Journal of Rare Earths 2009年第6期27卷 961-966页

作者：卢年端宋晓艳刘雪梅张久兴 College of Materials Science and Engineering Key Lab of Advanced Functional MaterialsChinese Ministry of EducationBeijing University of Technology

A series of rare earth bulks with the ultrafine nanocrystalline structure were prepared by applying an 'oxygen-free'(an environmental oxygen concentration less than 0.5 ppm) in-situ synthesis system,where the inert-gas condensation was combined with the spark plasma sintering technology into an entirely closed *** thermal and mechanical properties of the prepared ultrafine nanocrystalline bulks were characterized and compared with those of the raw polycrystalline *** was found that the specific ...

关键词： spark plasma sintering ultrafine nanocrystalline bulk physical property rare earths

Effect of nano-graphite on mechanical properties and oxidation resistance of ZrB_(2)-SiC-graphite electrode ceramics

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Journal of Iron and Steel Research International 2024年第6期31卷 1502-1513页

作者： Bo-lin Yang Chang-liu Kuang Zheng-long Liu Chao Yu Cheng-ji Deng Jun Ding The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina

ZrB_(2)-based ceramic composites were prepared by spark plasma sintering using ZrB_(2) powder prepared by molten salt method as raw material and SiC and nano-graphite as *** effects of nano-graphite addition on the physical properties and oxidation resistance of ZrB_(2)-based ceramic samples were *** results show that the addition of an appropriate amount of nano-graphite can effectively improve the density of ZrB_(2)-based ceramic composites and improve the physical properties of the *** flexural strength of the ceramic sample with 8 vol.%nano-graphite reached 418.54 MPa,which was 53.14% higher than that of ZrB_(2)-SiC ceramic material(273.31 MPa),and its oxidation resistance was also significantly *** demonstrats that the addition of an appropriate amount of nano-graphite can effectively improve the physical properties and oxidation resistance of ZrB_(2)-SiC ceramic *** prolonging its service life in application and promoting the development of ZrB_(2)-based ceramic composites,it is of great significance for clean steel smelting.

关键词： ZrB_(2)-SiC-graphite electrode ceramic ZrB_(2)-based ceramic composite Nano-graphite physical property Oxidation resistance

ADVANCED QUALITY CONCEPTS AND COMPOSITE RELIABILITY THROUGH STATISTICALPROCESS CONTROL

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Acta Metallurgica Sinica(English Letters) 1997年第3期10卷 263-269页

作者： D. Evans (CCLRC, Rutherford Appleton Laboratory, Chilton, Oxon. OX14 2HQ U.K.) Rutherford Appleton Lab Oxon United Kingdom

The physical properties of thermosetting resins and resin based composites may be influenced by changes in any one of the mang formulating or process related variables involved in their manufacture. When resins and composite materials are required to perform in aggressive environments, reliable and predicable performance is essential and therefore these materials must be prepared and tested in accorkance with a strictquality plan. This paper outlines the elements of statistical process control (S.P.C.)as it may be applied to non-metallic materials and discusses the concept of Capability Index (Cp).

关键词： physical property composite process control cryogenic application