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Development and performance evaluation of a high temperature resistant, internal rigid, and external flexible plugging agent for water-based drilling fluids

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Petroleum 2023年第1期9卷 33-40页

作者： Zhe Xu Jinsheng Sun Li Li Kaihe Lv Jingping Liu Zhiwen Dai Xianfa Zhang Zonglun Wang School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580China CNPC Engineering Technology R&D Company Limited Changping10206China Oil&Gas Technology Research Institute of Changqing Oilfield Company Xi'an710000China

During the drilling process for oil and gas production,a larger number of drilling fluids invade the formation,causing severe formation damage and wellbore collapsing,which seriously hinders the efficient production of deep oil and gas.Although several plugging agents have been developed for efficient fracture sealing in recent years,the development of high-performance plugging agents with self-adaptive ability and high-temperature resistance remain a challenge.Herein,we report the synthesis of an internal rigid and external flexible plugging agent PANS by reversed-phase emulsion polymerization with nano-silica as the rigid core and poly(acrylamide-co-N-vinylpyrrolidone)as a flexible shell.The plugging agent has a median particle size of 10.5μm and can self-adapt to seal the microfractures and fractures in the formation,leading to an effective reduction in the filtration loss of bentonite water-based drilling fluid under both low temperature and low pressure(LTLP)and high temperature and high pressure(HTHP)conditions.In addition,compared with the neat nano-silica(500 nm),the sealing efficiency of PANS toward 100–120 mesh sand bed was increased by 71.4%after hot rolling at 180°C.

关键词： Internal rigidity External flexibility plugging agent Filter loss reduction plugging performance

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Synthesis and Evaluation of a Water-Swelling Polymer plugging agent SWL-1

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Open Journal of Yangtze Oil and Gas 2021年第2期6卷 50-59页

作者： Li He Qichao Cao Xintong Li Song Wang School of Chemistry and Environmental Engineering Yangtze University Jingzhou China

In this paper, to solve the problems of low water absorption and weak pressure bearing capacity of current plugging materials, acrylic acid (AA), acrylamide (AM), and sodium allyl sulfonate (SAS) are used as monomers, and soluble starch is used as grafting. Material, the use of free radical aqueous solution method to synthesize the plugging agent SWL-1 with good water absorption and strong salt resistance. The monomer ratio is set as n (AA):n (AM):n (SAS) = 5:2:1, the experimental synthesis temperature is 70°C, and the orthogonal experiment is used to determine the experimental synthesis conditions as AA neutralization degree 80%, The amount of initiator is 0.60%, the amount of crosslinking agent is 0.50%, the ratio of monomer to starch is 7:1, and the amount of calcium carbonate is 13%. The comprehensive evaluation of the performance of the plugging agent SWL-1 shows that the water absorption performance at 60°C is the best 268.78 g/g, and the water absorption performance in 8% NaCl, 0.9% CaCl2 and composite brine is 21.5 g/g, 12.5 g/g and 24.9 g/g, indicating good resistance to sodium and calcium, the water retention rate is still higher than 30% after 15 days at 160°C. The sand bed plugging test found that the maximum pressure of SWL-1 was 7 MPa, and the crack plugging test found that when the crack width was 1 mm, 2 mm, and 3 mm, the maximum compressive strength of SWL-1 was 10 MPa. The acid solubility test showed that the maximum pressure was 10 MPa. The highest rate is 86.38%.

关键词： plugging agent Water Absorption Sand Bed plugging Crack plugging Acid Solubility

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