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Kinetic study of complicated anti-solvent and cooling crystallization of disodium 5′-ribonucleotide

Particuology 2023年第2期73卷 103-112页

作者： Wang Zhao Binghui Li Shiyuan Liu Yuehua Deng Rui Zhang Yanbin Jiang Guangdong Provincial Key Lab of Green Chemical Product Technology School of Chemistry and Chemical EngineeringSouth China University of TechnologyGuangzhou510640China Zhuhai Institute of Modern Industrial Innovation South China University of TechnologyZhuhai519175China School of Chemical Engineering Guangdong University of Petrochemical TechnologyMaoming525000China

Disodium 5′-ribonucleotide,which is composed of disodium 5′-inosine(IMP)and disodium 5′-guanosine(GMP),is an important food *** lack of kinetic studies of it causes a lack of clarity in understanding the complicated multi-solute crystallization of IMP+GMP in *** this work,process analytical technology tools were used to obtain the thermodynamics and kinetic data from the experiments,the kinetic parameters of anti-solvent and cooling crystallization were *** crystal form of IMP+GMP mixed crystal was determined,which was consistent with the IMP whether crystallized from pure water or *** effects of different anti-solvent addition rates and cooling rates on the metastable zone widths were studied,and the opposite effect on metastable zone width was *** modified exponential empirical function was developed to correlate nucleation and growth kinetic equations under different *** kinetic data were well fitted with adjusted correlation coefficient(adj-R^(2)>0.7),which is sufficient to provide a valid reference for process design and control.

关键词： Disodium 5′-ribonucleotide Multi-solute crystallization Nucleation and growth kinetics Process analytical technology tools metastable zone widthmixed crystal

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